Growth of Ag nanocrystals on multiwalled carbon nanotubes and Ag-carbon nanotube interaction

The experimental investigations on the interaction between Ag-nanocrystal particles (Ag-NCPs) and carbon nanotubes (CNTs) in Ag-nanocrystal particles/carbon nanotubes (Ag-NCPs/CNTs) hybrid structures were reported. The growth of Ag-NCPs on multiwalled carbon nanotubes (MWCNTs) was carried out by thermal evaporation deposition. High-resolution transmission electron microscopy and X-ray diffraction analyses revealed that Ag-NCPs had the crystal lattice feature of face-centered cube (fcc). The growth of Ag-NCPs on MWCNTs induced the cross-section deformation of MWCNT. The experimental results also showed that the synthesized Ag-NCPs/CNTs hybrid structure appeared as quasi-one dimensional nanowires containing the Ag-NCP/CNT hetero-junction. There was local cross-section deformation on MWCNTs at the interface of hetero-junction. These results involve the important topic about fundamental and practical studies for structure of MNCPs on CNTs and also find clues to further research of Ag nanocrystal growing on MWCNTs and related Ag-CNT interaction.     

Composite silicone rubber of high piezoresistance repeatability filled with nanoparticles

The ruthenium oxide nanoparticles with size less than 20 nm were fabricated by annealing the metallic ruthenium nanoparticles in air, which were synthesized by using the thermal reduction in the polyol solution. The rutile structure of the ruthenium oxide was proved by using transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS). The oxide has good electron conductivity. The surface of the ruthenium oxide was modified by a vinyl silane coupling agent. The assembling of the silane to the oxide surface was proved by Infrared (IR) absorption spectroscopy. By mixing the nanoparticles with poly(methylvinylsiloxane) (PMVS) silicone rubber, a composite filled with dispersive conducting phase was fabricated. The temperature dependent conductivity shows that the electron transportation through composite is mainly dominated by tunneling. The measurement of piezoresistance shows that the composite at low strain has high piezoresistance repeatability. The 3D reconstruction images of the composite filled with carbon black or ruthenium oxide show that the aggregation of the nanoparticles differs much for two composites. The narrow distribution range of the particle size was thought to be the main factor for the high piezoresistance recurrence.     

基于集对论的医疗卫生财政支出绩效评价

以集对论为基础,依据财政部预算司提出的医疗卫生财政支出绩效评价指标和绩效评价等级级别,对绩效等级评价值进行同一性、差异性和对立性分析,建立了集对评价分析模型.以联系度最大为准则,获得绩效评价等级级别,实例研究结果表明了该评价方法的有效性.     

区域对接的多目标决策模型研究

在系统目标分析的基础上,提出了系统的模型体系结构,确定了区域对接模型的目标、决策变量,及约束条件;根据模型要达到的不同日标,分别建立了3种发展方案.该模型可较好地反映局部与整体协调发展的制衡关系,为区域对接的定量研究提供了基础.     

基于 ISAPI 过滤器的 Web 防护系统

随着 Internet 的发展,恶意用户利用 Web 应用程序存在的漏洞,对 Web 站点实施攻击,从而完成获取信息资料、植入病毒木马、伪装钓鱼网站、恶意插入广告等恶意操作,危害用户的利益,降低网站的可信度。随着 Web 攻击的日益增长,网站的安全风险达到了前所未有的高度。针对 Web 站点安全问题,在 HTTP 协议模型的基础上,结合 URL 解析技术及 Web 服务器核心扩展技术,文章设计并实现了一个基于 ISAPI 过滤器的 Web 防火墙系统。该系统可抵御常见网络攻击行为,为基于 HTTP 协议的 IIS 网站提供安全保障。系统主要包括3个组成部分：配置模块、过滤模块及日志模块。文章对系统过滤模块的设计与实现进行了详尽的阐述,系统的主要功能包括：过滤 HTTP 请求类型、限制头部长度、禁止 SQL 注入、禁止 Cookie 注入、禁止跨站攻击、防止敏感目录扫描、过滤请求文件类型以及 IP 黑名单。系统通过上述功能可以有效检测 Web 攻击行为并能做出正确处理,为 Web 网站安全提供有效保障。文章最后对系统进行功能测试,测试表明,系统可以对常见的 Web 攻击行为进行过滤处理并做出预期响应。系统符合设计目标,具有较高的实用价值。     

压电陶瓷在声速测量中的应用

本文论述了压电陶瓷在声速测量中的应用,阐述了几种测量超声波波速的方法。     

Computational fluid dynamics (CFD) modeling of spouted bed: Influence of frictional stress, maximum packing limit and coefficient of restitution of particles

Following the previous article [Du, W., Bao, X., Xu, J., Wei, W., 2006. Computational fluid dynamics (CFD) modeling of spouted bed: assessment of drag coefficient correlations. Chemical Engineering Science 61 (5), 1401-1420], this contribution describes the influences of the frictional stress, maximum packing limit and coefficient of restitution of particles on CFD simulation of spouted beds. Using the two-fluid method embedded in the commercial CFD simulation package Fluent 6.1, the spouting hydrodynamics of a cylindrical-conical spouted bed was simulated and verified with the experimental data of He et al. [He, Y.L., Lim, C.J., Grace, J.R., Zhu, J.X., Qin, S.Z., 1994a. Measurements of voidage profiles in spouted beds. Canadian Journal of Chemical Engineering 72 (4), 229-234; He, Y.L., Qin, S.Z., Lim, C.J., Grace, J.R., 1994b. Particle velocity profiles and solid flow patterns in spouted beds. Canadian Journal of Chemical Engineering 72(8), 561-568]. The results showed that, for coarse particles, the frictional stress is important only for the annulus computation and has no obvious effects on the hydrodynamics of the solids flow in the spout region. The specification of the maximum packing limit could significantly affect the properties of the pseudo-fluid phase of the particles by changing the radial distribution function. The strong dependence of the pseudo-fluid properties of the particle phase, such as pressure, bulk viscosity and shear viscosity, on the granular temperature accounts for the influence of the coefficient of restitution of particles on CFD modeling. The solids volume fraction at loose packing state is suitable for spouted bed simulations, and a pretest of the coefficient of restitution of particles must be conducted when no experimental datum is available.     

基于有色Petri网的1553B总线建模及分析

针对1553B总线的实时性评估问题,提出一种基于有色Petri网(Colored Petri Net,CPN)的1553B总线模型;该模型基于分层建模的思想,分别建立了1553B总线的拓扑模型、总线控制器模型、远程终端模型和总线信道模型,有效刻画了1553B总线的拓扑结构和动态行为;仿真实验验证了所建模型的正确性和有效性,该模型可为构建满足特定实时性要求的1553B总线系统提供理论依据。     

化纤精纺陶瓷磨擦盘的研制

本文在Mgo—Al_2O_3—SiO_2三元系高铝瓷配方的基础上,选用高纯活性α—Al_2O_3粉料,将MgO 等复合添加剂按一定成份和比例加入配料中以促进烧结,并改善材料的显微结构。采用一次造粒的干压成型工艺,在高温隧道窑中连续烧成,获得了批量产品性能一致的细晶陶瓷磨擦盘制品。     

膨胀石墨在聚乙烯中阻燃协效作用的研究

以膨胀石墨(EG)与聚磷酸铵(APP)复配组成膨胀型阻燃剂，应用于高密度聚乙烯(PE-HD)中。热分析表明APP／FG的添加使得PE-HD材料的热稳定性增强，降解过程变缓，剩炭率增加。氧指数(LOI)结果表明APP／EG具有良好的阻燃协同作用。扫描电镜(SEM)显示APP／EG的加入可使得PE-HD样品生成连续致密的炭层。同时力学性能研究表明APP／EG对材料的力学性能的影响比其它膨胀型阻燃剂要小。