Hot-Corrosion Resistance of a Sputtered K38G Nanocrystalline Coating in Molten Sulfate at 900°C

The hot-corrosion behavior of a nanocrystalline coating of K38G alloy, prepared by magnetron sputtering and cast K38G in molten 75 wt.% Na₂SO₄+25 wt.% K₂SO₄ at 900°C was studied. The coating eliminated internal sulfidation during the early stage of corrosion as a result of the formation of a continuous and compact Al₂O₃ scale. The nanocrystallization of K38G alloy prolonged the incubation of breakaway corrosion and improved the corrosion resistance of K38G. The relevant corrosion mechanism is discussed.     

Charge-discharge process of MnO2 supercapacitor

Mechanochemical synthesis of α-MnO2 was carried out with KMnO4 and Mn（CH3COO）2 in 1：1 mole ratio. The electrochemical performance of MnO2 electrode was investigated by cyclic voltammograms and alternating current impedance. The charge-discharge process of MnO2 supercapacitor in 6 mol/L KOH was studied within 1.2 V at 200 mA/g, suggesting that it displays double-layer capacibility in low potential scope and pseudo-capacitance properties in high potential scope. It is found that Mn3O4, an electrochemical inert, mainly forms in the initial 40 charge-discharge cycles. During cycling, the pseudo-capacitance properties disappear and the discharge curves are close to ideal ones, indicating double-layer capability. The maximum capacitance of MnO2 electrode is as high as 416 F/g, and retains 240 F/g after 200 cycles. The equivalent series resistance increases from 17 to 41Ω.     

熔体过热对Ag-Cu合金生长取向的影响

通过对Ag-Cu合金熔体的过热处理，研究了不同生长速率时的平界面的结晶位向，发现高的熔体温度使平面单晶的位向产生分支现象。应用Leonard-Jones势能和团簇概念分析了位向分支的形成原因，表明团簇状态在母相中的分布对结晶取向具有重要作用。     

机械合金化Al-Cu-Fe准晶相形成的研究进展

综述了机械合金化A1-Cu-Fe准晶相的形成机理及热力学稳定性方面的研究进展.     

一种新型振动下料机的PLC控制

在分析了新型振动下料机采用继电器－接触器控制方式存在不足的基础上，指出了对其进行PLC控制的必要性。分析了该振动下料机的基本构成及工作原理，建立了相应的液压系统。针对下料机正常工作对控制系统要求，确定了PLC的输入量及输出量，建立了PLC控制的硬件接线图，编制了相应的梯形图控制软件。大量实验验证了该控制方案的可行性和实用性。     

旋具杆部镀铬与头部发黑的复合处理

研制了旋具杆部镀铬与头部发黑的复合处理工艺。确定了镀层组合与发黑前酸洗用酸的种类,以及发黑端电镀时的保护方法;介绍了镀液、煮黑溶液的工艺参数,以及溶液的配制方法。工艺应用效果良好,并能满足工业上大批量生产要求。     

Microstructure and Application of YBCO Superconductive Films with Low Surface Resistance

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淬火态TC4合金热循环硬化行为及断口特征

在７７－６２３Ｋ对淬火态ＴＣ４合金进行了热循环试验，测定了合金热循环后的硬度，并与６２３Ｋ时效合金的硬度进行了对比；还观察了拉伸试样断口形貌。结果表明：热应力能加速亚稳相的分解，使合金中的位错密度升高，层错和形变孪晶的数量增多；循环温度场作用下淬火态合金拉伸试样断口由韧窝型断裂向韧窝和撕裂棱混合型断裂转变。     

Performance of positive and negative electrodes in amorphous manganese oxide supercapacitor

Using potassium permanganate and acetic manganese as the reactants, amorphous manganese oxide was prepared with mechanochemical method. XRD was used for microstructure characterization, while cyclic voltammetry and constant current charge-discharge were used for electrochemical performance testing. The positive electrode （PE） and negative electrode （NE） were investigated respectively in amorphous manganese oxide supercapacitor, aiming to find their different performances in charging-discharging. The results show that the crystalline structure is destroyed in both the PE and NE material during charge-discharge process. Thereinto, the NE suffers a bit more seriously. When cycling, the PE potential scope diminishes while the NE potential scope enlarges. The increased inner resistance makes the NE curves almost bended to be a right angle, but not the PE curves. The cell＇s equivalent series resistance （ESR） is more dependent on the NE, and the capacitance is mainly determined by the rapid descent of the NE potential range. The capacitances of the NE are highly rate-dependent, decreasing from 121.3 to 53.1 F/g, by 56.2%, over the range of 5-25 mV/s. However, the PE appears to be weakly dependent and its capacitance is only dropped by 22.1%.     

Structural optimization of Z-axis tuning-fork MEMS gyroscopes for enhancing reliability and resolution

Inertial sensors such as gyroscopes and accelerometers are normally considered as the most important sensors in a navigation system. Especially in the underwater or under-ice applications, the accuracy of the entire navigation system has to mainly rely on the precision of the inertial sensors due to inapplicability of global positioning systems. For MEMS-based inertial sensors, fabrication variation and environmental disturbance are among the major error sources. To address these challenges, in this paper we propose an optimization methodology by using parametric analysis on a reference design for improving sensor reliability and resolution. Apart from studying the resolution improvement by deploying an alternative sensing scheme, the effects of changing location, shape, and size of critical cantilevers have been thoroughly explored. By using this method, we have derived an improved mechanical structure for tuning-fork gyroscopes. Our numerical analyses show that the bandwidth of the proposed structure, which is the most important stability measure in the vibratory gyroscopes with slightly mismatched resonant frequencies, is over 1.7 times more immune to fabrication imperfection than the other structural alternatives. The drive and sense resonant amplitude robustness against fabrication imperfection is also improved in the proposed structure. In addition, this structure is able to provide at least 2.3 times larger sense-mode capacitance response to external rotation compared to the previously published designs. More important, it is observed that there is always non-negligible room for improving performance of gyroscopes if our proposed structural optimization methodology is integrated into the conventional MEMS-based inertial sensor design flow.