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21.
Hanjin Kwag Dipak Rana Kyucheol Cho Jangweon Rhee Taewoo Woo Byung H. Lee Soonja Choe 《Polymer Engineering and Science》2000,40(7):1672-1681
The rheology and morphology of four sets of binary blends of polyethylene synthesized with metallocene catalysis (metallocene polyethylene: MCPE) with polyolefins prepared using Ziegler‐Natta catalysts have been investigated. The blend systems are MCPE with high density polyethylene (MCPE‐HDPE), polypropylene (MCPE‐PP), poly(propylene‐co‐ethylene) (MCPE‐CoPP), and poly(propylene‐co‐ethylene‐co‐1‐butylene) (MCPE‐TerPP). Cole‐Cole plots [storage melt viscosity (η′) versus loss melt viscosity (η″)], plots of the dynamic storage modulus (G′) versus the dynamic loss modulus (G″), and plots of the log melt viscosity (η*, η′, and η″) versus blend compositions were constructed. The morphology of the blends after microtoming and etching was studied. The phase morphology of MCPE‐HDPE appeared homogeneous, whereas the other three blends were heterogeneous. Rheological and morphological investigations indicated that the MCPE‐HDPE blend was miscible, but the other three blends were immiscible in the melt as well as in the solid state. These observations can be rationalized in terms of the similarity of the chemical structures of the polyolefins. 相似文献
22.
Byung-Hak Choe Soo-Keun Shin Sung-Joon Kim Yong-Tai Lee S. B. Kang Masuo Hagiwara 《Metals and Materials International》2005,11(6):429-433
The effects of aging treatment on the microstructures and mechanical properties of a metastable beta titanium alloy Ti-15-3
(Ti−15V−3Al−3Sn-3Cr) have been investigated with hardness measurements, tensile test, and optical and electron microscopy.
Precipitate-free beta structure with average grain size of about 56 μm was obtained after solution treatment at 800°C for
15 min followed by air cooling. Solution treated specimens were aged up to 800 h in the temperature range between 350 and
600°C. The morphology of the precipitates was varied significantly, depending on the aging temperature. The fine aggregates
of α precipitates were dominant above 450°C. Peak hardness values were maintained up to 800 h at 500°C, which showed the superior
thermal stability of α precipitates. Tensile strength increased up to 1600 MPa along with the decrease of elongation after
aging at 350 and 400°C. 相似文献
23.
24.
J. X. Hou C. W. Zhan X. L. Tian X. C. Chen Yong-Suk Kim Heeman Choe 《Metallurgical and Materials Transactions A》2012,43(11):4023-4027
The temperature-dependent viscosity and X-ray diffraction (XRD) patterns of a Cu65Sn35 melt were investigated at high temperatures. The viscosity of the melt changed discontinuously at about 1283?K (1010?°C). An XRD analysis of the Cu65Sn35 melt revealed no obvious changes in the correlation radius, whereas the coordination number increased abruptly at a similar temperature with that mentioned previously, i.e., 1283?K (1010?°C) during the cooling process. The results indicate a redistribution of atoms in the nearest environment. The structural transition at the higher temperature was attributed to a change of combination mode of nearest atoms in the short-range order cluster of the Cu65Sn35 melt. 相似文献
25.
This paper examines the feasibility of extracting useful information from customer comments using a Naïve Bayes classifier. This was done for a database, obtained from a large Korean mobile telephone service provider, of 533 customer calls to call centers in 2009. After eliminating calls not containing customer complaints or comments, the remaining 383 comments were classified by an expert panel into four domains and 27 complaint categories. The four domains were Transaction‐related (189 comments, 49%), Product‐related (120 comments, 31%), Customer Service or Support‐related (38 comments, 10%) and Customer Outreach and Marketing‐related (36 comments, 9%). The comments were then randomly assigned to either a training set (257 cases, 67%) or test set (126 cases, 33%). The training set was used to develop a Naïve Bayes classifier that correctly predicted the domain 75% of the time and the specific subcategory 51% of the time for the test set. Prediction accuracy was strongly related to prediction strength for both sets of predictions, suggesting that simple filtering strategies where difficult to understand comments are flagged for expert review and easy comments are automatically classified are both technically feasible and likely to be practically valuable. Several strong predictors were also identified that corresponded to categories more detailed than those originally assigned. © 2012 Wiley Periodicals, Inc. 相似文献
26.
This paper analyzes the stability and convergence properties of a proportional–integral protocol for coordination of a network of agents with dynamic information flow and quantized information exchange. In the setup adopted, each agent is only required to exchange its coordination state with its neighboring agents, and the desired reference rate is only available to a group of leaders. We show that the integral term of the protocol allows the agents to learn the reference rate, rather than have it available a priori, and also provides disturbance rejection capabilities. The paper addresses the case where the graph that captures the underlying network topology is not connected during some interval of time or even fails to be connected at all times. 相似文献
27.
Abdul Latif Ahmad Choe Peng Leo Syamsul Rizal Abd. Shukor 《Journal of Porous Materials》2009,16(1):33-40
Porous γ-alumina with well arranged secondary mesopores has been contrived using nanosized templating units. The pore size
of templated mesopores is precisely controlled as the pore shrinkage is insignificant. The primary pore diameter is ca. 4 nm
and the secondary pore diameter is ca. 50 nm. The porous material was characterized using N2 adsorption/desorption, TEM, XRD and FT-IR. γ-alumina with bimodal pore size distribution shows improved intra-particle diffusion
compared to γ-alumina with unimodal pore size distribution in a simple dye adsorption test. γ-alumina with different porous
structures were then impregnated with vanadium oxide for catalytic effect comparison. It was perceived that secondary pores
improve the styrene oxidation rate after the conversion of styrene reaches 30%. 相似文献
28.
J.W. Nam S.H. Cho Y.C. Choi J.S. Ha J.H. Park D.H. Choe J.B. Yoo J.H. Park 《Diamond and Related Materials》2005,14(11-12):2089
CNT paste consists of organic solution, inorganic binder and filler. Organic solution contains organic resins and solvent including surfactants which finely disperse CNTs. Filler affects surface morphology, electron emission property, viscosity, and rheological characteristics of CNT paste. We used different fillers such as silver and alumina in CNT paste for special function. The emission properties of CNT paste with silver are similar to those of CNT paste with alumina if filler portion is the same. From the scanning electron microscope (SEM) different morphologies of CNTs was observed depending on the type of filler. CNT paste which showed good emission property had vertically well-aligned CNTs on the surface after surface treatment using adhesive tape. We measured viscosity and rheological properties with rheometer RS600 from HAAKE. Emission property of CNT paste was evaluated in vacuum chamber of 10− 6 Torr with pulse generator and duty was 1/500. 相似文献
29.
ABSTRACT: Effects of sesame oil addition to soybean oil during frying on the lipid oxidative stability and antioxidants contents of fried products during storage in the dark were studied. Flour dough pieces (2 cm × 2 cm × 0.1 cm) were fried at 160 °C for 1 min in sesame oil-added soybean oil. Concentrations of sesame oil in the frying oil were 0%, 10%, and 20% by volume. Fried products were put into a glass bottle, and the bottles were tightly sealed and stored at 60 °C in the dark for 18 d. Lipid oxidation of fried products was determined by fatty acid composition changes and conjugated dienoic acid (CDA) and p -anisidine (PA) values. Tocopherols and lignan compounds in the fried products were determined by high-performance liquid chromatography. Relative content of linolenic acid decreased, and CDA and PA values increased during storage of the fried products in the dark. Fatty acid composition change and CDA and PA values during storage were lower in the products fried in sesame oil-added soybean oil than in the products fried in soybean oil without sesame oil. The results clearly showed that addition of roasted sesame oil to soybean oil at 10% and 20% during frying decreased the lipid oxidation of fried products during storage in the dark for 18 d by extension of induction period and decrease in decomposition of oxidized lipids. Fried products contained 134 to 267 ppm tocopherols and 0 to 148 ppm lignans before storage; however, their contents decreased during storage in the dark. Lignan compounds were more stable than tocopherols, and the rate of tocopherols degradation was lower in the products fried in sesame oil-added soybean oil than in the products fried in soybean oil without sesame oil, which could be because of protection of tocopherols from degradation by lignan compounds. 相似文献
30.
We present a fourth-order (4, 4) finite-difference time-domain (FDTD)-like algorithm based on the integral form of Maxwell's equations. The algorithm, which is called the integro-difference time-domain (IDTD) method, achieves its fourth-order accuracy in space and time by taking into account the spatial and temporal variations of electromagnetic fields within each computational cell. In the algorithm, the electromagnetic fields within each cell are represented by space and time integrals (or integral averages) of the fields, i.e., the electric and magnetic fluxes (D,B) are represented by the surface-integral average, and the electric and magnetic fields (E,H) by the line and time integral average. In order to relate the integral average fields in the staggered update equations, we have obtained constitutive relations for these fields. It is shown that the IDTD update equations combined with the constitutive relations are fourth-order accurate both in space and time. The fourth-order correction terms are represented by the modified coefficients in the update equations; the numerical structure remains the same as the conventional second-order update equations and more importantly does not require the storage of field variables at the previous time steps to obtain the fourth-order accuracy in time. Furthermore, the Courant-Friedrichs-Lewy (CFL) stability criteria of this fourth-order algorithm turns out to be identical to the stability limits of conventional second-order FDTD scheme based on differential formulation. 相似文献