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BACKGROUND: A simple and quick on‐site test for trace levels of cadmium (Cd) in food is needed because of the human toxicity of this heavy metal. We developed an immunochromatography kit which uses the antigen‐antibody complex reaction between the Cd–ethylenediaminetetraacetic acid (Cd–EDTA) complex and an anti‐Cd–EDTA antibody. We previously reported the successful use of this kit to determine Cd concentrations in brown rice with respect to the international standard: 0.4 mg kg?1. Here, we measured, using this immunochromatography kit, Cd concentrations in crops with lower international standards than rice. RESULTS: Cadmium extracted with 0.1 mol L?1 HCl from wheat grain and fresh eggplant was purified sufficiently using an ion‐exchange column treatment. Appropriate HCl extraction rates and dilution rates for the column eluate were selected; Cd concentrations in wheat grain and fresh eggplant were determined successfully by immunochromatography with respect to the international standards of 0.2 mg kg?1 and 0.05 mg kg?1 fresh weight, respectively. CONCLUSION: Approximate Cd concentrations in wheat grain and fresh eggplant can be monitored easily and quickly by this method at locations where facilities for acid digestion and precision analysis are not available. Copyright © 2011 Society of Chemical Industry  相似文献   
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A straightforward method, which is termed novel handspinning, is reported for producing uniaxially aligned sPP nanofibers. As demonstrated by SEM analysis, the morphologies of handspun sPP nanofibers are strongly dependent upon the processing conditions such as spinning method and solvent system. Compared to the normal electrospun sPP nanofibers, the handspun sPP nanofibers show smoother morphologies. FT‐IR analysis demonstrates a significant difference in polymer chain conformation between the handspun and electrospun sPP nanofibers. Moreover, interestingly, the handspun sPP single nanofibers show higher Young's modulus and tensile strength than electrospun sPP single nanofibers.

  相似文献   

105.
Abstract

The fibre space holder (FSH) method combines powder metallurgy and lost-foam casting with the aim of producing novel ultra-thin materials with micro-porous structures. A fabric, used as a spaceholder, is coated with metal powder (stainless steel, copper, nickel or titanium) in a water-soluble polymer binder. During sintering, the spaceholder is removed by a high temperature treatment to obtain the final porous metal sheet. This new material combines the advantages of fabric and porous metal. Its large specific surface area, minimum thickness of <30 μm, maximum porosity of >95% and strong liquid absorbency make it suitable for various application, in particular electrodes in hydrogen fuel cells and medical applications. The metal sheet can be further functionalised by coating with nanopowders.  相似文献   
106.
随着中国、印度、东南亚及其它新兴国家的汽车化,带动了全球对初级能源的需求。预计2030年将比现在增加40%,于此同时,汽车将消耗60%的石油。为了减轻环境负担和使石油的消耗最小化,汽车生产厂商正在加速开发环境友好与节省燃料的汽车。我们的粉末冶金产品也越来越多地在支持我们的顾客开发环境友好汽车。这份报告简要述评了汽车产业的总趋势和汽车制造厂商在致力于创造的环境友好汽车,另一方面,在第二节后半部分概述了日立化成的粉末冶金产品支持这项工作的例子。  相似文献   
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Bis(cyclopentadienyl)magnesium (Cp2Mg) is a common source for p-type doping in GaN and AlInGaP materials. It is a white crystalline solid with very low vapor pressure, leading to transport problems similar to solid trimethyindium (TMI). Some of these problems can be alleviated by a newly developed source-solution magnesocene, Cp2Mg, dissolved in a solvent that is essentially nonvolatile. In this paper, we report the growth and comparative results of Mg-doped GaN grown by OMVPE using solid and solution Cp2Mg. Using both sources, we optimized parameters to obtain high-quality GaN growth with hole concentrations up to 1 1018/cm3.  相似文献   
109.
7 抗短路冲击强度的计算与验证 我公司现生产的干式变压器额定容量范围为 30~2 500kVA,下面以2 500kVA容量为例作一探讨。  相似文献   
110.
Secure group communications using key graphs   总被引:7,自引:0,他引:7  
Many emerging network applications are based upon a group communications model. As a result, securing group communications, i.e., providing confidentiality, authenticity, and integrity of messages delivered between group members, will become a critical networking issue. We present, in this paper, a novel solution to the scalability problem of group/multicast key management. We formalize the notion of a secure group as a triple (U,K,R) where U denotes a set of users, K a set of keys held by the users, and R a user-key relation. We then introduce key graphs to specify secure groups. For a special class of key graphs, we present three strategies for securely distributing rekey messages after a join/leave and specify protocols for joining and leaving a secure group. The rekeying strategies and join/leave protocols are implemented in a prototype key server we have built. We present measurement results from experiments and discuss performance comparisons. We show that our group key management service, using any of the three rekeying strategies, is scalable to large groups with frequent joins and leaves. In particular, the average measured processing time per join/leave increases linearly with the logarithm of group size  相似文献   
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