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61.
SU-8 pillar-assisted epitaxial assembly of toric focal conic domains (TFCDs) arrays of smectic-A liquid crystals is studied. The 3D nature of the pillar array is crucial to confine and direct the formation of TFCDs on the top of each pillar and between neighboring pillars, leading to highly ordered square and hexagonal array TFCDs. Excellent agreement between the experimentally obtained critical pillar diameter and elasticity calculation is found.  相似文献   
62.
The aim of this project is the development of a noninvasive technique based on LED multispectral imaging (MSI) for monitoring the conservation state of the Dead Sea Scrolls (DSS) collection. It is well-known that changes in the parchment reflectance drive the transition of the scrolls from legible to illegible. Capitalizing on this fact, we will use spectral imaging to detect changes in the reflectance before they become visible to the human eye. The technique uses multivariate analysis and statistical process control theory. The present study was carried out on a "sample" parchment of calfskin. The monitoring of the surface of a commercial modern parchment aged consecutively for 2 h and 6 h at 80 °C and 50% relative humidity (ASTM) was performed at the Imaging Lab of the Library of Congress (Washington, DC, U.S.A.). MSI is here carried out in the vis-NIR range limited to 1 μm, with a number of bands of 13 and bandwidths that range from about 10 nm in UV to 40 nm in IR. Results showed that we could detect and locate changing pixels, on the basis of reflectance changes, after only a few "hours" of aging.  相似文献   
63.
Natural ventilation can contribute to the reduction of the air conditioning demand and to the improvement of thermal comfort in buildings. In this paper, the flow field and the air change rate generated by a simple configuration of natural ventilation, namely single-sided ventilation, are examined experimentally. The experiments are realized in a full scale building exposed to outdoor conditions, using several measurement techniques. The main features of the flow generated by stack and wind effect are examined for different outdoor conditions (temperature difference, wind speed and direction). Finally, measured air change rates are compared to those calculated by existing correlations in order to analyze their applicability to the experimental configuration. Results show that the wind generates turbulence diffusion at the opening, counteracting the stack effect. Moreover, in the case of windward opening, there is an additional effect, namely the effect of mixing layer, which tends to increase the airflow rate. Existing correlations give reasonably good results in the case of windward opening, while in the case of leeward opening they overestimate the airflow rate.  相似文献   
64.
Diamond micro-powders of 28/20 μm mean particle size were sintered under conditions of high pressure of 6.0 and 8.0 GPa at temperatures of 1600, 1700, and 1800 °C during various sintering times, aiming to obtain polycrystalline compacts with required strength. The experiments were carried out by using an anvil type high pressure device with toroidal concavity of 13.5 mm diameter. It was obtained samples with 4.5 mm diameter and 5.0 mm height. It was plotted the polycrystalline diamonds density dependency as a function of the process duration under the above mentioned sintering conditions. The kinetics of powder consolidation was studied by X-ray diffraction, which allowed the establishment of the correlation between the (3 3 1) plane enlargement of diamond and the structural transformations that took place during sintering. Another objective was the study of the graphitization kinetics of diamonds under the action of the sintering parameters. It was concluded that over the established consolidation mechanisms, also acts the partial shear mechanism.  相似文献   
65.
The present research examined the relationship between adherence to honor norms and emotional reactions after an insult. Participants were 42 Dutch male train travelers, half of whom were insulted by a confederate who bumped into the participant and made a degrading remark. Compared with insulted participants with a weak adherence to honor norms, insulted participants with a strong adherence to honor norms were (a) more angry, (b) less joyful, (c) less fearful, and (d) less resigned. Moreover, insulted participants with a strong adherence to honor norms perceived more anger in subsequent stimuli than not-insulted participants with a strong adherence to these norms. The present findings support a direct relationship among insult, adherence to honor norms, and emotional reactions. (PsycINFO Database Record (c) 2010 APA, all rights reserved)  相似文献   
66.
This analysis deals with advances in models concerning the floating zone technique as well as with novel results on the relative importance of various parameters in the crystal-growth process. The attention is focused in particular on microgravity fluid-dynamic aspects and on the effect of the volume of the liquid melt since the cylindrical configuration is expected to be only a very special case under microgravity conditions. The instability of Marangoni flow is investigated by direct three-dimensional and time-dependent simulation of the problem and parallel computations. Body-fitted curvilinear co-ordinates are adopted to handle the non-cylindrical shape. A novel realistic distribution is considered to model the surface heat flux generated by a ring heater positioned around the equatorial plane at a fixed distance from the axis of the liquid (full) zone.The fluid-dynamic environment that occurs inside the melt is very sensitive to the geometrical aspect ratio AF (length/diameter) of the floating zone and to the volume factor S (ratio of the volume of the liquid zone and the volume of the corresponding cylindrical configuration: convex S>1, concave S<1). The role played by the geometrical constraints and degrees of freedom of the Marangoni toroidal rolls in determining the azimuthal structure and the stability of the flow field is discussed.  相似文献   
67.
Polymer-supported methyltrioxorhenium (MTO) compounds are shown to act as efficient and selective catalysts for the oxy-functionalization of C–H bonds in representative hydrocarbon derivatives (leading to the corresponding alcohols or ketones), using H2O2 as oxidant. The different supports used for the heterogenation of MTO, such as poly(4-vinylpyridine), poly(4-vinylpyridine)-N-oxide and polystyrene resins, all showed different catalytic behaviour in terms of substrate conversion and product yield, depending on the experimental conditions used. It is noteworthy that the novel heterogeneous catalysts were found to be stable, it being possible to effect their recover and recycle at least five times without appreciable loss of activity.  相似文献   
68.
This paper applies a recently developed on-line parameter identification (PID) technique to sets of real flight data and compares the results with those of a state-of-the-art off-line PID technique. The on-line PID technique takes Linear Regression from Fourier Transformed equations and the off-line PID is based on the traditional Maximum Likelihood method. Sets of flight data from the NASA F/A-18 High Alpha Research Vehicle (HARV) aircraft, which has been recorded from specifically designed maneuvers and used for off line parameter estimation, are used for this study. The emphasis is given on the accuracy and on-line measure of reliability of the estimates. The comparison is performed for both longitudinal and lateral-directional dynamics for maneuvers at angles of attack ranging α=20δ through α=40δ. Results of the two estimation processes are also compared with baseline wind tunnel estimates whenever possible.  相似文献   
69.
Nb2O5 is known as good promoter for adsorption/desorption kinetics of hydrogen in magnesium hydride. In this article the interaction with hydrogen of bare Nb2O5, the oxidic component of the mixed MgH2/Nb2O5 system, is investigated in various conditions (i.e. employing atomic, molecular and nascent hydrogen). The state of the hydrogen-Nb2O5 system was monitored using various techniques including: X-ray Diffraction, Electron Paramagnetic Resonance, Diffuse Reflectance UV-Vis Spectroscopy, Thermal Desorption Spectroscopy -Mass Spectrometry, Differential Scanning Calorimetry and Thermal Programmed Desorption. Niobium (V) oxide is not at all inert while interacting with hydrogen. This oxide is partially reduced by hydrogen, which is incorporated in the solid and released as both molecular hydrogen and water. This peculiar behaviour, reminiscent of some properties of the bronze family, suggests an active chemical role played by Nb2O5 in the mixed MgH2/Nb2O5 system.  相似文献   
70.
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