氢化可的松母液错流萃取行为研究

将氢化可的松母液解析为氢化可的松、表氢化可的松和６α－羟基ＲＳ三种组分，模拟了母液的表观分配系数。拟合结果与实验值符合较好，平均相对误差＜５．５％。     

Micromechanical properties on the surface of PVC/SBR blends spatially resolved by a nanoindentation technique

The microhardness and micromodulus on the surface of poly(vinyl chloride) (PVC)/styrene‐butadiene rubber (SBR) blends were determined using a nanoindenter. A flat surface was obtained by microtoming the sample at ?100°C in liquid nitrogen. Dozens of indents along a line with a spatial interval of 0.5 μm were performed. From the loading and unloading curves of each indentation, the stiffnesses of the unloading curve and the contact area between the sample and the indenter were evaluated, and the local modulus and hardness were calculated. Profiles of the local hardness and modulus were obtained from the lines of indents. Pure PVC and a miscible PVC/acrylonitrile‐butadiene rubber (NBR) (40/10) blend showed constant modulus and hardness values. In the case of an immiscible PVC/SBR (50/50) blend, which has a morphology of elongated PVC droplets in the SBR matrix, the hardness and modulus profiles showed regions of the different phases. At the interface between the SBR and PVC phases, a step change in the modulus and hardness profiles was observed. The force required to deform the material at the same displacement increased systematically across the interface from the SBR to the PVC phase because of the increasing contribution of the PVC phase. Polym. Eng. Sci. 44:609–614, 2004. © 2004 Society of Plastics Engineers.     

PTC型BaTiO3陶瓷的孪晶和孪晶界

用透射电镜和高分辨电镜观察研究了PTC型BaTiO_3陶瓷的孪晶和孪晶界结构,并提出了可能的{111}孪晶及孪晶界的原子结构模型。结果表明,{111}孪晶形成氧八面体共面的共格倾斜孪晶界,在孪晶界处可能存在一定量的A空位且原子密度要低于孪晶体内。同时还发现两种其它特征的孪晶现象。     

基于计划值理论的互联网专线投资管理策略研究

计划值管理是一种有计划、高效率支撑企业生产运营的独特管理模式。借鉴其在钢铁行业成功应用的经验,结合互联网专线业务的特点,将计划值理论引入通信企业互联网专线投资管理工作中,构建科学、合理、灵活的互联网专线计划值管理指标体系。     

一种基于来电平台的新型提醒类业务

随着电信技术以及互联网应用的飞速发展,越来越多的新兴业务出现,给传统电信业务,尤其是各类手机业务带来了巨大挑战,同时,也对传统运营商的创新能力以及满足用户各类需求的能力提出了更高要求。本文介绍的换号提醒业务就是从用户需求的角度出发,对用户进行各种细节的关心,提升手机用户的业务体验。     

现代陶艺在环境空间中的应用

空间对于现代陶艺和环境建筑同样重要。陶艺空间和建筑空间因功能要求而定。现代陶艺以各种形式置身于环境空间之中,需要和它相适应的装饰语言。空间意识的改变,会产生一种全新的公共空间。增强人们对建筑与人文环境认识,将建筑的规模缩小为自然与人的空间。现代陶艺不仅构筑的是结构形体的空间,更表现的是一种博大的容纳品性。     

Polyimide foams with ultralow dielectric constants

To explore ultralow dielectric constant polyimide, the crosslinked polyimide foams (PIFs) were prepared from 3,3′,4,4′‐benzophenonetetracarboxylic dianhydride (BTDA), 4,4′‐oxydianiline (ODA), and 2,4,6‐triaminopyrimidine (TAP) via a poly(ester–amine salt) (PEAS) process. FTIR measurements indicated that TAP did not yield a negative effect on imidization of PEAS precursors. SEM measurement revealed the homogeneous cell structure. Through using TAP as a crosslinking monomer, the mechanical properties of PIFs could be improved in comparison with uncrosslinked BTDA/ODA based PIF. The crosslinked PIFs still exhibited excellent thermal stability with 5% weight loss temperatures higher than 520°C. In the field with frequency higher than 100 Hz, the dielectric constants of the obtained PIFs ranged from 1.77 to 2.4, and the dielectric losses were smaller than 3 × 10^?2 at 25–150°C. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 1734–1740, 2006     

气固下行流化床反应器Ⅱ气固两相的流动规律

气固下行流化床反应器气固两相流动过程是比较复杂的，沿轴向气固两相运动可分为第一加速、第二加速和恒速３个运动段，沿径向局部气体速度、颗粒速度和颗粒浓度都具有不同程度的不均匀性。而这种不均匀性是由气固两相顺重力场湍动运动所决定的。和循环床提升管相比，下行管反应器气固两相沿径向分布的不均匀性得到有效地改善，气固可以实现超短接触操作，因而是一种新型高效气固超短接触反应器     

改性蛋白土填充线型低密度聚乙烯的研究

对超细加工并经硅烷偶联剂处理的蛋白土填充线型低密度聚乙烯进行了研究,结果表明:采用适当的偶联剂及恰当的添加量,改性蛋白土可以降低塑料的成本。     

基于信息流缺陷定位方法在软件测试中的应用

随着软件产业的飞速发展,人们对软件质量的要求也越来越高.现在,软件已经直接影响到了我们项目的成功和设备的安全.而软件中的复杂缺陷难以排除,因为它们涉及到许多程序要素之间的相互作用.论文扩展了基于信息流覆盖的缺陷定位技术.扩展后的技术融合了语句覆盖和分支覆盖技术,它还能定位复杂缺陷.试验结果表明,文中方法比基于语句覆盖、分支覆盖和定义使用对覆盖的方法要更可靠、更精确.