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31.
Boehmite occurs in the form of nanoparticles. Upon drying, it can form the alumina that is common in catalyst support used in refining and petrochemicals. The topotactic transformation of boehmite alumina led to an interest in the precise shape and size of these nanoparticles which is highly linked to the catalyst activity. Boehmite nanoparticles can be observed by transmission electron microscopy. Although they are highly aggregated, the analysis of transmission electron microscopy images with a specific random model approach, here a dilution model, can give an accurate estimate of their size. To use this approach, electronic noise and diffraction artefacts on the edges of the nanoparticles have to be removed. Covariance measurements on micrographs can be performed. They can be used to fit a model. The fitting uses a novel numerical method to estimate the covariogram of grains. The model can take into account the specific orientations of the nanoparticles. The influence of noise, image filters used to remove noise and diffraction artefacts, as well as all the parameters of the model are all studied in this paper. We propose nanoparticle size estimations procedures based on both single and mixture-of-two particle models. 相似文献
32.
Raymond Rosenbloom Igor Gavrish Anna E. Tseng Kerstin Seidel Shivraj M. Yabaji Hans P. Gertje Bertrand R. Huber Igor Kramnik Nicholas A. Crossland 《International journal of molecular sciences》2022,23(11)
Pulmonary infections caused by the group of nontuberculosis mycobacteria (NTM), Mycobacterium avium complex (MAC), are a growing public health concern with incidence and mortality steadily increasing globally. Granulomatous inflammation is the hallmark of MAC lung infection, yet reliable correlates of disease progression, susceptibility, and resolution are poorly defined. Unlike widely used inbred mouse strains, mice that carry the mutant allele at the genetic locus sst1 develop human-like pulmonary tuberculosis featuring well-organized caseating granulomas. We characterized pulmonary temporospatial outcomes of intranasal and left intrabronchial M. avium spp. hominissuis (M.av) induced pneumonia in B6.Sst1S mice, which carries the sst1 mutant allele. We utilized traditional semi-quantitative histomorphological evaluation, in combination with fluorescent multiplex immunohistochemistry (fmIHC), whole slide imaging, and quantitative digital image analysis. Followingintrabronchiolar infection with the laboratory M.av strain 101, the B6.Sst1S pulmonary lesions progressed 12–16 weeks post infection (wpi), with plateauing and/or resolving disease by 21 wpi. Caseating granulomas were not observed during the study. Disease progression from 12–16 wpi was associated with increased acid-fast bacilli, area of secondary granulomatous pneumonia lesions, and Arg1+ and double positive iNOS+/Arg1+ macrophages. Compared to B6 WT, at 16 wpi, B6.Sst1S lungs exhibited an increased area of acid-fast bacilli, larger secondary lesions with greater Arg1+ and double positive iNOS+/Arg1+ macrophages, and reduced T cell density. This morphomolecular analysis of histologic correlates of disease progression in B6.Sst1S could serve as a platform for assessment of medical countermeasures against NTM infection. 相似文献
33.
Bertrand Bouriquet Jean-Philippe ArgaudRomain Cugnart 《Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment》2012,664(1):117-126
An optimal reconstruction of the neutronic activity field can be determined for a nuclear reactor core using a data assimilation framework to merge information from models and measurements. In this paper, we focus on solving the inverse problem of determining an optimal repartition of the measuring instruments within the core, to get the best possible results from the data assimilation reconstruction procedure. The position optimisation is realised using a Simulated Annealing algorithm, based on the Metropolis-Hastings proposition. Moreover, algebraic improvements of data assimilation have been developed, optimising their computational performance, and are presented here. 相似文献
34.
Martti Heinonen Miltiadis Anagnostou Stephanie Bell Mark Stevens Robert Benyon Reidun Anita Bergerud Jovan Bojkovski Rien Bosma Jan Nielsen Norbert B?se Plunkett Cromwell Aliye Kartal Dogan Seda Aytekin Ali Uytun Vito Fernicola Krzysztof Flakiewicz Bertrand Blanquart Domen Hudoklin Per Jacobson Anders Kentved Isabel Lóio George Mamontov Alexandra Masarykova Helmut Mitter Regina Mnguni Jan Otych Anton Steiner Nagyné Szilágyi Zsófia Davor Zvizdic 《International Journal of Thermophysics》2012,33(8-9):1422-1437
In the field of humidity quantities, the first CIPM key comparison, CCT-K6 is at its end. The corresponding European regional key comparison, EUROMET.T-K6, was completed in early 2008, about 4?years after the starting initial measurements in the project. In total, 24 NMIs from different countries took part in the comparison. This number includes 22 EURAMET countries, and Russia and South Africa. The comparison covered the dew-point temperature range from ?50?°C to +20?°C. It was carried out in three parallel loops, each with two chilled mirror hygrometers as transfer standards in each loop. The comparison scheme was designed to ensure high quality results with evenly spread workload for the participants. It is shown that the standard uncertainty due to the long-term instability was smaller than 0.008?°C in all loops. The standard uncertainties due to links between the loops were found to be smaller than 0.025?°C at ?50?°C and 0.010?°C elsewhere. Conclusions on the equivalence of the dew-point temperature standards are drawn on the basis of calculated bilateral degrees of equivalence and deviations from the EURAMET comparison reference values (ERV). Taking into account 16 different primary dew-point realizations and 8 secondary realizations, the results demonstrate the equivalence of a large number of laboratories at an uncertainty level that is better than achieved in other multilateral comparisons so far in the humidity field. 相似文献
35.
Aline Simo Bonex Mwakikunga Bertrand T. Sone Basil Julies Reginaldt Madjoe Malik Maaza 《International Journal of Hydrogen Energy》2014
Mott-type VO2 oxide nanobelts are demonstrated to be effective hydrogen gas sensors at room temperature. These nanobelts, synthesized by hydrothermal process and exhibiting the VO2 (A) crystallographic phase, display room temperature H2 sensitivity as low as 0.17 ppm. The nanobelts (ultralong belt-like) nanostructures could be an ideal system for fully understanding dimensionally confined transport phenomena in functional oxides and for building functional devices based on individual nanobelts. 相似文献
36.
Today, although intellectual properties (IP) and their reuse are common, their use is causing design security issues: illegal copying, counterfeiting, and reverse engineering. IP watermarking is an efficient way to detect an unauthorized IP copy or a counterfeit. In this context, many interesting solutions have been proposed. However, few combine the watermarking process with synthesis. This article presents a new solution, i.e. automatic low cost IP watermarking included in the high-level synthesis process. The proposed method differs from those cited in the literature as the marking is not material, but is based on mathematical relationships between numeric values as inputs and outputs at specified times. Some implementation results with Xilinx Virtex-5 FPGA that the proposed solution required a lower area and timing overhead than existing solutions. 相似文献
37.
Manhal Abouzlam Régis Ouvrard Driss Mehdi Florence Pontlevoy Bertrand Gombert Nathalie Karpel Vel Leitner Sahidou Boukari 《Control Engineering Practice》2013,21(1):105-112
This paper deals with the control of a wastewater treatment pilot by catalytic ozonation. In general, catalytic ozonation processes operate with a deliberate ozone overproduction to obtain a treated water which respects discharge standards. But, in this case, the oxygen consumption is not optimal and the operating costs are important. The objective of this study focuses on the optimization of the catalytic ozonation reactor. A continuous-time transfer function model is identified to represent the pilot behavior, and an optimal control is proposed to obtain a significant abatement of the pollutant. In this application, the pollutant abatement is represented by the absorbance. 相似文献
38.
The global oil market is experiencing a structural shift. Faced with a rapid price decline, large oil-producing countries had decided to protect their market share, with the hopes of permanently removing expensive supply from the market. Meanwhile, the ability of the US shale oil producers to respond quickly to positive price signals puts downward pressure on prices. On the demand side, advances in renewable technology and the continued effort to curb consumption of fossil fuel conspire to inhibit long-run growth.1 These factors suggest that the current down-cycle may continue for an extended period of time or even invoke another down-cycle. 相似文献
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