Temperature anomaly of the Cd hyperfine field in a trivacancy complex in Ni

The temperature dependence of the Cd hyperfine field in a trivacancy complex in Ni between 25 and300 K is reported. It was found that, unlike the Cd substitutional field in Ni which follows the temperature dependence of the magnetization, the Cd hyperfine field in a trivacancy complex is essentially temperature independent. This temperature anomaly is compared with other temperature anomaly of impurity hyperfine fields in ferromagnetic hosts.     

软x射线近贴显微技术

软x射线近贴显微技术不但可使活的生物样品成象,分辨率高于光学显微镜,而且人为的样品准备程序在该技术中都可避免。本文描述了用高功率激光打靶产生的等离子体作为软x射线源而进行的近贴显微研究,并得到了分辨率好于1μm的结果。     

光照与彩陶俑表面色变关系的实验研究

本文以秦彩俑表面色彩为研究对象,通过光照实验与色彩变化的色度测量,分析了光照引起彩俑颜料色变的规律,为秦彩俑这一大型重点文物的色彩保护提供了科学理论依据.     

超短脉冲激光微束对细胞作用的研究

本文详细地介绍了我们自己设计和安装的一个Nd:YAG超短脉冲激光微束系统,该系统分成二个部分:激光源和显微镜。由电光调Q非稳腔Nd:YAG激光倍频后得到355nm紫外光进入显微镜并由物镜聚焦。同时,这超短脉冲激光微束照射在细胞上并且在细胞上产生一个可以自恢复的小孔。在文中我们还讨论了超短脉冲激光微束与细胞之间作用效应及机理。     

Pullback attractors for a non-autonomous incompressible non-Newtonian fluid

This paper studies the pullback asymptotic behavior of solutions for a non-autonomous incompressible non-Newtonian fluid in two-dimensional (2D) bounded domains. We first prove the existence of pullback attractors AV in space V (has H²-regularity, see notation in Section 2) and AH in space H (has L²-regularity) for the cocycle corresponding to the solutions of the fluid. Then we verify the regularity of the pullback attractors by showing AV=AH, which implies the pullback asymptotic smoothing effect of the fluid in the sense that the solutions become eventually more regular than the initial data.     

丁基罗丹明B-Bi(Ⅲ)-SCN~--PVA-Tween-80体系荧光熄灭法测定痕量铋

本文研究了在PVA和Tween 80存在下,铋离子与硫氰酸钾和丁基罗丹明B形成缔合型三元配合物,使丁基罗丹明B的荧光熄灭,建立了痕量铋的荧光分析新方法。工作曲线线性范围为0～5.0μg/25mL。方法灵敏度高,ε_(588)为3.5×10~5L·mol~(-1)·cm~(-1),操作简便。用于铸铁中痕量铋的测定,结果满意。     

一类泛函微分方程周期解的存在性与应用

本文给出了一类滞后型泛函微分方程有一个周期解的四个充分性定理，其结果明显地优于著名的Ｙｏｓｈｉｚａｗａ周期解定理，最后给出了应用实例。     

Irradiation-induced reduction and luminescence properties of Sm doped in BaBPO5

Usually, Sm²⁺ ions could be reduced by heating the materials in reducing atmospheres. Exposure to ionizing radiations is also known to cause Sm³⁺→Sm²⁺ conversion. In this work, BaBPO₅ doped with the samarium ion was prepared by high temperature solid-state reaction. Sm²⁺ ions were obtained by two different reduction methods, i.e., heating in H₂ reduced atmosphere and X-ray irradiation. The measurements of X-ray diffraction (XRD), and scanning electron microscope (SEM) were investigated. It is found that the conversion of Sm³⁺→Sm²⁺ is very efficient in BaBPO₅ hosts after X-ray irradiation. Sm²⁺ ions under these two reduction methods exhibit different characteristics that were studied by measurements of luminescence and decay. The results showed that the luminescence properties of Sm²⁺ ions in BaBPO₅ were highly dependent on the sample preparation conditions.     

θ*r,s,t-图与唯一2-列表染色图的特征化

如果一个图G存在一个k-列表安排使得G具有一个唯一列表染色,则称 G是唯一列表可染色图,简称UkLC图．我们称图G具有M(k)性质当且仅当G不 是UkLC图．本文在借鉴θr,s,t-图概念的基础上引入θr,s,t-图的定义,并证明:除了 r=s=t=2以外,θr,s,t-图都是U2LC图．利用如上结果我们给出M．Mahdian and E．S．Mahmoodian对U2LC图所作特征化的一个简单证明．     

Synthesis of optically active poly(N‐propargylsulfamides) with helical conformation

A novel chiral N‐propargylsulfamide monomer ( 1a ) and its enantiomer ( 1b ) were synthesized and polymerized with (nbd)Rh⁺B^?(C₆H₅)₄ as a catalyst providing poly(1) (poly( 1a ) and poly( 1b )) in high yields (≥99%). Poly(1) could take stable helices in less polar solvents (chloroform and THF), demonstrated by strong circular dichroism signals and UV–vis absorption peaks at about 415 nm and the large specific rotations; but in more polar solvents including DMF and DMSO, poly(1) failed to form helix. Quantitative evaluation with anisotropy factor showed that the helical screw sense had a relatively high thermal stability. These results together with the IR spectra measured in solvents showed that hydrogen bonding between the neighboring sulfamide groups is one of the main driving forces for poly(1) to adopt stable helices. In addition, copolymerization of monomer 1a and monomer 2 was conducted, the solubility of poly(1) was improved drastically. However, the copolymerization had adverse effects on the formation of stable helices in the copolymers. © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 500–508, 2007