A new efficient method for one‐pot conversions of aryl carboxylic acids into nitriles without solvent

A new efficient method for synthesising nitriles, important organic reagents, is reported in this paper. In an environmentally benign solvent‐free system, aryl carboxylic acids were converted into the corresponding nitriles via one‐pot reactions, by amidation with ethyl carbamate followed by dehydration with thionyl chloride, in excellent yields. The results showed that the method has the advantages of lower cost, higher yield, less pollution and greater ease of work‐up. Copyright © 2008 Society of Chemical Industry     

电视导引头模型参考控制器设计

借鉴模型参考控制器的设计思想,采用经过线性二次型输出反馈控制后的系统作为参考模型,以它的输出作为期望输出,让实际输出跟随这个期望输出;二者的误差信号反馈到原系统的输入端,设计出一种模型参考控制器.经该控制器优化后,电视导引头系统的快速性可得到较大提高.参考模型可由RC网络或计算机软件来实现.     

氨氮监测中样品蒸馏预处理对结果的影响分析

氨氮监测采用预蒸馏处理后，比色测定结果明显偏低。在样品预蒸馏处理过程中，硼酸作为吸收液，使显色时溶液pH值偏低，导致显色不充分是其主要影响因素。通过采取增加显色剂加入量的方法，解决了显色pH值偏低的问题，得到满意的测定结果。     

The new structure of fibre glass reinforced plastics bolt

The develop actuality and direction of FRP (fibre glass reinforced plastics) bolt in the world are analyzed. The new type structure of FRP bolt was designed. Trial data indicate that, all kinds of capability target of this FRP bolt all achieve and exceed the country stand-ard, substitute present metal bolt, wood bolt and bamboo bolt and other side bolt, it can gain magnitude technology and economy benefit. FRP bolt mechanization product line produce ef-ficiency is high, its throughput a day are 750 base, this can meet demand of hit-small mining company.     

企业不但应该做大更应该做强

从入世的角度 ,分析了我国企业在重组过程中存在的问题 ,并指出了我国企业做强做大的紧迫性     

用光谱仪检测材料元素时的注意事项

阐述了使用光谱仪检测材料时需注意的一些问题.     

电镀工艺条件变化对片状铁吸收剂吸波性能的影响

通过电镀法制备片状磁性吸收剂，用SEM、XRD等手段对其进行表征。用网络分析仪测试了不同工艺条件下吸收剂样品2～18GHz的电磁参数，并结合晶粒尺寸因素研究了不同工艺条件下对吸收剂电磁参数的影响．结果表明，不同的工艺条件对吸收剂电磁参数的影响具有规律性，可通过合理配置工艺参数来提高吸收剂的吸波性能。