Optomechanical scanning systems for microstereolithography (MSL): Analysis and experimental verification

Optomechanical scanning systems with focused laser spot are used in several applications including microstereolithography (MSL), scanning optical tweezers, and laser cutting. Systems used so far in the literature for scanning a focused laser spot on a substrate are: (a) galvanomirror preobjective scanning, (b) galvanomirror postobjective scanning and (c) ‘off-axis’ lens scanning system (originally proposed by coauthors). Major performance criteria due to end application, (say for example, to obtain high resolution microdevices in MSL) translates into the following criteria on optical scanning system: (i) uniform spot size and (ii) uniform intensity profile over the entire range of scan. This paper presents comparative optical analysis, both theoretical and experimental, of these systems based on the proposed performance criteria. Optical analysis of the optomechanical scanning systems is carried out by using geometric ray tracing method. Image evaluation in this case is done using diffraction wave optics. Simulations are carried out to determine spot characteristics at image plane when scan distances are changed by moving optics in the above mentioned optomechanical scanning systems. Simulation and experimental results clearly show that there is lesser distortion of spot characteristics (size and intensity profile) in case of proposed off-axis lens scanning system as compared to other systems over wider scan range. Hence this system is more promising to fabricate high resolution micro-components and in general for other similar applications as well.     

Ability of lymphokine-activated killer cells to lyse mycobacteria-infected cells

In cats and monkeys, we examined the parasympathetic component of the oculomotor complex, which directly innervates the ciliary muscle, using horseradish peroxidase (HRP). Labeled neurons of varying form and size were found in the Edinger-Westphal(EW) and the Perlia nuclei of the cat and in the anteromedian, EW, and Perlia nuclei of the monkey. Our study confirmed that a direct parasympathetic pathway exists from the midbrain to the ciliary muscles, and that accommodation is controlled in part by this direct link from the midsagittal region via a parasympathetic neuron of the oculomotor nuclear complex.     

Morphology,Ionic Conductivity,and Impedance Spectroscopy Studies of Graphene Oxide-Filled Polyvinylchloride Nanocomposites

Graphene oxide was synthesized using modified Hummers method. The preparation of polyvinylchloride/graphene oxide nanocomposites was carried out using colloidal processing. The morphology of polyvinylchloride/graphene oxide nanocomposite confirms that graphene oxide was uniformly distributed within the polyvinylchloride matrix indicating complete exfoliation of graphene oxide. Significant improvement in the microhardness of the nanocomposite was observed as compared to neat polyvinylchloride. The impedance spectroscopy of nanocomposites was carried out in the frequency range (50 Hz to 35 MHz) and temperature range (80–150°C). Thus, based on the results obtained, we found that polyvinylchloride/graphene oxide nanocomposites hold great promise in many potential applications such as an electrode material for supercapacitors.     

Influence of Varying SiO2?% on the Mechanical Properties of Al Based MMC

The current investigation is focused on effective utilization of rice husk ash (RHA) SiO₂??an industrial waste available in abundance, by systematically dispersing into an Al?CMg (0.5, 1.0, 2.5, and 5.0?% by weight) matrix resulting in synthesis of composites via Liquid Metallurgy route. The effect of increasing Mg?% to improve the wettability with the increase in SiO₂?% as reinforcement was studied comparatively. The increase in the percentage of SiO₂ beyond 5?% as reinforcement into Al?CMg alloy increases the agglomeration of SiO₂ particles which creates more sites for crack initiation and hence lowers down the load bearing capacity of the composite while microhardenss and wear testing analysis. For the composite, Al?CMg (2.5?%)?CSiO₂ (5.0?%) the hardness was observed to be maximum corresponding to minimum wear loss. The uniform distribution of maximum amount of hard spinel structure of extremely small size within the matrix confirms maximum wetting characteristic of 2.5 wt% Mg.     

Differential expression of acidic and basic fibroblast growth factors in benign prostatic hyperplasia identified by immunohistochemistry

OBJECTIVES: Transitional cell carcinomas of upper urinary tract (uttTCC) constitute 5% to 6% of all urothelial tumors. Ureteropyeloscopy has become the standard for clinical evaluation of uutTCC. Moreover, endoscopic treatments have been advocated as a conservative approach for low grade tumors or patients with intermediate grade tumors whose renal function is compromised. Therefore, grading has become the most predictive variable in defining therapeutic approach. In addition to morphologic evaluation, a series of biologic markers may be used to increase the accuracy of grading such as DNA analysis and p53 protein expression. In this study, we have evaluated these markers by means of cell image analysis with the SAMBA 400 system. METHODS: Thirteen cases of uttTCC were studied with cytologic smear, cell block, and histologic confirmation. DNA analysis was performed on cytologic smear. Immunostaining was performed on cell blocks. A grade was assigned on the basis of DNA evaluation and p53 expression quantitation. These grades were combined for each case and compared with the initial cytologic grading and the final histologic grading. RESULTS: Cytology alone diagnosed TCC in all but 1 case that was diagnosed atypical. Discrepancies were found in primary grading: cytologic grading concurred with histologic grading in 6 of the 13 cases. CONCLUSIONS: These results, although in a limited but selected number of cases, show the potential of computerized evaluation of biologic markers as parameters for a more objective grading of tumors.     

Electrochromic performance of mixed V2O5–MoO3 thin films synthesized by pulsed spray pyrolysis technique

Mixed V₂O₅–MoO₃ thin films were deposited onto the glass and fluorine doped tin oxide (FTO) coated glass substrates, at 400 °C by pulsed spray pyrolysis technique (PSPT). Equimolar vanadium chloride (VCl₃) and ammonium molybdate aqueous solutions were mixed together in volume proportions (5–15% molybdenum) and used as a precursor solution for the deposition of mixed V₂O₅–MoO₃ thin films. The structural, morphological, optical and electrochromic properties of the films deposited at different Mo concentrations were studied. With increase in the percentage of Mo the peaks belonging to tetragonal phase of V₂O₅ eventually disappear and the (1 0 1) orthorhombic V₂O₅ phase is observed. Scanning electron microscopy (SEM) shows micro thread like reticulated morphology. The optical band gap energy varied over 2.91–2.85 eV. All the films exhibited cathodic electrochromism in lithium containing electrolyte (0.5 M LiClO₄ + propylene carbonate (PC)). The highest coloration efficiency (CE) for the V₂O₅ film with 15% MoO₃ mixing was found 35.27 cm² C⁻¹.     

Effect of Ga doping on micro/structural, electrical and optical properties of pulsed laser deposited ZnO thin films

Undoped and Ga doped ZnO thin films (1% GZO, 3% GZO and 5% GZO) were grown on c-Al₂O₃ substrates using the 1, 3 and 5 at. wt.% Ga doped ZnO targets by pulsed laser deposition. X-ray diffraction studies revealed that highly c-axis oriented, single phase, undoped and Ga doped ZnO thin films with wurtzite structure were deposited. Micro-Raman scattering analysis showed that Ga doping introduces defects in the host lattice. The E₂^High mode of ZnO in Ga doped ZnO thin film was observed to shift to higher wavenumber indicating the presence of residual compressive stress. Appearance of the normally Raman inactive B₁ modes (B₁^Low, 2B₁^Low and B₁^High) due to breaking of local translational symmetry, also indicated that defects were introduced into the host lattice due to Ga incorporation. Band gap of the Ga doped ZnO thin films was observed to shift to higher energy with the increase in doping concentration and is explicated by the Burstein-Moss effect. Electrical resistivity measurements of the undoped and GZO thin films in the temperature range 50 to 300 K revealed the metal to semiconductor transition for 3 and 5% GZO thin films.