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41.
Ken Hosoya Mitsuko Bendo Nobuo Tanaka Yoshiyuki Watabe Tohru Ikegami Hiroyoshi Minakuchi Kazuki Nakanishi 《大分子材料与工程》2005,290(8):753-758
Summary: Uniformly sized polymer particles were prepared by an emulsification and polymerization technique utilizing a silica monolithic membrane, namely the “silica monolithic membrane emulsification technique”. In this paper, we utilized silica monolithic membrane as a device for the preparation of uniformly sized polymer particles. A mixture of monomers, diluents and oil‐soluble initiator was emulsified into a continuous medium through the silica monolithic membrane and polymerized. The particles obtained had a higher size uniformity than that of particles prepared by previously reported membrane emulsification techniques, such as the Shirasu Porous Glass (SPG) emulsification technique. Through the silica monolithic membrane emulsification technique, we could prepare particles having availability as a possible packing material for solid‐phase extraction (SPE) and high performance liquid chromatography (HPLC).
42.
求解变系数方程的高斯消元法与高斯-约当消元法计算原理类似、问题相近,但前者计算速度高于后者.提出分段对称反向高斯-约当消元法,其中包括根据系数矩阵结构特点构成特殊增广阵,以展示和应用元素的变化规律,并分段对上下三角元素消元以大大提高计算效率.对矩阵下三角元素正向消元及对称计算可简化所有下三角元素计算,而对上三角元素反向消元可再省略所有上三角元素计算,而取倒后的对角元素作为规格化因子可大大减少除法计算.根据单位矩阵结构特点,对其规格化或对系数矩阵上下三角元素消元时均仅计算部分对角元素和下三角元素可进一步提高计算效率.所有元素均用四角规则计算而无需计算公式以简化计算和编程.新方法大大减少了高斯-约当消元法中元素的计算,且原理简单、易于编程,可快速求解各种变系数方程,还可利用元素对称性求解常系数的节点阻抗矩阵.与高斯消元法和高斯-约当消元法相比,新方法计算速度大大提高. 相似文献
43.
Pin Yang Carolina A. Gomez Samantha Andrews Josef D. Sorenson Ken S. Chen 《Journal of the American Ceramic Society》2021,104(7):3247-3259
The electric discharge across a varistor granule filled air gap under a fast-rising voltage pulse was investigated for surge protection applications. The effects of temperature and pressure on the arc and the electrical conduction were analyzed by the characteristic changes in voltage waveforms triggered by a fast-rising high voltage pulse. In addition to the gap size, experimental results show that competing mechanisms among arc conduction, conduction through the varistor granule network, thermionic emission from Joule heating at granule-to-granule contact points, and the magnitude of the switching voltage dictate the maximum surge protection voltage for the filled air gap. Experimental evidence indicated that accumulated degradation was created at small contact points between varistor granules by repetitive assaults from longer duration, high voltage pulses. The uniqueness of using varistor over other dielectric granules in an air gap for surge protection is identified and discussed. 相似文献
44.
Lingyun Lyu Takeshi Hanada Naohiro Yamahira Jun Morita Ryota Yamamoto Ken Itomi Takumi Adachi Sho Kubouchi Shin Horiuchi 《应用聚合物科学杂志》2021,138(45):51443
The distribution of nano-sized silica in binary rubber blends is characterized by scanning transmission electron microscopy (STEM) tomography combined with energy dispersive X-ray spectrometry (EDX). 3D distribution of silica is visualized by STEM-EDX tomography with the tilt-series of silicon elemental maps, while the phase-separated morphologies of polyisoprene rubber (IR) and styrene-butadiene rubber (SBR) are visualized by STEM-tomography in high-angle-annular-dark field (HAADF) mode. The combination of STEM-EDX and STEM-HAADF tomography enables us to determine the distribution of silica between the two rubber phases quantitatively even with high contents of silica up to 70 phr (weight parts per hundred rubber). It is found that silica is preferentially distributed in the SBR phase, but it is also distributed in the IR phase when the IR fraction in the total rubber components is higher than 40 wt%. The preferential distribution of silica in the SBR phase improves the dispersion of the IR domains. This is the first use of this technique for a multicomponent polymer system, showing the advantage to characterize the complicated multicomponent polymer composite morphologies. 相似文献
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46.
Negative bias illumination stress assessment of indium gallium zinc oxide thin‐film transistors 下载免费PDF全文
Electrical performance stability of indium gallium zinc oxide (IGZO) thin‐film transistors (TFTs) is evaluated under negative bias illumination stress (NBIS). A bottom‐gate IGZO TFT whose top surface is passivated with zinc tin silicon oxide (ZTSO) exhibits a dramatic improvement in NBIS stability compared with that of an unpassivated, bottom‐gate IGZO TFT. Oxygen chemisorption/desorption at the channel layer top surface is proposed to explain why an unpassivated TFT exhibits significantly more NBIS than a passivated TFT. 相似文献
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For precise orientation and strain measurements, advanced Electron Backscatter Diffraction (EBSD) techniques require both accurate calibration and reproducible measurement of the system geometry. In many cases the pattern centre (PC) needs to be determined to sub-pixel accuracy. The mechanical insertion/retraction, through the Scanning Electron Microscope (SEM) chamber wall, of the electron sensitive part of modern EBSD detectors also causes alignment and positioning problems and requires frequent monitoring of the PC. Optical alignment and lens distortion issues within the scintillator, lens and charge-coupled device (CCD) camera combination of an EBSD detector need accurate measurement for each individual EBSD system.This paper highlights and quantifies these issues and demonstrates the determination of the pattern centre using a novel shadow-casting technique with a precision of ∼10 μm or ∼1/3 CCD pixel. 相似文献
50.
Recently, we revealed a standard pattern of a macroscopic molecular network for controlling morphogenetic processes such as the development of organs, including blast, mesoderm, heart, and hands during about sevenfold cell divisions and a standard bio-chemical clock like the circadian one (Naitoh in Artif Life Robot 13, 2008; Japan J Ind Appl Math 28(1), 2011; J Phys Conf Ser 344, 2012; Artif Life Robot 17, 2012) A network model derived logically based on experimental observations is described by a nonlinear differential equation for predicting time evolutions of six macroscopic molecular groups: three gene groups and three enzyme groups, which include promoting and suppressing factors. Here, the macroscopic model extended for also describing aging processes shows various types of cycles and reveals the physical condition for determining whether or not living beings such as humans can survive after getting ill. It is stressed that, after becoming ill, living systems with overly fast generation of information molecules such as various genes end in death, whereas relatively fast production of enzymes leads to recovery. This may also explain an essential feature underlying carcinogenic processes. 相似文献