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61.
Depolymerization of the biopolymer chitosan by an autoclaving process at 121°C and 15 psi was investigated using various treatments. Acetic acid was found to be the most effective solvent in decreasing chitosan viscosity among the six organic acids tested. The rate of viscosity decrease increased with increasing chitosan concentration. The viscosity of 1% chitosan in 1% acetic acid decreased rapidly to 91% of the initial viscosity following the initial 15 min of autoclaving. This decreased gradually to 93% and 94% in 30 and 60 min, respectively, without being adversely affected by the chitosan solution volume. The degree of deacetylation was comparable before and after autoclaving for 60 min. Chitosan at three molecular weights (Mr = 1597, 1110, and 789 kDa) decreased in molecular weight by 46%–51% in the 15‐min treatment, 55%–60% in the 30‐min treatment, and 60%–62% in the 60‐min treatment. The addition of 0.1%–1.0% (v/v) concentrations of hydrogen peroxide to the chitosan solution autoclaved for 15 min decreased viscosity by 94%–98% and molecular weight by 69%–83%. This process is a simple, timesaving, homogeneous depolymerization procedure, and it is possible to prepare partially hydrolyzed chitosan with specified molecular weights by regulating the time of treatment. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 87: 1890–1894, 2003 相似文献
62.
The adsorption of molecular hydrogen on model zeolites has been simulated employing Grand Canonical Monte Carlo (GCMC) procedure. The effects of cation type, available volume, surface area, temperature, pressure and pre-adsorbed organics such as benzene on the hydrogen uptake are analyzed. The hydrogen adsorption can be affected mainly by the available volume and surface area per g-zeolite at the same temperature and pressure. Increase of temperature results in the decrease of sorption intensity and capacity. The adsorption capacity correlates well with the pressure with high linearity at room temperature. Adsorption is lowered by the pre-adsorbed benzene molecule. The orientation and the number of benzene molecule in zeolite affect the adsorption capacity. The organic zeolite with larger available volume shows larger adsorption capacity. 相似文献
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64.
本文对“TL-1”天龙一号国产弧焊机器人在汽车车厢前板总成焊接生产线上实际应用进行了分析,并对焊接对象的选取、工艺布置、夹具及夹具控制系统,机器人与夹具的循环系统,系统可靠性和抗干扰措施的诸方面进行了论述。 相似文献
65.
本文得出了PbS和PbO交互反应的速率方程:(da)/(dt)=kx_(PbS)~3x_(PbO)^(-2);发现了反应过程中有过渡产物碱式硫酸铅(PbSO_4·2PbO);从电子转移角度,探讨了反应机理。 相似文献
66.
Jong-Young?Park Young-Soo?No Byung-Jun?Park Hyun-Woo?Lee Ji-Won?Choi Jin-Sang?Kim Y.?Ermakov Seok-Jin?Yoon Young-Jei?Oh Won-Kook?ChoiEmail author 《Metals and Materials International》2004,10(4):351-355
A low energy N2 ? ion beam impinged on a α-Al2O3(0001) single crystal surface in the range of fluence 5×1015/cm2?1×1018/cm2 at room temperature. After ion bombardment, chemical bonding on the modified sapphire surface was investigated by x-ray photoelectron spectroscopy. Below a fluence of 1×1015/cm2, only a non-bonded N1s peak at the binding energy 398.7 eV was found, but further irradiation up to 2×1017/cm2 induced Al?O?N bonding at around 403 eV. The occurrence of Al?N bonding was identified at ion fluence higher than 5×1017/cm2 at 396.6 eV. II–VI ZnO thin films were grown on an untreated/ion-beam-induced sapphire surface by pulsed laser deposition (PLD) for the investigation of the modified-substrate effect on photoluminescence. The ZnO films grown on modified sapphire containing Al?O?N bonding only, and both Al?O?N and Al?N bonding showed a significant reduction of the peak related to deep-level defects in photoluminescence. These results are explained in terms of the formation of Al?N?O and Al?O?N layers and relaxation of the interfacial strain between Al2O3 and ZnO. 相似文献
67.
用2kw CO 激光和送粉工艺,在4Cr5MoV_1Si 钢表面熔覆一层高温耐磨合金(Ni 基高温合金+WC),并应用于轧钢机导向板工作面。用扫描电子显微镜、电子探针和 x 射线衍射技术分别进行熔覆层的组织形态观察,微区成分分析和物相的鉴定。结果表明,熔覆层显微组织主要有许多弥散分布的 W_2C、(W,Ti)C_(1-x)、WC 和共晶态的 M_(12)C 及γ(f、c、c)母体相组成。室温及高温硬度测试结果表明,熔覆层有适中的室温硬度和相对较高的高温硬度。实际生产考核结果表明,激光熔覆导向板使用寿命大大提高,每对可轧钢1000~1100吨,而4Cr_5MoV_1Si 和普碳钢分别为400~500吨和200吨。 相似文献
68.
69.
Kirsten Bobzin Erich Lugscheider Felix Ernst Reimo Nickel Nazlim Bagcivan Daniel Parkot Arne Schlegel Stefania Ferrara Tatyana Kashko Noémi Leick 《Microsystem Technologies》2008,14(12):1887-1894
Nowadays, micro components have to fulfill rising optical requirements for different scientific and industrial fields like
astronomy, medicine or multimedia. For this purpose, advanced miniaturized chip-cameras are produced for the microsystems
engineering market. The assembly and joining technologies play a very important role in the production of these micro components.
Several challenges are associated with the joining of chip-cameras. In this study, the application of the soldering technology
has been considered in order to face these challenges. Two joining technologies have been investigated: active soldering and
transient liquid phase (TLP) bonding. Both soldering processes have shown a big potential for hybrid microsystems joining
in previous studies. For both processes, soldering alloys and parameters have been conceived in order to fulfill the joining
requirements of the micro camera components. For instance, the joining temperature represents a major challenge because the
chip-camera consists of a plastic material, polymethyl methacrylate (PMMA). Therefore, particular attention has been directed
to the soldering as well as to the coating temperature. The experimental investigations concerning the solders application
through physical vapor deposition (PVD) have been supported by finite element method (FEM) simulations. The analysis of the
temperature distribution in the micro components during the coating process was the focus of the calculations. Possible undesirable
local overheated areas of the chip-camera components can be detected through simulation.
相似文献
Tatyana KashkoEmail: |
70.
Hyun Uk Yun Chul Jin Kim Sung Joo Kim No Cheol Park Hyunseok Yang Young-Pil Park 《Microsystem Technologies》2009,15(10-11):1531-1538
Microactuators for micromirror system have found many applications in various areas including projection displays, optical switches, RF switches and so on. In this paper we demonstrated micromirror actuator using ionic polymer metal composites (IPMC) that is a suitable candidate, since it has many attractive qualities such as durability, aquatic, miniature and light-weighted. Specially, IPMC has extraordinary advantages which are simple bending motion for low driving voltage (1–2 V), low power consumption, and simple structure. The IPMC actuator is made of Nafion NE-1110 (Dupont Co, Ltd., 260 µm thick) layer and electrode (platinum) layers and driven by 1–4 V. The displacement measured vertically is 0.25 mm and tilting angle is 11.3°. The angular motion, which is more than 10°, is a good advantage in the field of display module. This paper shows that the IPMC actuator has enough possibility for other applications. 相似文献