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101.
Effects of Atmospheric Composition on the Molecular Structure of Synthesized Silicon Oxycarbides 下载免费PDF全文
Masaki Narisawa Fuji Funabiki Akihiro Iwase Fumihiro Wakai Hideo Hosono 《Journal of the American Ceramic Society》2015,98(10):3373-3380
The dependence of silicon oxycarbides' chemical composition and molecular structure on their reaction conditions was tested by varying the atmosphere under which pyrolysis was performed. To obtain the silicon oxycarbides, densely cross‐linked silicone resin particles with an averaged diameter of 2 μm were pyrolyzed in various atmospheres of H2, Ar, and CO2, in the temperature range 700°C–1100°C. The residual mass of resin after pyrolysis was almost constant at 700°C, although their apparent colors varied distinctly. The sample obtained from the H2 atmosphere was white, whereas that obtained from the CO2 atmosphere was dark brown. Fourier‐transform infrared (FT‐IR) spectra of the residues suggested that the Si–O–Si network evolution was accelerated in the CO2 atmosphere. Beyond 800°C, the chemical compositions of the compounds obtained from a H2 atmosphere increasingly approached near‐stoichiometric SiO2–xSiC composition with increasing the pyrolysis temperature. Compounds from a CO2 atmosphere approached a composition of SiO2–xC with no free SiC as the pyrolysis temperature increased. In the products from an Ar atmosphere, SiO2–xSiC–yC compositions were typically obtained. The observed effects of the pyrolysis atmosphere on the resulting chemical compositions were analyzed in terms of thermodynamic calculations. Electron spin resonance (ESR) spectra revealed broad and intense signals from products obtained from either Ar or CO2. Estimating from the signal intensity, the residual spin concentrations were in the range 1018–1019 g?1. Meanwhile, the spectra from the samples obtained in H2 showed weak and sharp signals with estimated spin concentrations ranging from 1016–1017 g?1. This signal attenuation may have been due to the hydrogen capping of dangling bond formed during pyrolysis. 相似文献
102.
Akihiro Ishimi Kozo Katsuyama Koji Maeda Tsuyoshi Nagamine Takeo Asaga Hirotaka Furuya 《Journal of Nuclear Science and Technology》2013,50(12):1144-1155
The X-ray CT technology previously developed by JAEA was upgraded. The shape of the X-ray source beam was changed from a circular shape to an elliptical one and the collimator slit width was decreased from 0.3 to 0.1 mm. The X-ray detector was improved by changing a CdWO4 scintillator to a highly sensitive silicon semiconductor detector. The analysis code of X-ray CT image was revised with respect to the number of points by using two kinds of experimental results and taking into account the effects of crack existence and deviation of the central void position from the radial center of a fuel pellet. As a result, high resolution X-ray CT images could be obtained on the transverse cross section of irradiated fuel assemblies. The error of the dimensional measurement was improved from ±0.1 to ±0.03 mm by upgrading the instrument and revising the analysis code of X-ray CT image. The discriminating accuracy of density difference could be increased, and the low density region (undisturbed region) and high density region (equi-axial and columnar regions) in the X-ray CT image on the cross section of irradiated fuel could be discriminated from each other. The reliability of fuel performance analysis improves because a large number of PIE data can be collected, compared with the conventional destructive PIE. 相似文献
103.
Takuro Tomita Ayahito Uetake Tsutomu Asahina Kentaro Kayanuma Akihiro Murayama Yasuo Oka 《Journal of Superconductivity and Novel Magnetism》2005,18(3):405-410
Spin injection processes in the double quantum dots of ZnSe-based diluted magnetic semiconductors are discussed. Double quantum
dots are fabricated from ZnSe-based double quantum wells by electron beam lithography and wet etching. In these samples, the
photo-excited carriers in the magnetic dots are injected into the non-magnetic dots. The circular polarization degrees of
photoluminescence from the non-magnetic dots are measured by micro-photoluminescence measurement system under the magnetic
field up to 5 T. The maximum spin polarization degrees of injected carriers determined from our experiment are 10% for double
quantum wells and 15% for double quantum dots. The spin injection efficiency was estimated both from the observed circular
polarization degree and the diffusion length of carriers. We concluded that the spin injection efficiency is increased in
the double quantum dots. 相似文献
104.
E Totsuka S Todo Y Zhu N Ishizaki Y Kawashima MB Jin A Urakami T Shimamura TE Starzl 《Canadian Metallurgical Quarterly》1998,187(3):276-286
Workplace AIDS training is a recent addition to many corporations' occupational health agenda. However, little is known about the objectives, content, and practices of AIDS training programs. A survey of 126 workplace AIDS trainers was conducted to determine the impact of the trainer's organizational affiliation (in-house, consultant, union, etc.) and personal motives on training program objectives, content, and practices. Results indicate that the organizational affiliation of trainers is significantly related to training objectives, topics, and practices, whereas strong personal motives for becoming an AIDS trainer is significantly associated with an emphasis on more controversial content areas and training practices. Findings are discussed in terms of applicability to other values-oriented training topics, applications to practice, and future research needs. 相似文献
105.
Dr. Tomoya Hirano Dr. Takashi Fujiwara Dr. Hideaki Niwa Michitake Hirano Kasumi Ohira Yusuke Okazaki Shin Sato Dr. Takashi Umehara Dr. Yuki Maemoto Prof. Akihiro Ito Prof. Minoru Yoshida Prof. Hiroyuki Kagechika 《ChemMedChem》2018,13(15):1530-1540
The histone methyltransferase SET7/9 methylates not only histone but also non‐histone proteins as substrates, and therefore, SET7/9 inhibitors are considered candidates for the treatment of diseases. Previously, our group identified cyproheptadine, used clinically as a serotonin receptor antagonist and histamine receptor (H1) antagonist, as a novel scaffold of the SET7/9 inhibitor. In this work, we focused on dibenzosuberene as a substructure of cyproheptadine and synthesized derivatives with various functional groups. Among them, the compound bearing a 2‐hydroxy group showed the most potent activity. On the other hand, a 3‐hydroxy group or another hydrophilic functional group such as acetamide decreased the activity. Structural analysis clarified a rationale for the improved potency only by tightly restricted location and type of the hydrophilic group. In addition, a SET7/9 loop, which was only partially visible in the complex with cyproheptadine, became more clearly visible in the complex with 2‐hydroxycyproheptadine. These results are expected to be helpful for further structure‐based development of SET7/9 inhibitors. 相似文献
106.
Nakazawa M Kosugi T Nagatsuka H Maezawa A Nakamura K Ueha S 《IEEE transactions on ultrasonics, ferroelectrics, and frequency control》2007,54(10):2165-2174
Ultrasonic transducers using polyurea piezoelectric thin film are studied in this paper. Aromatic polyurea thin films, prepared by vapor deposition polymerization, have useful characteristics for use as an ultrasonic transducer. This paper presents the fabrication and experimental evaluation of ultrasonic transducers formed using polyurea films. First, the vapor deposition polymerization process using two monomers is briefly reviewed, and the temperature conditions for higher piezoelectric constants are explored. Second, in order to test the fundamental characteristics of this material as a high-frequency, ultrasonic transducer, a polyurea film of 2.5 microm thickness was deposited on a silicon substrate. In the pulse/echo experiment results, a resonant frequency of about 100 MHz was observed. Third, we fabricated a concave point focus transducer and a cylindrical line focus transducer. To examine the performances of the focus transducers, two-dimensional images of a coin and V(z) curve measurements for an aluminum surface were demonstrated. 相似文献
107.
Akihiro Imura Tomoya Takahashi Masami Fujitsuna Tadanao Zanma Shinji Doki 《IEEJ Transactions on Electrical and Electronic Engineering》2014,9(1):83-89
Model predictive instantaneous‐current control (MPIC), which was proposed in our earlier works, enables us to achieve better instantaneous current control using mathematical models of an inverter and permanent magnet synchronous motors (PMSMs). However, dead‐time to avoid short breakdown in the inverter is not usually considered in a general inverter model. Such an unmodeled part in the inverter model prevents accurate prediction of current evolution in motor systems based on the model predictive control. Therefore, in this paper, we analyze current response resulting from the dead‐time in the MPIC, and propose a refined inverter model considering the dead‐time so that control performance is improved. The effectiveness of the proposed method is verified through simulation and experiments. © 2013 Institute of Electrical Engineers of Japan. Published by John Wiley & Sons, Inc. 相似文献
108.
Nobuhisa Ochi Shigetaka Okano Masahito Mochizuki Junji Shimamura Nobuyuki Ishikawa 《Welding International》2013,27(3):174-183
In recent years, in order to reduce the costs of transportation and construction of pipelines, which are often constructed using multiple-electrode submerged arc welding (SAW), higher joint performance is required. Therefore, there has arisen the need to understand theoretically and control appropriately metallurgical and mechanical characteristics in heat-affected zone (HAZ), which has a significant influence on the strength and toughness of welded joints. Commonly, metallurgical phenomena in HAZ are evaluated based on the highest temperature and the cooling rate. Therefore, in order to control metallurgical and mechanical characteristics in HAZ by means of the welding conditions, evaluating the temperature distribution and the temperature history near the melted zone is essential. However, a detailed investigation of the temperature distribution for multiple-electrode SAW has not yet been carried out enough. In this study, in order to investigate the temperature distribution and histories during multiple-electrode SAW, the experimental results are compared with the theoretical results. In the theoretical analysis, the temperature rise equation in multiple heat sources welding is developed using the method of summation. Furthermore, on temperature distribution during welding, the effects of multiple heat sources, such as the number of heat sources and the distance between each electrodes, are considered quantitatively through the thermal conduction theoretical analysis. As the result, the distance between lead heat source and final heat source primally influences the area with the difference between a single heat source welding and multiple heat sources welding. Based on the results, it is expected to control temperature distribution near melted zone by more appropriate heat input characteristics, which is depended on heat source arrangement. 相似文献
109.
Shingo Hirose Akihiro Yoshida Masaaki Yamaura Nobuo Kano Hiro Munekata 《Journal of Materials Science: Materials in Electronics》2000,11(1):7-10
We demonstrate a method for successfully controlling carbon incorporation in AlAs layers grown by atomic layer epitaxy (ALE) using various GaAs substrates with different orientations. The number of alkyl radicals attached to an Al atom at the surface, which is a main factor in carbon incorporation, can be intentionally controlled by changing substrate orientation. We found that the carbon incorporation in ALE-AlAs using the (3 1 1)B surface is 2 x 1017,cm-3, which is the lowest value ever reported for ALE-AlAs that satisfies one-monolayer self-limiting growth conditions. 相似文献
110.
Correction and evaluation of the effect due to parasitic motion on primary accelerometer calibration 总被引:1,自引:0,他引:1
Primary accelerometer calibration is carried out under the assumption that a vibration exciter gives a rectilinear motion to an accelerometer to be calibrated. However practical vibration given by the vibration exciter includes parasitic motion such as transverse, rocking, and bending motion. Such parasitic motion would give two serious effects on primary calibration results, transverse motion effect and vibration distribution effect. Transverse motion effect is caused by an inner product of the vectors of both transverse motion and transverse sensitivity. On the other hand, the vibration distribution effect is caused by relative motion between a sensing point of accelerometer and a spot sensed by the interferometer. As these effects have close interaction between parasitic motion and measuring instruments, it would be very difficult to evaluate them by measuring independently each component. 相似文献