ZrO_2（Y－TZP）－Si_3N_4复合材料中抑制ZrN生成研究

研究了气氛加压烧成ＺｒＯ２（Ｙ－ＴＺＰ）－Ｓｉ３Ｎ４复合材料中抑制ＺｒＮ生成工艺问题，相组成分析表明：无论添加２０ｗｔ％工业ＺｒＯ２或者Ｙ－ＴＺＰ（３ｍｏｌ％Ｙ。Ｏ。）的氯化硅复合材料，在低于１８５０℃，３ＭＰａｋ气压力下烧成，表面无ＺｒＮ生成．通过加入有效的烧结助剂（Ｙ。Ｏａ＋ＡＩ。Ｏｓ）、增加埋粉中ＳＩＯ分压以及增加保护气氛氮气压力，适当的烧成条件等工艺措施可有效地抑制ＺｒＮ的生成．实验还证实了ＺｒＮ很容易氧化，含有ＺｒＮ的ＺｒＯ。（Ｙ－ＴＺＰ）－ＳｉｓＮ。复合材料试样经９００℃，０．ｓｈ热处理已粉碎性裂开．     

Direct electroless Ni-P deposition on AM50 magnesium alloy from sulfate bath

A bright electroless Ni-P deposition on AM50 magnesium alloy in a sulfate plating bath was proposed by using direct plating process with non-chromate pretreatment. The electroless Ni-P plating on AM50 magnesium alloy has an admirable appearance and good adhesion. The results indicate that the electroless Ni-P deposition with non-chromate pretreatment has better adhesion than that of zinc immersion coating. Anodic polarization curves indicate that the electroless Ni-P deposition obtained from the sulfate bath has similar corrosion-resistance to that obtained from basic nickel carbonate bath. The deposition process generates less pollutant by a non-chromate plating bath and is suitable for the magnesium alloys manufacture because of its low cost. The hardness of the electroless Ni-P plated AM50 is about HV 720.6 and HV 969.7 after heat treatments at 180℃ for 2 h. The wear resistance of Ni-P plated magnesium alloy specimens is about 5 to 9 times as high as that of bare magnesium alloys.     

Φ3.3m/3m×60m回转窑轮带的挖补修复

我厂Φ3.3m/3m×60m回转窑为70年代产品,是出口增大变径窑,四档支撑。轮带设计尺寸有2种,宽×厚分别为700mm×250mm和500mm×250mm,材质为ZG55,中空箱式结构,见图1。图1轮带结构经过30余年的运转,高温带Ⅰ档700mm×250mm轮带表面出现了1块700mm×600mm的连片缺陷,深度达65mm。2002年9月8日,该缺陷处有1块面积300mm×200mm的碎片脱落,不能继续使用,我厂决定采用局部挖补的方法修复。具体步骤如下:1)详细检查缺陷部位,确定挖补的位置尺寸,再沿挖补位置向外量100mm划线,做为校对检查线。2)用16Mn钢板卷制1块弧度R1950mm、宽700mm,弧长1100mm…     

进一步增强整体开放意识开创我市对外开放工作的新局面

九十年代是中国社会主义现代化建设进程的关键时期。作者从宏观角度提出了青岛市如何进一步增强整体开放意识,开创对外开放工作的设想。对我市今后更好适应我国的经济振兴和社会进步意义重大。     

树木盆景的制作——（六）树木盆景造型的基本原则

以小见大,主次分明世上任何事物都不是单独存在的,而是有着千丝万缕的联系。大与小只是两者相比较而言,世上没有绝对大的事物,也没有绝对小的事物。没有大就显不出小,反之,没有小也就显不出大。以小见大,小是手段,不是目的;小是形式,大是内容,     

兴山煤矿地质构造体系的分析

通过简单的力学分析 ,总结了兴山煤矿断层发展、发育的规律。     

Fabrication of Ormocer Containing Eu3＋ Ion and Their Optical Spectra

Eu3 ions were incorporated in sol and gel by a sol-gel processing using 3-glycidoxypropyltrimethoxysilane(CH2OCHCH2O(CH2)3Si(OCH3)3, GPTMS) and ethyl silicate (TEOS) as precursors. The basic chemical-physical properties such as DTA curve, FF-IR spectra and specific surface area were recorded. The characteristics of their optical spectra were measured and investigated. The results indicate that the emission intensity of Eu3 ion in ormocer is much higher and the global line width is wider than those in SiO2 gel. The relationship between the composition and structure of gels and the fluorescence intensity and width were discussed. The obtained ormocer shows good mechanical strength, which can be cut and polished in machine without broken.     

电视画面前期色彩高速技巧

电视艺术是用光影和色彩进行造型的艺术形式.一部成功的影视作品,它的色彩或基调是在开机拍摄之前就已经确定的.但如何实现预想的效果呢?不外乎两种途径--前期摄像师的把握和后期剪辑师的加工.