Friction on a single MoS2 nanotube

Friction was measured on a single molybdenum disulfide (MoS₂) nanotube and on a single MoS₂ nano-onion for the first time. We used atomic force microscopy (AFM) operating in ultra-high vacuum at room temperature. The average coefficient of friction between the AFM tip and MoS₂ nanotubes was found considerably below the corresponding values obtained from an air-cleaved MoS₂ single crystal or graphite. We revealed a nontrivial dependency of friction on interaction strength between the nanotube and the underlying substrate. Friction on detached or weakly supported nanotubes by the substrate was several times smaller (0.023 ± 0.005) than that on well-supported nanotubes (0.08 ± 0.02). We propose an explanation of a quarter of a century old phenomena of higher friction found for intracrystalline (0.06) than for intercrystalline slip (0.025) in MoS₂. Friction test on a single MoS₂ nano-onion revealed a combined gliding-rolling process.PACS, 62.20, 61.46.Fg, 68.37 Ps     

Influence of Field Effects on the Performance of InGaAs-Based Terahertz Radiation Detectors

A detailed electrical characterization of high-performance bow-tie InGaAs-based terahertz detectors is presented along with simulation results. The local surface potential and tunnelling current were scanned over the surfaces of the detectors by means of Kelvin probe force microscopy (KPFM) and scanning tunnelling microscopy (STM), which also enabled the determination of the Fermi level. Current-voltage curves were measured and modelled using the Synopsys Sentaurus TCAD package to gain deeper insight into the processes involved in detector operation. In addition, we performed finite-difference time-domain (FDTD) simulations to reveal features related to changes in the electric field due to the metal detector contacts. The investigation revealed that field-effect-induced conductivity modulation is a possible mechanism contributing to the high sensitivity of the studied detectors.     

Stereometric analysis of nanostructured boehmite coatings synthesized by aluminum nitride powder hydrolysis

We studied the morphological properties of precipitated, nanostructured, boehmite coatings on a polished alumina surface by exploiting the aluminum nitride (AlN) powder hydrolysis at elevated temperatures. The hydrolysis tests of the 3 wt% AlN powder suspensions in the temperature range 50–90 °C were performed in order to estimate the time needed for the synthesis of the coatings. They consisted of interlocked boehmite lamellas, positioned perpendicularly to the ceramic surface, and they exhibited a strong temperature-dependent size and surface density. The aim of this research was a quantitative assessment of the as-formed boehmite coatings. Based on electron microscopy micrographs, a stereometric analysis of the as-prepared coatings was performed in order to estimate the relevant geometric parameters of the lamellas. In spite of the temperature-dependent lamellas’ size and surface density, the specific volume of the coatings was similar for all the synthesis temperatures.     

Discrete (n + 1)-valued states and n-perfect pseudo-effect algebras

We give sufficient and necessary conditions to guarantee that a pseudo-effect algebra admits an (n + 1)-valued discrete state. We introduce n-perfect pseudo-effect algebras as algebras which can be split into n + 1 comparable slices. We prove that the category of strong n-perfect pseudo-effect algebras is categorically equivalent to the category of torsion-free directed partially ordered groups of a special type.     

Signal shaper with a distributed delay: Spectral analysis and design

Input shapers with time delays have proved useful in many applications related to controls for various oscillatory devices, for example flexible manipulators and cranes. In the paper, a novel approach for designing a zero-vibration signal shaper based on equally distributed delay is proposed. The parameter assessment of the shaper is based on the spectral approach. Various characteristics of the shaper are analyzed and compared with the classical zero-vibration shaper with a lumped delay. The analysis shows that the novel shaper is a slower, but more robust alternative to the classical shaper. Besides, the discrete implementation of the shaper is proposed and tested. It includes zero placement based parameter adjustment with the objective to preserve full compensation of the oscillatory mode by the discrete algorithm.     

Analyzing probabilistic pushdown automata

The paper gives a summary of the existing results about algorithmic analysis of probabilistic pushdown automata and their subclasses.     

Validation of a Method for Analysis of Aroma Compounds in Red Wine using Liquid–Liquid Extraction and GC–MS

An analytical method for determination of volatile composition of wines using sample preparation by liquid–liquid extraction and gas chromatography coupled to mass spectrometry for separation and detection has been developed and validated. Extraction of volatile compounds was performed in dichloromethane, and 1-octanol was added as an internal standard. Kékfrankos red wine produced in Villány wine region in Hungary was used as a model wine for testing and validation of the method. The developed method allowed satisfactory determination of 33 volatile compounds in the wines. Compounds analyzed include alcohols, esters, lactones, fatty acids, furans, and nitrogen compounds. The calibration curves of the four reference compounds used (2-phenyl ethanol, ethyl nonanoate, butyrolactone, and tyrosol) were linear in all cases with correlation coefficients (R ²) ranging from 0.9951 to 0.9992. The accuracy of the method was checked with a standard addition method (recovery 92.2–103 %), showing good repeatability and reproducibility (RSD?<?10 %).