Crystallization mechanisms of phase change (GeSbSn)(100-x)Co(x) optical recording films

In this study, the (GeSbSn)(100-x0Co(x) films (x = 0-13.3) were deposited on natural oxidized silicon wafer and glass substrate by dc magnetron co-sputtering of GeSbSn and Co targets. The ZnS-SiO2 films were used as protective layers. The thicknesses of the (GeSbSn)(100-x)Co(x) films and protective layer were 100 nm and 30 nm, respectively. We investigated the effects of Co addition on the thermal property, crystallization kinetics, and crystallization mechanism of the GeSbSn recording film. The crystallization temperatures of (GeSbSn)(100-x)Co(x) films were decreased with Co content. It was found that the activation energy of the (GeSbSn)(100-x)Co(x) films will decrease from 1.53 eV to 0.55 eV as Co content increased from 0 at.% to 13.3 at.%.     

A novel authenticated group key agreement protocol for mobile environment

An authenticated group key agreement protocol allows a group of parties to authenticate each other and then determine a group key via an insecure network environment. In 2009, Lee et al. first adopted bilinear pairings to propose a new nonauthenticated group key agreement protocol and then extend it to an authenticated group key agreement protocol. This paper points out that the authenticated protocol of Lee et al. is vulnerable to an impersonation attack such that any adversary can masquerade as a legal node to determine a group key with the other legal nodes and the powerful node. This paper shall employ the short signature scheme of Zhang et al. to propose a new authenticated group key agreement protocol. The short signature scheme of Zhang et al. is proven to be secure against the adaptive chosen-message attacks in the random oracle model, so the proposed protocol can withstand the possible attacks. Besides, compared with the authenticated protocol of Lee et al., the proposed protocol is more secure and efficient.     

Design to suppress return-back leakage current of charge pump circuit in low-voltage CMOS process

A new charge pump circuit has been proposed to suppress the return-back leakage current without suffering the gate-oxide reliability problem in low-voltage CMOS process. The four-phase clocks were used to control the charge-transfer devices turning on and turning off alternately to suppress the return-back leakage current. A test chip has been implemented in a 65-nm CMOS process to verify the proposed charge pump circuit with four pumping stages. The measured output voltage is around 8.8 V with 1.8-V supply voltage to drive a capacitive output load, which is better than the conventional charge pump circuit with the same pumping stages. By reducing the return-back leakage current and without suffering gate-oxide overstress problem, the new proposed charge pump circuit is suitable for applications in low-voltage CMOS IC products.     

Identification of rod dynamics under influence of Active Magnetic Bearing

The purpose of this paper is to apply the wavelet transform algorithm to identify the magnetic damping and magnetic stiffness coefficients of the drive rod with which a set of 4-pole Active Magnetic Bearing (AMB) is equipped. By taking advantage of time–frequency analysis feature, the ridge curve of rod free response after wavelet transformation can be extracted to find the natural frequency of the rod/AMB system. In other words, due to the influence of magnetized field by the AMB, the stiffness of the rod dynamics is not linear any more and can be estimated from the curve of the amplitude versus frequency by wavelet transformation. On the other hand, the nonlinear damping coefficients can be estimated from the derivative of amplitude versus amplitude by wavelet transformation of rod free vibration. It is found that the nonlinear magnetic damping coefficients are up to 2nd-order in polynomial and the stiffness coefficient is mainly of 3rd-order respectively. In addition, the identified 2nd-order damping coefficient is negative and hence implies that under specific rod displacement and speed, the dynamic of the rod/AMB system in axial direction is unstable.     

Computerizing ICBF Method for Schedule Delay Analysis

Schedule delay is a common construction dispute. For analyzing schedule delays, a previous study had proposed an academic analysis method, the “isolated collapsed but-for” (ICBF) method. However, because many construction projects involve numerous complex activities, the procedure of using the ICBF method for schedule delay analysis is time-consuming. Therefore, this study used Microsoft Visual Basic for Applications (VBA) language and spreadsheet techniques to develop an Excel-based program for rapid delay analysis rather than manual calculation. A case study confirmed that the program automatically produces analytical results with only common delay documents (as-planned and as-built schedules and identified delay events). Compared with previous studies, schedule analysts can obtain analysis results quickly and correctly. Research results provide not only a convenient tool for schedule delay analysis but also a guide to computerize various academic delay analysis methods in the future.     

Occurrence of histamine and histamine-forming bacteria in kimchi products in Taiwan

Twenty kimchi products sold in supermarkets and 17 products sold in retail markets were purchased from southern Taiwan and tested to determine the occurrence of histamine and histamine-forming bacteria. The levels of pH and salt content in all samples ranged from 3.6 to 5.1 and 1.5–16.0%, respectively. The supermarket kimchi products had 1–7.2 log CFU/g of APC and <3–600 MPN/g of total coliform (TC), and the retail market kimchi products had 4–8.03 log CFU/g of APC and <3 to >2400 MPN/g of TC. Only one of the retail market kimchi products contained 20 MPN/g Escherichia coli. Although, supermarket kimchi products had an average histamine content of 49.8 mg/100 g, 15 of them had histamine content greater than 5 mg/100 g, the allowable level set by the US Food and Drug Administration (FDA) for scombroid fish and/or product. In contrast, only eight retail market kimchi products had histamine levels greater than 5 mg/100 g. Among the supermarket samples, three contained histamine at 50.2, 273 and 535 mg/100 g, that are more than the 50 mg/100 g hazard action level. Four histamine-producing bacteria capable of producing 13.6–43.1 ppm of histamine in MRS broth supplemented with 0.25% l-histidine were identified as Lactobacillus para. paracasei (one strain), Lb. brevis (one strain), and Brevibacillus brevis (two strains). To our knowledge, this is the first report to demonstrate the occurrence of high contents of histamine and histamine-forming bacteria in kimchi products.     

Improved agar diffusion method for detecting residual antimicrobial agents

The improved agar diffusion method for determination of residual antimicrobial agents was investigated, and the sensitivities of various combinations of test organisms and assay media were determined using 7 organisms, 5 media, and 31 antimicrobial agents. Bacillus stearothermophilus and synthetic assay medium (SAM) showed the greatest sensitivity for screening penicillins (penicillin G and ampicillin). The combination of Bacillus subtilis and minimum medium (MM) was the most sensitive for tetracyclines (oxytetracycline and chlortetracycline), B. stearothermophilus and SAM or Micrococcus luteus and Mueller-Hinton agar (MHA) for detecting tylosin and erythromycin, B. subtilis and MHA for aminoglycosides (streptomycin, kanamycin, gentamicin, and dihydrostreptomycin), B. stearothermophilus and SAM for polyethers (salinomycin and lasalocid), and B. subtilis and MM or Clostridium perfringens and GAM for polypeptides (thiopeptin, enramycin, virginiamycin, and bacitracin). However, gram-negative bacterium Escherichia coli ATCC 27166 and MM were better for screening for colistin and polymixin-B. For detecting the synthetic drugs tested, the best combination was B. subtilis and MM for sulfonamides, E. coli 27166 and MM for quinolones (oxolinic acid and nalidixic acid), B. subtilis and MM for furans (furazolidone), and the bioluminescent bacterium Photobacterium phosphoreum and luminescence assay medium for chloramphenicol and oxolinic acid. The results showed that the use of four assay plates, B. stearothermophilus and SAM, B. subtilis and MM, M. luteus and MHA, and E. coli 27166 and MM, was superior to the currently available techniques for screening for residual antimicrobial agents in edible animal tissues.     

A reactive modifier that enhances the thermal mechanical properties of epoxy resin through the formation of multiple hydrogen-bonded network

In this study, we synthesized a reactive modifier [DOPO-tris(azetidine-2,4-dione)], terminated with three azetidine-2,4-dione functional groups, from [(9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-yl)tris(4-aminophenyl)methane; DOPO-triamine] and [4-isocyanato-4′-(3,3-dimethyl-2,4-dioxo-acetidino)diphenylmethane; IDD]. We embedded this reactive modifier, which contains multiple hydrogen bond donor and acceptor units, into epoxy resins to promote intermolecular interactions and to tailor its flexibility through the formation of unique pseudo-crosslinked polymer networks. The resulted epoxy resins were found to exhibit glass transition temperature as high as 187 °C and excellent flame retardancy with limited oxygen index (LOI) values around 38. Meanwhile, the dynamic mechanical analysis (DMA) of epoxy systems increases from 0.67 to 2.13 GPa for storage modulus and 0.73–1.67 GPa for loss modulus at 100 °C. Incorporation of reactive modifier into epoxy networks with noncovalent interactions via thermosetting blend was demonstrated to be an effective way to enhance the thermal and physical properties simultaneously.     

Drawing and tensile properties of polyamide 6/calcium chloride composite fibers

The influence of calcium chloride (CaCl₂) contents on the drawing and tensile properties of polyamide 6 (PA6)/CaCl₂ composite fibers prepared at varying drawing temperatures were investigated. At any fixed drawing temperature, the achievable draw ratio (D_ra) values of PA6_x(CaCl₂)_y as-spun fiber specimens approach a maximum value, as their CaCl₂ contents are close to the 3 wt% optimum value. The maximum D_ra values obtained for PA6_x(CaCl₂)_y as-spun fiber specimens prepared at the optimum CaCl₂ content reach another maximum as their drawing temperatures approach the optimum drawing temperature at 120 °C. The initial modulus, tensile strength and birefringence values of the PA6 and PA6_x(CaCl₂)_y fiber specimens were found to improve consistently with D_ra or with drawing temperatures when they were stretched to a fixed D_ra. Similar to those found for their achievable drawing properties, the ultimate initial modulus, tensile strength and birefringence values of PA6_x(CaCl₂)_y fiber specimens approach a maximum value, as their CaCl₂ contents and drawing temperatures approach the 3 wt% and 120 °C optimum values, respectively. Experiments including thermal, FTIR, melt shear viscosity and wide angle X-ray diffraction experiments were performed on the PA6_x(CaCl₂)_y resin and/or fiber specimens to clarify the possible reasons accounting for the interesting drawing, tensile and birefringence properties found for the PA6_x(CaCl₂)_y fiber specimens.