液态混合有机标准物质研究

本研究采用重量法配制有机液态混合标样 ,并对配制方法、混合标样的均匀性、稳定性及影响不确定度的因素进行了研究 ,并用气相色谱法进行了比对分析。经稳定性监测 ,稳定度大于等于一年 ,不确定度小于± 2 %。     

La doping effects on intergrowth Bi2WO6–Bi3TiNbO9 ferroelectrics

La doping effects on intergrowth Bi₂WO₆–Bi₃TiNbO₉ ferroelectric ceramics were studied by X-ray diffraction, electron probe microanalysis and dielectric spectroscopy. It was found that the La³⁺ distribution, ferroelectric phase transition and dielectric relaxation behavior are apparently affected by La doping. With increasing La³⁺ content, the site of dopant ion varies, the grain growth of Bi₅TiNbWO₁₅ is restrained, the Curie temperature is reduced and broadened. Furthermore, two dielectric relaxation loss peaks were observed both in temperature and frequency spectra. The calculated relaxation parameters revealed the oxygen vacancy related to the relaxation process.     

Data mining of resilience indicators

In recent years, the Asia-Pacific region has experienced several financial setbacks, including speculative attacks in 1998 and the SARS outbreak in 2003. Financial stresses of this nature are unanticipated, and not all of the dangers can be predicted by the examination of market information and macroeconomic indicators. The Early Warning System (EWS) that has been adopted by the International Monetary Fund may not be able to predict future financial crises for all possible scenarios, because shocks come in many different forms. To supplement the EWS, this paper proposes a data mining framework to measure the resilience of an economy. The resilience framework does not predict a crisis, but rather assesses the current state of health of an economy and its ability to withstand a financial shock should one occur. The framework is based on a feedback system consisting of two stages. The first stage assigns a resilience score to each economy based on a fuzzy logic scoring scheme that is built on the ambiguous reasoning of experts. The second stage uses the classification tree approach to estimate thresholds for each economic indicator, and examines the quality of the fuzzy score. The result from the second stage is then passed back to the first stage as feedback. The final result is obtained when the feedback system reaches its equilibrium state. The proposed resilience framework is applied to the external-sector and the public-sector economies of several countries to illustrate its applicability.     

The thermal behavior of mechanically activated galena by thermogravimetry analysis

The thermal decompositions of mechanically activated and nonactivated galenas were studied by thermogravimetry analysis (TGA) at the heating rate of 10 K min⁻¹ in argon. Results indicate that the initial temperature of thermal decomposition (abbreviated as T _di) in the TGA curves for different galenas decreases gradually with increased grinding time. The specific granulometric surface area (S _G), the structural disorder, and the content of elemental sulfur of mechanically activated galenas were analyzed by an X-ray diffraction (XRD) laser particle-size analyzer, XRD analysis, and the gravimetric method, respectively, which shows that the specific granulometric surface area of mechanically activated galenas remains almost constant after a certain grinding time, but the lattice distortions (ε) rise, the crystallite sizes (D) decrease, and the elemental sulfur contents of mechanically activated galenas increase with increased grinding time. The results imply that the decrease of the initial temperature of thermal decomposition in the TGA curves for mechanically activated galenas is mainly caused by the increase of lattice distortions, and the formation of new dangling bonds resulted from the production of elemental sulfur of mechanically activated galenas with increased grinding time. Finally, the differences in the thermal-decomposition reactivity between nonactivated and mechanically activated galenas were also discussed.     

自蔓延高温合成TiNi多孔体合金

为了开发新型的生体材料，本文对自蔓延高温合成TiNi多孔体合金——人造骨材料进行了研究。以单质钛粉和镍粉作原料，在氩气保护条件下，采用预热点燃模式和热爆模式制得了不同形态的多孔TiNi形状记忆合金。采用SEM和XRD分析了样品的孔洞特征和相组成，测试了其力学性能，并研究了合成条件参数与样品表面形貌和孔隙状态之间的关系。结果表明，用SHS法制备TiNi多孔体合金是可行的。     

WLAN chip antenna mountable above the system ground plane of a mobile device

A novel wireless local-area network (WLAN) chip antenna suitable to be mounted above the system ground plane of a mobile device is presented. The antenna in the study is easily fabricated from folding a single metal plate onto a foam base, and mainly comprises a short-circuited radiating strip and an antenna ground. The antenna ground occupies the bottom surface and two adjacent side surfaces of the foam base. When the antenna is mounted at the corner of the system ground plane, this antenna ground structure is expected to effectively reduce the antenna's possible fringing electromagnetic fields inside the mobile device. In this case, when the associated element such as the radio-frequency shielding metal case is placed under the proposed antenna, small or negligible variations in the antenna performance are obtained. Design considerations of the proposed antenna for WLAN operation in the 2.4 GHz band are described, and results of the constructed prototypes are presented.     

Surface-mount dual-loop antenna for 2.4/5 GHz WLAN operation

A surface-mount dual-loop antenna suitable for dual-frequency WLAN operation is presented. For achieving dual-frequency operation with a compact size, the antenna comprises two loop strips of different sizes printed on a flexible printed circuit board, which is then bent and attached onto a foam base of compact size. The antenna shows an attractive feature of high antenna gain, about 4 and 5 dBi for frequencies across the 2.4 and 5 GHz WLAN bands, respectively.     

Hydrogenated amorphous silicon thin-film transistor arrays fabricated by digital lithography

A jet-printed digital-lithographic method, in place of conventional photolithography, was used to fabricate 64 /spl times/ 64 pixel (300 /spl mu/m pitch) matrix addressing thin-film transistor (TFT) arrays. The average hydrogenated amorphous silicon TFT device within an array had a threshold voltage of /spl sim/3.5 V, carrier mobility of 0.7 cm/sup 2//V/spl middot/s, subthreshold slope of 0.76 V/decade, and an on/off ratio of 10/sup 8/.     

水性涂料VOC测定偏差对计算结果的影响

阐述水性涂料VOC的三项测定偏差对计算VOC结果的影响 ,指出国内现有标准的检测方法与国际标准方法存在的差距