Characterization of wet microalgal cells pretreated with steam for lipid extraction

Steam pretreatment was employed to disrupt microalgal cells for lipids extraction.Effects of steam pre-treatment on microstructure of microalgal cells were investigated through scanning electron microscopy(SEM) and transmission electron microscopy (TEM).Effect of treatment on lipid extraction was also stud-ied.Microalgal cell walls were distorted after steam pretreatment due to the hydrolysis of organic macro-molecules contained in cell wall.Maximum curvature was increased from 1.88 × 10-6 m-1 to 1.43 × 10-7 m-1 after treatment with the steam at 130 ℃.The fractal dimension of microalgal cells increased from 1.25 to 1.30 after pretreatment for 15 min,and further increased to 1.47 when the pre-treatment time was increased to 60 min.Increased steam pretreatment temperature and time enhanced the hydrolysis of organic macromolecules,and finally destroyed microalgal cell walls at pretreatment temperature of 130 ℃ and pretreatment time of 60 min.Lipid extracted from wet microalgal was signif-icantly increased (2.1-fold) after pretreatment.     

Microstructure and properties of WC-8Co cemented carbides prepared by multiple spark plasma sintering

In this study, WC-8Co cemented carbides were prepared by spark plasma sintering. When the samples sintered at 1300℃ were cooled to room temperature, the samples were sintered multiple times at 1250℃. The changes in microstructure and mechanical properties of WC-8Co cemented carbides prepared by multiple spark plasma sintering were studied. The hardness of cemented carbides increased in the first two sintering, reaching 16.5 GPa. However, the hardness decreased seriously in the last two sintering. The attenuation rates of hardness were 6.2% and 2.5% due to the abnormal coarse grains. Furthermore, the crack path along the grain boundary was almost straight, causing a decrease in the indentation fracture toughness of cemented carbides. Additionally, the grains of cemented carbides were abnormally coarsened, and the morphologies of grains became unstable due to multiple sintering.     

Adsorption Mechanism and Electrochemical Properties of Methyl Blue onto Magnetic CoxCu(1–x)Fe2O4 Nanoparticles Prepared via an Alcohol Solution of Nitrate Combustion and Calcination Process

Journal of Inorganic and Organometallic Polymers and Materials - Magnetic CoxCu(1–x)Fe2O4 nanoparticles were prepared via an alcohol solution of nitrate combustion and calcination process....     

水压环形缝隙泄漏量的试验研究

在水压系统环形缝隙泄漏试验基础上，对圆柱形配合状态下的缝隙泄漏量进行了理论和试验对比研究，分析了两者的变化规律。得出的结果可以为水压元件的设计提供试验依据。     

MICROSTRUCTURES AND TEXTURES IN COLD-ROLLED ALUMINIUM STRIP

ＭＩＣＲＯＳＴＲＵＣＴＵＲＥＳＡＮＤＴＥＸＴＵＲＥＳＩＮＣＯＬＤＲＯＬＬＥＤＡＬＵＭＩＮＩＵＭＳＴＲＩＰ①ＮｉｅＺｕｏｒｅｎ，ＺｈａｎｇＸｉｎｍｉｎｇ，ＹｉｎＺｈｉｍｉｎＤｅｐａｒｔｍｅｎｔｏｆＭａｔｅｒｉａｌｓＳｃｉｅｎｃｅａｎｄＥｎｇｉｎｅｒｉ...     

热爆合成－热挤压TiNi棒材的组织结构和性能

研究了热爆合成－热挤压法制得的ＴｉＮｉ合金棒材的组织结构和性能。研究结果表明，所制取的棒材具有用传统法——熔铸法生产ＴｉＮｉ合金的性能，证明了用该法制取ＴｉＮｉ型材的途径是可行的     

深冷处理与工模具的耐磨性

热处理后的金属材料再经低落曙处理，其力学能明显提高，尤其是高碳高合金工模具钢的耐磨性提高特别显著。本文着重研究了应用面较广的Ｗ６Ｍｏ５Ｃｒ４Ｖ２钢的处理工艺制度，组织性能及其磨损机理。     

Conductivity enhancement in transparetn ZnO films via Al-dopping produced by CW-CO2 laser-induced evaporation

Highly conductive transparent aluminium-doped ZnO (ZnO:A1) films were successfully deposited by CW-CO₂ laser-induced evaporation. Optimisation of evaporation parameters was based on laser power, substrate temperature, O₂ partial pressure in the vacuum chamber and amount of Al in the ZnO source pellet. ZnO:A1 films with an electrical resistivity as low as 6.6 × 10⁻²Ω·cm and an optical transmission of 80% at 500nm were obtained at laser power of 15 W, substrate temperature of about 200°C, O₂ partial pressure of 6—7 × 10⁻⁴ Torr and 5wt.% Al. Conductivity of ZnO films can be increased one order via Al-doping in ZnO films. The films obtained by laser-induced evaporation have compared quite favorably with the high quality films obtained by sputtering.     

稀土含量对喷熔层组织及耐蚀性的影响

本文通过在镍基自熔合金粉末中加入不同含量的稀土，研究了稀土含量对喷熔层组织及耐蚀性的影响规律及其作用机制。结果表明，在喷熔材料中加入适量稀土，可使喷熔层组织细化、晶界净化，从而使腐蚀过程中的表面活性点减少，耐蚀性提高。     

锻压机械打击力测量误差的加速度补偿

提出了锻压机械打击力测量中存在的问题，介绍了常用的补偿法，并通过实验验证了加速度补偿法是消除锻压机械打击力测量误差的有效途径。