Preparation of branched polyacrylonitrile through self‐condensing vinyl copolymerization

Branched polyacrylonitrile (PAN) was prepared through a self‐condensing vinyl copolymerization of acrylonitrile and 2‐(2‐bromopropionyloxy)ethyl acrylate (BPEA). The branched architecture of the product was confirmed by NMR spectra and the average degree of branching (DB ) was estimated. Through a comparison of the intrinsic viscosity of the product with that of its linear analogue, the contraction factor g′ was calculated. It was found that the viscosity of the branched PAN was obviously lower that that of linear PAN. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008     

Green and self-lubricating polyoxymethylene composites filled with low-density polyethylene and rice husk flour

Polyoxymethylene (POM) composites filled with low-density polyethylene (LDPE) and rice husk flour (RHF) were prepared by injection molding. The POM/5 wt % LDPE/7.5 wt % RHF composite exhibited the lowest wear rate, whereas the coefficient of friction remained low, and the POM/5 wt % LDPE/5 wt % RHF composite had the best mechanical properties. X-ray diffraction analysis was carried out, and the worn surfaces were examined with scanning electron microscopy. The results showed that the addition of the filler reduced the crystallinity degree of the POM composites. The main wear mechanism for unfilled POM was adhesion, whereas for the POM composites, wear seemed to occur mainly by fatigue and abrasion. It was experimentally confirmed that the POM composite filled with LDPE and RHF, which is well-performing, low-cost, and environmentally friendly, could be a potential material for tribological applications. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008     

发展3G时不我待--兼析民族3G标准的发展

当今通信业最热门的话题非3G莫属。尽管2000年3G许可证的拍卖引发了欧洲乃至全球电信经济的萧条,但中国实行的“积极试验,谨慎决策”的政策,确保了电信业的快速增长。如2001年和2002年中国的电信业务收入分别增长了16.1%和14.4%,继续高于GDP的增长速度。今天,3G在国际市场上正步入良性发展轨道,中国移动通信市场也在向纵深发展,包括促进有效竞争、支持民族3G标准TD-SCDMA的发展和应用等。一、中国发展3G迫在眉睫1.用户需要3G中国市场对移动话音、移动新业务和新应用的需求潜力十分巨大。2002年底,中国移动通信的用户数(中国移动+中国…     

影响带锯机锯切质量的原因及处理措施

通过对锯切装置的改进，提高了锯切性能，降低了锯条成本，保证了锯切质量，使设备更加高效、安全的工作。     

真空蒸发沉积VOPc薄膜及磁场对薄膜结构与性能的影响

用真空蒸发制备了酞菁氧钒 (VOPc)薄膜 ,并在磁场中进行了热处理。用X光电子能谱、X射线衍射、紫外 可见吸收光谱、原子力显微镜等手段对制备的薄膜进行了表征。结果表明沉积的酞菁氧钒薄膜为α 型 ,成分接近酞菁氧钒的分子式。制备的薄膜在磁场中进行了热处理 ,发现磁场使酞菁氧钒薄膜性质发生改变 :UV VIS吸收谱Q带发生红移 ;XRD谱图衍射峰强度明显增强 ,峰位略有变化 ;原子力显微镜 (AFM)分析发现晶粒大小无明显变化。以上结果说明磁场的存在使得VOPc分子在热处理过程中发生了定向的排列     

一种网络服务自动部署方法

为满足网络服务使用者对网络服务部署的功能性和非功能性需求,运用Petri网的方法进行了互联网动态多变环境下的网络服务自动部署的研究,建立了一种基于Petri网的网络服务部署网模型,从形式化的角度描述了网络服务功能的部署情况,提出了一种按照服务质量来选择最优网络服务部署的算法。仿真的结果表明,与目前常用的固定部署算法和随机部署算法相比,按照该方法得到的网络服务部署能最好地满足服务使用者对服务的非功能性方面的需求。     

A Parallel Deadlock Detection Algorithm with O(1) Overall Run-time Complexity

This article proposes a novel parallel, hardware-oriented deadlock detection algorithm for multiprocessor system-on-chips. The proposed algorithm takes full advantage of hardware parallelism in computation and maintains information needed by deadlock detection through classifying all resource allocation events and performing class specific operations, which together make the overall run-time complexity of the new method O(1). We implement the proposed algorithm in Verilog HDL and demonstrate in the simulation that each algorithm invocation takes at most four clock cycles in hardware.     

A Newly Developed Non, Destructive Tritium Measurement Technique and Its Application to V-4Cr-4Ti Alloy

A non-destructive and in-situ technique for the measurement of tritium in materials, namely β-ray-induced X-ray spectrometry （BIXS）, has been developed recently. In the present study a V-4Cr-4Ti alloy was pre-heated at 1000℃ for 2 h to form a recrystallization structure before the tritium absorption experiments were conducted. Firstly the hydrogen isotope gas was charazterized by means of a quadrupole mass spectrometer （QMS） and a small-sized ionization chamber. Then hydrogen isotope absorption tests of V-4Cr-4Ti alloy were performed at 400 ℃ and the atomic concentration of hydrogen isotope in V-4Cr-4Ti alloy was estimated as 0.17% with a tritium content of approximately 2.5 ppm. Experimental results indicate that BIXS is a quite useful tool for quantitatively measuring the tritium content and tritium distribution in the surface layers of vanadium alloys and no strong trapping effects of tritium exist in the pre-heated V-4Cr-4Ti alloy.     

重庆温泉寺及其寺庙园林史略

本文以重庆温泉寺庙园林为例,说明现在重庆园林布局仍以寺庙建筑为中心,组成严整的东西对称格局,其建造充分体现了“天人合一”的思想境界和“道”的自然无为的原则。