热重分析对高分子材料中碳酸钙的定量研究

碳酸钙是高分子材料中常用的无机填料，在高温时会同二氧化碳而失重。利用热重分析可准确定出高分子材料中碳酸钙的含量，同时还可测出聚合物，挥发物的含量，热重分析法样品用量小，灵敏度高，所需时间短。     

玻璃两面重叠手印拍摄机理

根据斯涅尔定律和菲涅尔公式阐述清水衬底法消除玻璃下界面手印或玻纹的影像，以及用偏振光，紫外线拍摄玻面痕迹的方法和机理。     

基于遗传算法的水轮机最优工况参数计算

利用遗传算法计算水轮机的最优工况参数，给出遗传算法的具体实现步骤，并结合某电站的实际运行参数进行计算，结果表明，利用遗传算法计算水轮机的最优工况是可行的，而且寻优效率高，结果可靠。表2个。     

新型涂料增稠剂的化学成分鉴定

本文用红外光谱法对一种新型涂料增稠剂进行了化学成分鉴定,其主要成分为羟丙基甲基纤维素与蒙脱土。     

负载化非茂单活性中心催化剂乙烯聚合的研究

在硅胶上负载了双(N-环己基-3-叔丁基水杨醛亚胺基)二氯化锆配合物,得到负载化非茂单活性中心催化剂。该催化剂用于乙烯聚合,考察了配合物用量、共聚单体1-己烯用量、聚合温度、聚合压力、聚合时间、三乙基铝用量对乙烯聚合性能的影响及对聚合物的相对分子质量、相对分子质量分布、熔体流动指数和密度的影响。实验结果表明,负载化非茂单活性中心催化剂保持了原均相催化剂的乙烯聚合性能;该催化剂在淤浆聚合工艺中聚合平稳,所得聚合物的颗粒形态良好。     

对构建高校后勤危机管理体系的思考

本文根据高校后勤服务的特点，引出高校后勤危机和高校后勤危机管理的概念，并在进一步分析了高校后勤危机的诱因、主要特点、特殊性和构建高校后勤危机管理体系的必要性等基础上，提出了构建高校后勤危机管理体系所依据的理念、原则和三个阶段。     

Use of Fiber Bragg Grating Sensors for Determination of a Simply Supported Rectangular Plane Plate Deformation

A measurement method has been developed to determine the full-field deformation of a simply supported plane plate under transverse load. The method utilizes strain information provided by a set of four fiber Bragg grating sensors mounted on the plate in a way that all sensors measure strains along one certain direction. The sensors were interrogated using a wavelength swept fiber laser. Utilizing the strain information and the first four terms of Navier solution of simply supported rectangular plate, the necessary parameters for determining the deflection could be computed. By substituting the values of x- and -y- coordinates of each position on the rectangle plate, the full-field deformation information can be obtained. Single-point loading tests were experimentally performed to verify the accuracy of the method.     

Shape-Controlled Synthesis and Upconversion Luminescence of Y2O3:Yb, Er Microstructures

The Y2O3: Yb3 , Er3 microstructures were fabricated by a hydrothermal method without surfactants.The microstructures structure was characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM,KYKY 1000B).The up-conversion luminescence spectra were studied under 978 nm laser diode excitation.In Yb3 and Er3 codoped Y2 O3 microcrystals, the relative intensity of green emission became stronger as the morphology of sample changed from wires to films.     

High-yield synthesis of single-crystalline 3C-SiC nanowires by a facile autoclave route

Single-crystalline 3C-SiC nanowires have been synthesized in large scale through a one-step autoclave route by the reaction of SiCl₄, (C₅H₅)₂Fe and metallic Na at 500 °C. Electron microscopy investigations show that the nanowires have typical diameters of 15-50 nm, lengths up to several tens of micrometers and grow along the [111] direction. The possible growth mechanism of the nanowires is discussed.     

Squeeze-film effects in MEMS devices with perforated plates for small amplitude vibration

Squeeze-film effects of perforated plates for small amplitude vibration are analyzed through modified Reynolds equation (MRE). The analytical analysis reckons in most important influential factors: compressibility of the air, border effects, and the resistance caused by vertical air flow passing through perforated holes. It is found that consideration of air compressibility is necessary for high operating frequency and small ratio of the plate width to the attenuation length. The analytical results presented in this paper agree with ANSYS simulation results better than that under the air incompressibility assumption. The analytical analysis can be used to estimate the squeeze-film effects causing damping and stiffness added to the system. Since the value of Reynolds number involved in this paper is low (< 1), inertial effects are neglected.