NUMERICAL SIMULATION OF ALTERNATIVE HORIZONTAL LEVITATION ELECTROMAGNETIC CONTINUOUS CASTING（Ⅱ）

ＮＵＭＥＲＩＣＡＬＳＩＭＵＬＡＴＩＯＮＯＦＡＬＴＥＲＮＡＴＩＶＥＨＯＲＩＺＯＮＴＡＬＬＥＶＩＴＡＴＩＯＮＥＬＥＣＴＲＯＭＡＧＮＥＴＩＣＣＯＮＴＩＮＵＯＵＳＣＡＳＴＩＮＧ（Ⅱ）￥ＺｈｕＳｈｏｕｊｕｎ；ＲｅｎＺｈｏｎｇｍｉｎｇ；ＤｅｎｇＫａｎｇ；Ｊｉａｎ...     

9SiCr钢中的筐篮编结状马氏体及其性能

将9SiCr钢的粒状原始组织改变为片状,再经830℃淬火后,其马氏体形态为筐篮编结状。而传统工艺所获得的马氏体形态为针状.这种筐篮编结状马氏体是9SiCr钢中一种崭新的组织形态,其精细结构为平行成束的板条。亚结构为高密度缠结位错.它有良好的综合机械性能,强韧性高,耐磨性高。     

论高校管理创新的路径

高校教育教学活动总是在管理过程中进行的，其创新从一定意义上取决于高校管理的创新。就其创新的路径而言，应从管理理念上实现从物本管理向人本管理转变，从管理职能上实现从控制型管理向服务型管理转变，从管理组织上实现从垂直管理向扁平管理转变，从管理方式上实现从经验管理向制度管理转变，从管理机制上实现从维持学校向经营学校转变，这些路径是一个相互联系、相互影响的有机整体。     

CdZnTe Crystal Growth by Vertical Gradient Freezing Method

ＣｄＺｎＴｅＣｒｙｓｔａｌＧｒｏｗｔｈｂｙＶｅｒｔｉｃａｌＧｒａｄｉｅｎｔＦｒｅｅｚｉｎｇＭｅｔｈｏｄＨｏｕＱｉｎｇｒｕｎ；ＷａｎｇＪｉｎｙｉ；ＤｅｎｇＪｉｎｃｈｅｎｇ；ＤｕＢｉｎｇ，（侯清润）（王金义）（邓金诚）（杜冰）；ＬｉＭｅｉｒｏｎｇａｎｄＣ...     

邻苯基苯酚合成工艺及应用

介绍了邻苯基苯酚的主要用途，国内外邻苯基苯酚主要的合成工艺路线及应用情况，通过对主要合成路线的比较，对今后国内的邻苯基苯酚的产业化提出合理的建议。     

2,4,6-三硝基苯甲酸的合成工艺改进

对TNT(2，4，6-三硝基甲苯)氧化制备2，4，6-三硝基苯甲酸的工艺进行了深入的研究，结果表明氧化剂的种类、用量、加料方式及溶剂的种类对产物的收率有较大影响。TNT的较佳氧化工艺条件为：氧化20gTNT，以摩尔比为4：1的HNO3和HCI混合液作为溶剂，采用液体加料方式加入氧化剂KClO4 40g，2，4，6-三硝基苯甲酸的收率最高达96％。     

高岭土改性聚酯纤维

介绍了高岭土在改性聚酯中的作用、纤维级高岭土的性质以及改性聚酯的制造方法．指出了我国开发高岭土改性聚酯纤维的的前景．     

Coloring effect of the organic hybrid of polyamide 6 and N,N′‐ethylene‐bis(tetrabromophthalimide)

Coloring study in organic hybrid of polyamide (PA6) and N,N′‐ethylene‐bis(tetrabromophthalimide) (EPT), where the chromophore was self‐assembled by hydrogen bonding formed between PA6 molecular chains and EPT compound, have been characterized by several techniques. CS930 double wavelength lamella scanner was employed to measure the change of color. The existence of hydrogen bonding in PA6/N‐N′‐ethylene‐bis (tetrabromophthalimide) (PA6EPT) was investigated with Fourier transform infrared (FTIR), the results of which were compared with that of PA6 with the same thermal history. FTIR spectra at room temperature revealed that there is essentially hydrogen bonding between PA6 and EPT. The crystallization behavior of PA6EPT affected by hydrogen bonding was studied by using FTIR. The temperature‐dependent behavior of both PA6 and PA6EPT was studied by temperature‐FTIR spectroscopy and differential scanning calorimetry (DSC). With temperature increasing, changes in sensitive, high‐resolution absorbance spectra are observed as dissolve‐volatilizing thin film. Temperature‐FTIR results showed that the hydrogen bonding in PA6EPT attenuated and dissociated considerably at a smaller rate than PA6, that is to say, hydrogen bonding in PA6EPT is more stable than that in PA6. DSC showed that the melting temperature of PA6EPT and PA6 are similar. However, the crystalline degree and crystalline temperature and melting enthalpy of PA6 and PA6EPT are different. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 104: 594–600, 2007     

Study of stability of high‐temperature polyimides using TG/MS technique

The oxidative stability of the carbon fiber‐reinforced composite of polyimide was examined, in real time, using the evolved gas analysis techniques. Off‐gas degradation products suggested the onset temperature for chain scissions to be fairly low at about 190–220°C. Based on the off‐gas products present and the trend of their release, the composite degradation mechanism appeared to be similar between 190 and 371°C, thereby marking 371°C to be the highest accelerated aging temperature for its long‐term lifetime prediction. Beyond 371°C, different degradation mechanisms would apply. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 1219–1227, 2002     

明胶中过氧化物的控制

在用药用明胶为主要原料生产药用空心胶囊的生产中,由于明胶中的过氧化物对胶囊中各种色素的颜色具有氧化褪色作用,胶囊产品放置时间过长,其颜色就会发生变化,加上药品自身安全性的要求等原因,故国内引进的外国胶囊生产线对明胶原料中的过氧化物含量的要求特别严格,要求明胶中不得检出过氧化物成分.尽管目前我国药典和轻工行业对药用明胶标准未作过氧化物含量的规定,相信很多生产药用空心胶囊的厂家对此项目都有内控标准,如本胶囊公司就规定,凡对购进的明胶均不得检出过氧化物成分,否则一律退货.笔者相信,不久的将业,药用明胶的标准修订肯定会增加过氧化物含量的规定.为此,明胶生产企业就必须在明胶生产中严格控制过氧化物的含量,使其达到客户的要求.