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为了进一步掌握等离子体流动控制机理,完善等离子体激励器数学模型,提升等离子体激励器扰动能力,采用粒子图像测速技术,在静止空气下开展了介质阻挡放电等离子体激励器诱导射流特性研究.实验时,将非对称布局激励器布置在平板模型上,随后将带有激励器的模型放置在有机玻璃箱内,从而避免环境气流对测试结果的影响.基于激励器诱导流场,分析了激励电压对诱导射流特性的影响,揭示了较高电压下诱导射流近壁区的拟序结构,获得了卷起涡、二次涡等拟序结构的演化发展过程,计算了卷起涡脱落频率,阐述了卷起涡与启动涡的区别,初步探索了卷起涡的耗散机制.结果表明:(1)层流射流不能完全概括等离子体诱导射流特性,激励电压是影响射流特性的重要参数.当电压较低时,诱导射流为层流射流;当电压较高时,诱导射流的雷诺数提高,射流剪切层不稳定,层流射流逐渐发展为湍流射流.(2)等离子体诱导湍流射流包含着卷起涡、二次涡等拟序结构;在固定电压下,这些涡结构存在恒定的卷起频率.(3)当激励电压较高时,流动不稳定使得卷起涡发生了拉伸、变形,引起了流场湍动能增大,从而加速了卷起涡的耗散.研究结果为全面认识激励器射流特性,进一步挖掘激励器卷吸掺混能力,提升激励器控制能力积累基础. 相似文献
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高效阴离子交换色谱-脉冲安培检测法测定牛乳及制品中的唾液酸 总被引:1,自引:0,他引:1
建立了高效阴离子交换色谱分离-脉冲安培检测法检测常见唾液酸N-乙酰神经氨酸(Neu5AC)和N-羟乙酰神经氨酸(Neu5Gc)的方法,对影响分离和检测的条件进行了优化。以NaOH和NaAc为淋洗液,在CarboPac PA20阴离子交换柱上梯度分离,在30℃柱温,0.5 mL/min的流速下,20 min内可完成两种唾液酸的分析。使用脉冲安培检测法测定Neu5AC和Neu5Gc的线性范围为5~500μg/L;检出限为3.0和1.8μg/L(25.0μL进样,以3倍信噪比计算检出限)。将该方法用于15个牛乳及制品中Neu5AC和Neu5Gc的测定,两种唾液酸的标准加入回收率为88%~115%。方法具有灵敏、简便和环境友好的特点,样品前处理方法简单,方法适用性好。 相似文献
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氨基酸自动分析仪快速分析方法的研究 总被引:6,自引:0,他引:6
本文研究了适用于日立L8900氨基酸自动分析仪(L8800同样适用)的国产化缓冲溶液和茚三酮反应液配方,研究出了适用于日立L8900氨基酸自动分析仪的快速分析程序方法。结果表明:本文所研究的国产化试剂能够完全达到原装进口试剂的效果,并且相比原装试剂拥有更好的适应性,便于在国内推广使用。快速分析程序方法相比原装程序方法分析时间缩短至43 min,减少20%,具有分析时间短、检测成本更短,工作效率更高的优点,同时也减少了有机试剂的排放,降低了对实验人员和环境的伤害。 相似文献
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Measurement of the polarization for soft X-ray magnetic circular dichroism at the BSRF beamline 4B7B
Three ultra-short-period W/B4C multilayers (1.244 nm, 1.235 nm and 1.034 nm) have been fabricated and used for polarization measurement at the 4B7B Beamline at the Beijing Synchrotron Radiation Facility (BSRF). By using the rotating analyzer ellipsometry method, the linear polarization degree of light emerging from this beamline has been measured and the circular polarization evaluated for 700-860 eV. The first soft X-ray magnetic circular dichroism measurements are carried out at BSRF by positioning the beamline aperture out of the plane of the electron storage ring. 相似文献
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X-ray magnetic circular dichroism (XMCD) has become an important and powerful tool because it allows the study of material properties in combination with elemental specificity, chemical state specificity, and magnetic specificity. A new soft X-ray magnetic circular dichroism apparatus has been developed at the Beijing Synchrotron Radiation Facility (BSRF). The apparatus combines three experimental conditions: an ultra-high-vacuum environment, moderate magnetic fields and in-situ sample preparation to measure the absorption signal. We designed a C-type dipole electromagnet that provides magnetic fields up to 0.5 T in parallel (or anti-parallel) direction relative to the incoming X-ray beam. The performances of the electromagnet are measured and the results show good agreement with the simulation ones. Following film grown in situ by evaporation methods, XMCD measurements are performed. Combined polarization corrections, the magnetic moments of the Fe and Co films determined by sum rules are consistent with other theoretical predictions and experimental measurements. 相似文献