直接氯化法合成对硝基氯化苄

介绍了以对硝基甲苯和氯气为原料 ,在催化剂存在下合成对硝基氯化苄的方法 ,考察了催化剂种类、反应温度、溶剂配比等因素对反应的影响 ,优化的反应条件为 :对硝基甲苯用量 1 3 7g,对硝基甲苯 /邻二氯苯 (摩尔比 ) =1∶ 0 .6,w (偶氮二异丁腈 ) =0 .6% ,反应时间 3 h,反应温度 1 60℃ ,产物单程收率大于 65 % ;将反应混合物中未反应的原料分离后 ,以无水乙醇为溶剂结晶纯化 ,物料 /溶剂 (摩尔比 ) =1∶ 1 .5时晶体含量在 99.0 %以上 ,结晶收率达 67     

On the interaction impedance of the coupled cavity structure

The formula and program for calculating the total and negative first harmonic interaction impedance from the data of “large perturbation measurement” are given. This program is a part of the programs for CCTWT design.     

基于一种特定混沌映射的跳频序列

使用一种简单的分段线性映射构造混沌跳频序列。用于跳频通信中取代传统的伪随机序列（PN序列），分析了此混沌序列的周期性。平衡性，汉明相关特性和线性间隔，最后给出了混沌序列的神经网络实现。仿真和实验结果表明，此序列具有较好的统计特性。应用于跳频多址通信中，可获得较好的抗干扰。抗截获能力。     

新型高温高密度W/O乳化钻井液的研制

研制了油包水乳化钻井液的基本配方，评价了其抑制性，热稳定性，以及抗水侵污能力，抗钻屑侵污能力，抗水泥侵污能力。现场应用表明，该体系具有较强的抑制作用，能很好地稳定井壁，保护油气层。     

Nondestructive evaluation of the characteristics of degraded materials using backward radiated ultrasound

The frequency dependency of Rayleigh surface wave is investigated indirectly by measuring the angular dependency of the backward radiation of the incident ultrasonic wave in two kinds of degraded specimens by scuffing or corrosion. Then, the frequency dependency is compared with the residual stress distribution or the corrosion-fatigue characteristics for the scuffed or corroded specimens, respectively. The width of the backward radiation profile increases with the increase of the variation in residual stress distribution for the scuffed specimens. In the corroded specimens, the profile width decreases with the increase of the effective aging layer thickness and is inversely proportional to the exponent, m, in the Paris’ law that can predict the crack size increase due to fatigue. The result observed in this study demonstrates high potential of backward radiated ultrasound as a tool for nondestructive evaluation of subsurface gradient of material degradation generated by scuffing or corrosion.     

Partitioning for pseudo-exhaustive testing is NP-complete

In the letter, two schemes of circuit partitioning for pseudo-exhaustive testing are described. The complexities of both are proved to be NP-complete.     

数字电视传输流的实时码率变换系统

数字视频压缩后通常是打包成传输流的形式进行传送，年个传输流有其固定的发送码率，在某些应用场合，比如信道调制前端，需要对输入传输流码率进行改变以适应该信道要求，描述了一种全硬件实现，双路输出，实时，节目可选择的码率变换系统的原理及具体实现。     

功率电子器件用AlN陶瓷基板的研制

阐述了AlN陶瓷的烧结原理 ,分析了烧结工艺参数对大面积AlN基板性能的影响 ,成功研制出了高热导率(190W /m·K)、大面积 (14 0mm× 90mm)、翘曲度为 2 0 μm/5 0mm的AlN陶瓷基板。     

Pruning Redundant Alarm Correlation Patterns

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Parameters evaluation of SOLA algorithm for time scale modification

Successful operation of the Synchronous Overlap and Add (SOLA) algorithm for Time Scale Modification (TSM) of speech is closely tied to the proper choice of parameters. This paper investigates the quality of time scale modified speech under different values of primary parameters. Based on Mean Opinion Score (MOS) tests and Bark Spectral Distortion (BSD) measure, the proper choices of synthesis shift (Ss) and the duration of the shift search interval (K _max?) are given experimentally. The conclusions can be helpful for operating the SOLA algorithm for time scale modification of speech.