Development of FeSiB/CoSiB Bilayered Melt-spun Ribbon by?Melt-spinning Technique

The investigation addresses the bilayer melt-spun ribbons in which the positively magnetostrictive layer Fe_77.5Si_7.5B₁₅ is toward the free surface, while the negatively magnetostrictive layer of Co_72.5Si_12.5B₁₅ forms the one in contact with the quench wheel. Scanning electron microscopy (SEM) elemental scan showed drastic changes in concentration profiles of Co, Fe and Si across the bilayer, indicating the efficacy of rapid quenching by melt spinning. Crystallization onsets, saturation magnetization and dilatation studies of the single-layered alloys distinctly reflected the properties of the bilayered ribbons. The thermal variation of coercivity below crystallization onset in the case of a bilayer revealed a softening mechanism due to reduction of stresses. Ribbon deflection studies showed interesting results.     

Effect of mineral acids on the production of alumina nanopowder from raw bauxite

In this study a novel synthetic method for the large-scale production of spherical, high surface area and ultra-fine alumina (Al₂O₃) powder has been described. Synthetic Bayer liquor was extracted by alkali fusion of raw bauxite with sodium hydoxide. Alumina nanopowders were synthesised through a ball mill-aided precipitation method using the synthetic Bayer liquor and mineral acid precipitants. The powders produced were characterised by X-ray diffraction (XRD), particle size distribution (PSD), Fourier transform infrared spectroscopy (FTIR), Brunauer-Emmett-Teller surface area and pore size analysis, energy-dispersive spectroscopy (EDS), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). In this article, the effects of precipitants such as H₂SO₄, HCl and HNO₃ on crystallite and particle size, surface area, pore volume, and pore size and shape are reported. The experimental results prove that precipitation leads to an aggregated particle that is disaggregated by the ball-milling method. The ball milling process strongly influences the formation of uniform-sized spherical particles with a high surface area. It was revealed that nitric acid is an effective precipitant for controlling particle size and textural properties of Al₂O₃ powder. A nanopowder of γ-Al₂O₃ with an average crystallite size of 3 nm and an average particle size of 58 nm with a specific surface area (SSA) of 190 m² g^− 1 is produced. This article elucidates a new method with a simple reaction scheme for the mass production of Al₂O₃ nanoparticles from raw bauxite for various commercial applications.     

Impact modification of poly(trimethylene terephthalate)/polypropylene blend nanocomposites: Fabrication and characterization

A poly(trimethylene terephthalate) (PTT)/polypropylene (PP) blend and the nanocomposites were prepared with and without the addition of a compatibilizer precursor [maleic anhydride grafted polypropylene (MAPP)]. A reactive route was used for the compatibilization with the addition of MAPP during melt blending in a batch mixer. Organically modified nanoclays were used as nanoscale reinforcements to prepare the blend nanocomposites. Mechanical tests revealed optimum performance characteristics at a PTT/PP blend ratio of 80 : 20. Furthermore, incorporation of nanoclays up to 3 wt % showed a higher impact strength and higher tensile strength and modulus in the blend nanocomposites compared to the optimized blend. The nanocomposite formation was established through X‐ray diffraction and transmission electron microscopy (TEM). Thermal measurements were carried out with differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). DSC thermograms revealed an increase in the crystallization temperature in the presence of the nanoclays in the blend system containing Cloisite 30B. TGA thermograms also indicated that the thermal stability of blend increased with the incorporation of Cloisite 30B. Furthermore, dynamic mechanical analysis measurements showed that the Cloisite 30B nanocomposite had the maximum modulus compared to other nanocomposites. TEM micrographs confirmed an intercalated morphology in the blend nanocomposites. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2011     

Piezoelectric components wirelessly driven by dipole antenna-like electric field generator

A new technique of transmitting electric energy wirelessly to piezoelectric components by using a dipole antenna-like electric field generator is explored. Two square size brass plate-shaped live and ground electrodes are used to form a dipole antenna-like electric field generator. When the dipole antenna-like electric field generator in electric resonance with an inductor, a maximum output power of 2.72 mW and an energy conversion efficiency of 0.0174% have been achieved wirelessly by the piezoelectric plate area of 40 mm² operating in the thickness vibration mode, placed at the center 4 mm away from the antenna plane with an optimum electrical load of 1365 Ω, resonant frequency of 782 kHz, 1 cm electrodes separation, 2500 cm² electrode area of dipole antenna-like structure, and input ac source power of 15.58 W applied to the series of dipole antenna-like structure and inductor. The theoretically calculated results have been validated by the experimental studies. It is seen that at the resonance frequency and optimum electrical load, the output power of the wirelessly driven piezoelectric component decreases with the size of piezoelectric component, distance of piezoelectric component from the electrode of antenna plane, but increases with the antenna electrode area.     

On the Variation of Ortho-hydrogen and?Para-hydrogen Ratio with Magnetic Field Strength at?Low Temperature

We report inversion of population between the ortho and para states of hydrogen at very low temperature with homogeneous external magnetic field. At low temperature, one needs to apply very high magnetic fields to get this population inversion when ortho states will be more populated than the para one. A?numerical study of the change of bond length with magnetic field has been employed to find the precise field strengths at crossover points.     

Solubilization and refolding of bacterial inclusion body proteins

Inclusion bodies produced in Escherichia coli are composed of densely packed denatured protein molecules in the form of particles. Refolding of inclusion body proteins into bioactive forms is cumbersome, results in poor recovery and accounts for the major cost in production of recombinant proteins from E. coli. With new information available on the structure and function of protein aggregates in bacterial inclusion bodies, it has been possible to develop improved solubilization and refolding procedures for higher recovery of bioactive protein. Inclusion bodies are formed from partially folded protein intermediates and are composed of aggregates of mostly single types of polypeptide. This helps to isolate and purify the protein aggregates to homogeneity before solubilization and refolding. Proteins inside inclusion body aggregates have native-like secondary structures. It is assumed that restoration of this native-like secondary structure using mild solubilization conditions will help in improved recovery of bioactive protein in comparison to solubilization using a high concentration of chaotropic agent. Analysis of the dominant forces causing aggregation during inclusion body formation provides information to develop suitable mild solubilization procedures for inclusion body proteins. Refolding from such solubilized protein will be very high due to restoration of native-like secondary structure. Human growth hormone inclusion bodies were purified to homogeneity from E. coli cells before solubilization and refolding. Pure inclusion bodies were solubilized at alkaline pH in the presence of 2 M urea solution. The solubilized proteins were refolded using a pulsatile renaturation process and subsequently purified using chromatographic procedures. More than 40% of the inclusion body proteins could be refolded back to the bioactive native conformation. Mild solubilization is thus the key for high recovery of bioactive protein from inclusion bodies.     

多孔电极臭氧发生器氧化废水中有机物的吸收和反应动力学分析(英文)

A novel electrode design for the in situ generation of ozone in the reaction zone of a tubular reactor is described in this work.The ozone generator uses a porous inner electrode tube in the corona discharge assembly,and the ozone generated around the outer periphery of the porous tube diffuses into the tubular reactor and reacts with the contaminants in the fluid that is being treated.A mathematical model that includes absorption and second order reaction in the film is developed to describe ozonation kinetics of a contaminant dye in the tubular reactor.The model describes the experimental data for dye decolorization,oxidation byproducts,dissolved ozone,and ozone gas concentrations well.Model analysis indicates that the fast dye decolorization reaction occurs partly in the liquid film and partly in the bulk fluid.The model can be used in the selection of appropriate gas-liquid contactors for efficient oxidation of contaminants in effluents.     

A compact dual‐band 2 × 1 metamaterial inspired mimo antenna system with high port isolation for LTE and WiMax applications

This article proposes a compact (43 × 26 × 0.8 mm³) dual‐band two‐element metamaterial‐inspired MIMO antenna system with high port isolation for LTE and WiMAX applications. In this structure, each antenna element consists of a square–ring slot radiator encircling a complementary split ring resonator. A tapered impedance transformer line feeds these radiating apertures and shows good impedance matching. A 2 × 3 array of two‐turn Complementary Spiral Resonator structure between the two antenna elements provides high dual‐band isolation between them. The fabricated prototype system shows two bands 2.34 – 2.47 GHz (suitable for LTE 2300) and 3.35 – 3.64 GHz (suitable for WiMAX). For spacing between two antennas of 10 mm only, the measured isolation between the two antenna elements in the lower band is around ?32 dB while that in the upper band is nearly 18 dB. The system shows a doughnut‐shaped radiation patterns. The peak measured antenna gains for the proposed MIMO system in the lower and higher bands are 3.9 and 4.2 dBi, respectively. The MIMO system figure of merits such as the envelope correlation coefficient, total efficiency are also calculated and shown to provide good diversity performance.     

Potential field method to navigate several mobile robots

Navigation of mobile robots remains one of the most challenging functions to carry out. Potential Field Method (PFM) is rapidly gaining popularity in navigation and obstacle avoidance applications for mobile robots because of its elegance. Here a modified potential field method for robots navigation has been described. The developed potential field function takes care of both obstacles and targets. The final aim of the robots is to reach some pre-defined targets. The new potential function can configure a free space, which is free from any local minima irrespective of number of repulsive nodes (obstacles) in the configured space. There is a unique global minimum for an attractive node (target) whose region of attraction extends over the whole free space. Simulation results show that the proposed potential field method is suitable for navigation of several mobile robots in complex and unknown environments. Saroj Kumar Pradhan is faculty of Mechanical Engineering Department with N.I.T., Hamirpur, HP, India. He has received his B.E. degree in Mechanical Engineering from Utkal University and M.E. in Machine Design and Analysis from NIT Rourkela. He has published more than 17 technical papers in international journals and conference proceedings. His areas of research include mobile robots navigation and vibration of multilayred beams. Dayal R. Parhi is working as Assistant Professor at NIT Rourkela, India. He has obtained his first Ph.D. degree in “Mobile Robotics” from United Kingdom and Second Ph.D. in “Mechanical Vibration” from India. He has visited CMU, USA as a “Visiting Scientist” in the field of “Mobile Robotics”. His main areas of current research are “Robotics” and “Mechanical Vibration”. He is supervising five Ph.D. students in the fields of Robotics and Vibration. Email: dayalparhi@yahoo.com. Anup Kumar Panda Received his M.Tech degree from IIT, Kharagpur in 1993 and Ph.D. degree from Utkal University in 2001. He is currently an assistant professor in the Department of Electrical Engineering at National Institute of Technology, Rourkela, India. His areas of research include robotics, Machine Drives, harmonics and power quality. He has published more than 30 technical papers in journals and conference proceedings. He is now involved in two R&D projects funded by Government of India. R. K. Behera is a Senior Lecturer of Mechanical Engineering at National Institute of Technology, Rourkela, India. He has been working as lecturer for more than 10 years. He obtained his BE degree from IGIT, Sarang, of Utkal University. He obtained his ME and Ph.D degrees, both in the field of mechanical engineering from NIT Rourkela.