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51.
Birgit Kanngießer Andreas-Germanos Karydas Dimosthenis Sokaras Stefan Röhrs Joseph Salomon 《Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms》2007,264(2):383-388
The paper describes a novel experiment characterized by the development of a confocal geometry in an external Micro-PIXE set-up. The position of X-ray optics in front of the X-ray detector and its proper alignment with respect to the proton micro-beam focus provided the possibility of carrying out 3D Micro-PIXE analysis. As a first application, depth intensity profiles of the major elements that compose the patina layer of a quaternary bronze alloy were measured. A simulation approach of the 3D Micro-PIXE data deduced elemental concentration profiles in rather good agreement with corresponding results obtained by electron probe micro-analysis from a cross-sectioned patina sample. With its non-destructive and depth-resolving properties, as well as its feasibility in atmospheric pressure, 3D Micro-PIXE seems especially suited for investigations in the field of cultural heritage. 相似文献
52.
John S. Wright Joseph M. Schwartz Lanny D. Schmidt Lorraine Falter Francis 《Journal of the American Ceramic Society》1995,78(9):2360-2366
The crystalline phase development and microstructural changes with heating of sol-gel-derived lead titanate (PT) particles and films on silica with and without a fugitive (or removable) diffusion barrier layer were investigated. Amorphous gel-derived PT particles were deposited on SiO2 -coated TEM grids with and without polyimide (PI) or carbon barrier layers between SiO2 and PT. TEM analysis showed that PI or carbon barriers prevented reaction between the gel-derived PT particles and SiO2 . PT particles crystallize and then the PI or carbon film decomposes. Sol-gel-derived PT films were deposited on oxidized Si substrates (Si/SiO2 ) with and without a PI barrier layer. Perovskite PT films were prepared on Si/SiO2 substrates with a PI barrier; however, some porosity remained in the films. Identically prepared films without the PI barrier formed a mixture of pyrochlore and perovskite. X-ray photoelectron spectroscopy results indicate that the PI film pre- vents the diffusion of Si into the PT film. 相似文献
53.
This study investigated the effectiveness of different types of on-line feedback following user errors for informing users of the information and functions available in a system with a natural language interface. Twenty-four individuals performed a task based on an industry cost savings program, in which they were given general goals to pursue with regard to the task. Three feedback levels which differed according to the type and amount of feedback provided, along with two levels of system complexity, were examined. In addition, subjects performed the task again after one week to determine the effects of feedback on retention. Results indicated that the subjects in the second level of feedback generally performed better with respect to accessing system functions and information than those in the first level. Although there was some performance improvement from the second to third level, it was not significant. However, the third level of feedback did significantly improve the efficiency with which subjects used information to complete the task during the return condition. Overall, feedback did not affect the errors made, though at certain more limited stages of the tasks this effect was observed. 相似文献
54.
Joseph Leu 《软件工程师》2006,(4):55-57
Silicon Valley is hom e to the m ostdynam ic industries in the C aliforniaeconom y .These industries —— thehigh-tech sector—— are driven by in-novation,and each new wave of inno-vation is usually led by cre ativeentrepreneurs starting new firm s.D uri… 相似文献
55.
Joseph J. Niemela 《Journal of Low Temperature Physics》1997,109(5-6):709-732
Liquid Helium II drops, of diameter 1 mm or less, are charged with positive helium ions and subsequently levitated by static
electric fields. Stable levitation was achieved for drops of order 100–150 micrometers in diameter. The suspended drops could
be translated to arbitrary positions within the levitator using additional superimposed DC electric fields, and also could
be made to oscillate stably about their average positions by means of an applied time-varying electric field. A weak corona
discharge was used to produce the necessary ions for levitation. A novel superfluid film flow device, developed for the controlled
deployment of large charged drops, is described. Also discussed is an adjustable electric fountain that requires only a field
emission tip operating at modest potentials, and works in both Helium I and Helium II. 相似文献
56.
57.
AG Heriot D Kumar V Thomas M Young J Pilcher AE Joseph 《Canadian Metallurgical Quarterly》1998,85(12):1713-1715
BACKGROUND: The use of fine-needle aspiration cytology (FNAC) in the diagnosis of colonic lesions was investigated. METHODS: Some 22 patients (median age 71 years) with a colonic lesion identified on abdominal ultrasonography underwent ultrasonographically-guided FNAC using a 21-G needle. The sample was checked immediately by a cytopathologist for adequacy. RESULTS: Eighteen patients had colonic carcinoma; aspiration cytology detected malignant epithelial cells consistent with colonic carcinoma in 17 patients and severely dysplastic cells in one patient. The sensitivity and specificity of ultrasonographically-guided FNAC in the diagnosis of colonic carcinoma was 94 and 100 per cent respectively. The remaining four patients had a diagnosis of ileocaecal tuberculosis, ileocaecal Crohn's disease, and metastatic adenocarcinoma in the liver with no identifiable primary (two patients). One demonstrated granulomata, grew acid-fast bacilli and the patient was treated for tuberculosis. One had inflammatory cells and the patient was found to have Crohn's disease on histology. The remaining two patients had confirmed metastatic adenocarcinoma in the liver on aspiration cytology but suspected colonic lesions were found to be benign on cytological examination and no primary lesion was subsequently demonstrated. There were no complications of FNAC and patients complained of minimal discomfort. There has been no evidence of tumour recurrence with a median follow-up of 12 (range 1-25) months. CONCLUSION: Ultrasonographically-guided FNAC is a valid method for the diagnosis of colonic tumours. 相似文献
58.
Lavine Howard; Huff Joseph W.; Wagner Stephen H.; Sweeney Donna 《Canadian Metallurgical Quarterly》1998,75(2):359
In 3 experiments, the authors assessed whether attitude strength moderates the susceptibility of attitudes to item context effects in surveys. In Experiment 1, respondents completed multiple measures of attitude strength. Three weeks later, respondents participated in a context experiment. Results revealed that respondents with weak attitudes exhibited significantly larger context effect for 1 of 2 issues. In Experiment 2, the results of Experiment 1 were conceptually replicated by use of measures of interattitudinal embeddedness to assess attitude strength. In Experiment 3, significant strength-moderated context effects were found when attitude strength was assessed in a multi-item, multidimensional manner but not when it was assessed with a single item. Discussion focuses on measurement and theoretical issues related to the moderation and mediation of context effects in attitude surveys. (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
59.
Emma P. Bullock Allison L. Roxburgh Patricia S. Moyer-Packenham Elif Bektas Joseph S. Webster Kathleen A. Bullock 《Journal of Computer Assisted Learning》2021,37(2):557-586
This study focused on an examination of how type, quality and children's awareness of design features in digital math games, along with an awareness of the mathematics goals of the game, were related to learning outcomes. We conducted a parallel conversion mixed methods study with 45 students in Grades 3 and 4 (ages 9–10). Students participated in clinical interviews using three digital math games. The results suggest a moderated mediation relationship in which the quality of the design features moderated the mediating impact of children's awareness of the game's design features, specifically when the child was aware of the mathematics content learning goal (MCLG) of the game. These findings show how important it is that design features are of high quality in a digital math game, and how this is intertwined with children's awareness of the features and the MCLG. When these variables intertwined in just the right way, the interactions between the children and the digital math game afforded mathematical learning growth. 相似文献
60.
Joseph H. Magill 《Journal of Inorganic and Organometallic Polymers》1992,2(2):213-229
Variations in thermotropic behavior have been investigated for many crystalline polyphosphazenes. Experimental results obtained from DSC, solid-state MAS NMR, dilatometry, mechanical property (creep and dynamic) measurements, birefringence, X-ray (wide and small-angle), and electron diffraction have been made as a function of temperature in an attempt to elucidate the structure-morphology behavior in these polymers. Initially all polyphosphazenes described in this study crystallize from dilute or moderately concentrated solutions in the monoclinic form with relatively low crystallinity (50%). When heated, these specimens expand atT(1) and adopt a chain-extended 2D mesophase morphology in order to relieve congestion. Above this first-orderT(1) temperature a chain-extended –P=N– chain backbone morphology transforms into an isotropic phase at the melting temperatureT
m. When cooled, samples transform into the mesostate. However, crystallization from the mesophase belowT(1) takes place into a 3D orthorhombic state. These two modes of ordering/disordering are in accordance with (i) a hexatic chain packing [betweenT(1) andT
m] with variously mobile side groups that also exhibits smectic features when mesogenic side groups are present and (ii) a 3D orthorhombic structure of high crystallinity belowT(1). The initial monoclinic phase is accessible only via a solution crystallization route. Solid-state MAS NMR, crystallization kinetic measurements, and optical microscopy studies obtained from oriented and unoriented polymers have been especially germane in providing a unifying picture for mesophase formation and ordering in polyoxyphosphazenes. X-ray and electron diffraction evidence is complicated by critical overlapping peaks that are found under these same conditions. They demonstrate that (a) positional disorder exists along the chain direction and (b) the side chain above, as well as below, theT(1) transition is governed by the mobility, size, and type of side group in circumstances where phase transformations occur. 相似文献