超高效液相色谱-荧光法测定蜂蜜中百里香酚的残留量

建立了超高效液相色谱-荧光检测法测定蜂蜜中百里香的残留量的检验方法。用40%乙腈-水溶液提取蜂蜜中的百里香酚,经离心、上清液过滤后,以0.1%甲酸水溶液-乙腈为流动相进行梯度洗脱,采用Accucore aQ色谱柱(150 mm×2.1 mm,2.6μm)分离,荧光检测器检测(激发波长274 nm,发射波长297 nm),外标法定量。结果表明,百里香酚在0.01～3.00μg/mL范围内线性关系良好,决定系数(R²)为0.9999,在蜂蜜基质中的平均加标回收率在87.4%～106.9%之间,变异系数在0.7%～7.3%之间,定量限为0.10 mg/kg。利用该方法测定了48份市售蜂蜜样品,仅有1份样品存在百里香酚残留。本研究建立的方法简单、迅速、可靠,适用于蜂蜜中百里香酚残留的批量筛查和定量测定。     

孟加拉硫磷项目完成工程设计

孟加拉侯赛化学有限公司(HCCL)150kt/a粒状普钙(GSSP)工程是由南化集团设计院和中国化工建设总公司共同承包的化肥交钥匙工程.该工程包括60kt/a硫磺制酸及150kt/a粒状普钙,硫酸工艺采用快速熔硫、自然沉降和"3+1”两转两吸工艺,普钙采用湿磨磷矿、磷矿浆混化、皮带化沉、造粒和干燥工艺.中方主要负责工程的设计,主要设备、材料的采购,设备安装和开车指导;外方负责工程的土建设计,施工及设备、材料的安装工作.工程造价约406万美元(不含外方负责工作费用).目前,已完成工程的详细设计和主要设备的采购,预计工程将于2002年8月完工投产,工程建成后,可极大缓解该国的化肥紧缺状况. (南化集团设计院邱世庭)     

降低轧棉和纺纱工序中杂质的模块化解决方案

杂质分离器是一种有效的降低纤维杂质的工具。搭配几种灵敏感应器模块的系统能有效地检测和去除几类杂质。这样的系统也可成功地用于轧棉工序。     

Defects in CVDZnS

Defects seriously influence the optical properties and mechanical properties of CVDZnS.The deposition technique was introduced and experiment methods such as SEM,TEM and OM were adopted to study the defects:hexagonal phase,abnormally large grains,micro-cracks,micro-pores and impurities.The microstructures of these defects were observed,and the formation mechanisms of these defects were analyzed.Hexagonal ZnS as an impurity causes anisotropy in different directions with different refraction indexes and increases the scattering of CVDZnS.Increasing the deposition temperature can inhibit the formation of the hexagonal phase.The main reason for the growth of abnormally large grains in CVDZnS is high deposition rate.The lower deposition temperature increases growth stress in CVDZnS,which consequently results in the bowing of CVDZnS plates,and introduces microscopic defects such as grain blending and micro-cracks in the crystal.Micro-pores and impurities are induced by high reactant concentration in the local deposition chamber,which can be avoided by improving the gas flowing so as to make the concentration more uniform.     

巴勒体育馆

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制水花园的神秘故事

项目地点:西班牙塞埃欣项目类型:景观设计开工日期:2005年12月该项目获2005年豪瑞可持续建筑大奖赛欧洲地区提名奖     

Volatile fraction and sensory characteristics of Manchego cheese. 2. Seasonal variation

An automatic purge and trap apparatus, coupled to a GC-MS was used to study the seasonal variability of the volatile fraction of raw milk Manchego cheese. Both season and dairy significantly affected abundance of most volatile compounds. Most aldehydes, methyl ketones, n-alcohols, and secondary alcohols reached significantly higher concentrations in spring cheeses. Branched chain alcohols showed significantly higher concentrations in autumn and winter cheeses, while significantly higher amounts of diketones were found in summer cheeses. Most ethyl esters reached higher concentrations in spring and winter cheeses and lower in autumn cheeses. Lower concentrations of alpha-pinene were found in spring cheeses, and higher amounts of limonene were observed in winter cheeses. Heptane and octane were significantly more abundant in summer cheeses. No significant seasonal differences were found either for quality or intensity scores.     

Molecular identification of nine commercial flaffish species by polymerase chain reaction-restriction fragment length polymorphism analysis of a segment of the cytochrome b region

Commercial refrigerated or frozen flatfish fillets are sometimes mislabeled, and identification of these mislabeled products is necessary to prevent fraudulent substitution. Identification of nine commercial flatfish species (order Pleuronectiformes), Hippoglossus hippoglossus (halibut), Lepidorhombus boscii (four-spotted scaldfish), Lepidorhombus whiffiagonis (megrin), Platichthys flesus (flounder), Pleuronectes platessa (European plaice), Reinhardtius hippoglossoides (Greenland halibut), Scophthalmus maximus (turbot), Scophthalmus rhombus (brill), and Solea vulgaris (=Solea solea) (sole), was carried out on the basis of the amplification of a 486-bp segment of the mitochondrial genome (tRNA(Glu)/cytochrome b) by using the polymerase chain reaction (PCR) and universal primers. Sequences of PCR-amplified DNA from the flatfish species were used to select eight restriction enzymes (REs). The PCR products were cut with each RE, resulting in species-specific restriction fragment length polymorphism. Seven species groups could be identified by application of the single RE DdeI and six species groups by using HaeIII, HinfI, MaeI, or MboI. Different combinations of only a couple of these REs could unambiguously identify the nine flatfish species. Genetic polymorphisms of the target sequence were examined by comparison with previously published DNA sequences, and the results of this comparison confirmed the usefulness of this technique in distinguishing and genetically characterizing refrigerated or frozen pieces of these nine flatfish species.     

Evanescent wave coupling in light scattering of an off-axis normally incident Gaussian beam by two parallel nonabsorbing cylinders

A theoretical and numerical investigation is devised for resonant light scattering of an off-axis normally incident Gaussian beam by two parallel nonabsorbing cylinders based on the related beam theory developed in J. Opt. Soc. Am. A 14, 640 (1997). By varying the half-beam width, we show that the multireflection process between the two scatterers can be minimized. Moreover, the study is an attempt to understand the underlying physics present in the process of resonance excitation by evanescent wave coupling.     

图形点阵LCD在手提式多元素X荧光仪中的应用

基于T6963C的图形点阵液晶显示器,功能低、与微机适配接口电路简单、显示方式灵活。介绍了该显示器在电致冷半导体探头手提式多元素X荧光仪应用中,汉字、下接菜单、能谱曲线等显示的编程技巧,及其与嵌入式PC104工控机的实用接口电路。