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81.
采用熔融法结合放电等离子烧结(SPS)技术合成了P型填充方钴矿化合物Sr0.5Co4-xFexSb12,并研究了Fe掺杂对该化合物高温热电性能的影响。采用X.射线衍射(XRD)及电子探针(EPMA)表征了化合物的物相及化学成分,在300~850K温度范围内测试了化合物的电导率、赛贝克系数和热导率,采用Vande Pauw方法测试了化合物的室温载流子浓度。实验结果表明,化合物的主要相组成为Sr0.5Co4-xFexSb12方钴矿相,同时含有少量FeSb2和CoSb2杂质相。化合物的赛贝克系数均为正值,表明为空穴导电。随着Fe掺杂量的增加,化合物的载流子浓度及电导率增加,赛贝克系数降低,晶格热导率降低,最小室温晶格热导率为1.97 Wm^-1K^-2。对于化合物Sr0.5Co2.32Fe1.68Sb12在850K时获得的最大热电性能指数ZT约为0.60。 相似文献
82.
ZHANGWei LIJiuqing WUYinshun ZHANGPei HEJianping 《稀有金属(英文版)》2004,23(1):48-52
Cerium contained conversion films were deposited on LC4 aluminum alloy using square wave pulse (SWP) in aCeCl3 solution with KMnO4 as the oxidant. Energy dispersive spectroscopy (EDS) and scanning electron microscopy (SEM) were adopted to study the composition and the morphology of the film. It is found that the film is composed of Al, Zn, Cu,and small amount of cerium. The polarization curves of the specimens treated with SWP technique measured in 3.5% (mass fraction) NaCl solution reveal that the film thus formed inhibits both the anodic and cathodic process of the corrosion of the specimen. The immersion tests of treated specimens in 3.5% NaCl solution indicate that the corrosion resistance of the SWP treated specimen is better than that of the untreated and is equivalent to or even better than that of the traditionally electro-chemically treated specimens. 相似文献
83.
84.
高Co稀土热作模具钢析出相沉淀析出的研究 总被引:1,自引:0,他引:1
采用X射线衍射和透射电镜对新研制的高Co稀土热作模具钢的析出相及析出动力学进行了分析和探讨。结果表明 ,经过固溶和时效处理后合金中同时析出大量金属间化合物和碳化物。金属间化合物主要为 μ相和Laves相 ,碳化物主要为MC、M2 3 C6和M6C。在 70 0℃时效不同时间后 ,析出相的总量随时效时间的延长而不断增大 ,但 μ相增加的速度比较缓慢 ;M2 3 C6、M6C、Laves相增加较快 ;而MC逐渐减少。M2 3 C6、M6C是通过基体中的M和C原子的直接反应的形式析出长大的。 相似文献
85.
86.
Fuzzy adaptive networks in machining process modeling: surface roughness prediction for turning operations 总被引:6,自引:0,他引:6
Yue Jiao Shuting Lei Z. J. Pei E. S. Lee 《International Journal of Machine Tools and Manufacture》2004,44(15):1643-1651
Due to the complexity of the machine tool structure and the cutting process, the dynamics of machining processes are still not completely understood. This is especially true due to the demand of high-speed machining to increase productivity. In order to model and control these complex processes, new approaches, which can represent complex phenomenon combined with learning ability, are needed. The combined neural–fuzzy approach appears to be ideally suited for this purpose. In this paper, the recently developed fuzzy adaptive network (FAN) is used to model surface roughness in turning operations. The FAN network has both the learning ability of neural network and linguistic representation of complex, not well-understood, vague phenomenon. Furthermore, it can continuously improve the initially obtained rough model based on the daily operating data. To illustrate this approach, a model representing the influences of machining parameters on surface roughness is established and then the model is verified by the use of the results of pilot experiments. Finally, a comparison with the results based on statistical regression is provided. 相似文献
87.
高强度低合金结构钢焊缝与母材的强度匹配研究 总被引:3,自引:0,他引:3
焊缝金属与母材的强度匹配系数是焊接接头力学性能非均匀参数之一,匹配方式不仅取决于焊缝金属和母材的名义强度,还取决于它们的分布形式和特征参数。试验和统计计算结果表明,12Ni3CrMoV钢和10Ni5CrMoV钢母材和焊缝金属的抗拉强度都服从正态分布。12Ni3CrMoV钢和其焊缝金属的强度匹配属于低强匹配,其低强、等强和超强匹配的概率分别为59.33%,37.03%和3.64%,低强匹配特征明显。10Ni5CrMoV钢和其焊缝金属的强度匹配属于等强匹配,其低强、等强和超强匹配概率分别为47%,48%和5%,其等强匹配分布比较明显。对应的两种钢的焊接接头,其超强匹配概率分别为3.64%和5%,在结构、焊接材料、工艺设计中值得注意。由于强度匹配系数的随机性,如何确定强度匹配系数,在什么范围内分别属于超强、等强、低强匹配,特别是等强匹配的界定方式应有别于低强和超强匹配,都是有特研究的问题。 相似文献
88.
Two nano-composite coatings based on nc-TiC particles in an a-C:H matrix are deposited via closed-field unbalanced reactive magnetron sputtering. The compositions of the coatings are varied by changing the acetylene gas flow during the depositions. A Cr/Cr–Ti/Ti–TiC graded interlayer is introduced between substrate and coating. Electron probe micro-analyses (EPMA) show that the Ti content of the coatings varies between 31.7 and 11.5 at.%. The coatings exhibit a hardness (H) of 20.0 and 15.7 GPa, and a Young's modulus (E) of 229.4 and 136.6 GPa, respectively, as measured through nano-indentations. Cube corner indentations are performed to probe the fracture toughness of the coatings through the determination of critical indentation loads (Lr) at which radial cracks start to propagate. Transmission electron microscopy (TEM) observations and energy-filtered TEM are employed to characterize the coatings nanostructures. The variation in Ti content is accompanied by a variation in TiC particle size and volumetric fraction, as well as a change in the columnar structure of the coatings. A focus ion beam (FIB) slicing technique is employed to prepare samples from nano-indented locations of coated Silicon and stainless steel (SS) substrates. TEM inspection of the FIB sliced samples determines that the most brittle phase in the coating is the C-enriched columnar boundary, and identifies the location of failure within the interlayer. As a consequence of the different nanostructure, the coatings exhibit different elastic recovery properties and toughness. 相似文献
89.
D. Galvan V. Ocelík Y. Pei B. J. Kooi Jeff Th. M. De Hosson E. Ramous 《Journal of Materials Engineering and Performance》2004,13(4):406-412
TiB/Ti-6Al-4V metal-matrix composite (MMC) layers were produced on Ti-6Al-4V substrates by laser cladding. A TiB2/Ti powder mixture was used as a precursor to obtain a dispersion of TiB needles in the Ti alloy matrix, with the aid of an
exothermic reaction between TiB2 and Ti. A eutectic microstructure was obtained that consisted of an extremely homogeneous dispersion of TiB eutectic needles
in the Ti alloy matrix, having a volume fraction as high as 0.33. Also, an equilibrium-like microstructure was found, consisting
of a dispersion of both primary and eutectic TiB needles inside the Ti alloy matrix. An analysis of the geometry of the layers
was performed and proved successful in determining the percentage of B. Further, it correctly predicted the variation of atomic
B content as a function of laser power. The relative wear resistance coefficient, defined as the wear coefficient of the uncoated
matrix divided by that of coating, shows an improvement by a factor as high as 1500 for the eutectic microstructure.
This paper was presented at the 2nd International Surface Engineering Congress sponsored by ASM International, on September
15–17, 2003, in Indianapolis, Indiana, and appeared on pp. 411–18 of the Proceedings. 相似文献
90.
1 INTRODUCTIONMagnesiumchlorideisabasicmaterialforchem icalindustry ,andithaswideapplicationsinmetallur gy,architecturalmaterialandtextileindustry .Itisalsoamaterialforfire resistantproducts ,cryogenandcompoundfertilizerproductions[1] .Thefullydehy dratedmagnesiumchlorideisagoodmaterialforelec trolyticmetalmagnesium production .Becausemag nesiumchloridehasastrongadsorptiveability ,itisalsousedasadryingagent .Manysuccessfulworkshavebeendoneonthedehydrationofbischophite[2 10 ] .Butinfact,… 相似文献