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61.
基于工频或高频磁化条件下磁芯的测试数据不能准确反映磁芯在单次脉冲磁化下的性能,给出了一种脉冲磁化条件下磁芯性能的测试方法和数据处理方法,实验研究了快脉冲磁化条件下非晶态合金磁芯的损耗特性,磁芯最短饱和时间67 ns,最大磁化速率达到40 T/s。通过数据处理,给出了磁芯损耗与磁化速率的关系曲线,获得了不同磁化速率下磁芯的损耗数据。分析了脉冲磁化条件下涡流损耗和磁滞损耗所占的比例。研究结果表明:脉冲磁化条件下非晶态合金磁芯损耗与磁化速率关系符合饱和波模型,磁芯损耗随磁化速率增大而线性增大。 相似文献
62.
测定了不同浓度、不同温度条件下含Schiff碱基的单链两亲性化合物在C16SBC6N+OH水溶液的电子吸收光谱。结果表明,两亲性分子在高温低浓度水溶液中处于较为分散状态,而在低温高浓度水溶液中呈聚集状态(双分子膜)。同时,通过量化计算比较,得出了不同聚集态时Schiff碱基的构象(即N-苯环与C-苯环的扭转二面角)。 相似文献
63.
Using a full configuration-interaction method with Hylleraas-Gaussian basis function, this paper investigates the 110+, 11(–1)+ and 11(–2)+ states of the hydrogen negative ion in strong magnetic fields. The total energies, electron detachment energies and derivatives of the total energy with respect to the magnetic field are presented as functions of magnetic field over a wide range of field strengths. Compared with the available theoretical data, the accuracy for the energies is enhanced significantly. The field regimes 3 < γ < 4 and 0.02 < γ < 0.05, in which the 11(–1)+ and 11(–2)+ states start to become bound, respectively, are also determined based on the calculated electron detachment energies. 相似文献
64.
一种基于图像特征和神经网络的苹果图像分割算法 总被引:7,自引:1,他引:7
苹果识别是开发苹果采摘机器人的关键环节,利用图像处理技术和神经网络分类器探索苹果图像分割算法.从苹果树图片中选取苹果图像样本和背景网像样本.分别计算这两类图像样本的颜色特征和纹理特征.颜色特征的计算基于RGB色彩模型,纹理特征的计算基于灰度共生矩阵.选取适当的颜色特征(R/B值)和纹理特征(对比度值和相关性值)作为输入节点,利用反向传播神经网络分类器建模,输出值是一个O~1之间的计算值.通过阈值将输出结果分类为苹果或背景.试验结果表明,该算法正确率大于87.6%,对光照的影响不敏感,是一利较为实用的苹果分割算法. 相似文献
65.
Wei Zhou Xiangning Fang Qinglong Qiao Wenchao Jiang Yue Zhang Zhaochao Xu 《中国化学快报》2021,32(2):943-946
With the development of single-molecule detection and super-resolution fluorescence imaging, rhodamine dyes gain new life. Through the modification of the N-substituents and the replacement of the oxygen atom in xanthene, the wavelength and brightness can be effectively changed. However, the spectra of rhodamine, especially due to the balance between ring-closed non-fluorescent lactone and ring-opened fluorescent zwitterion/cation, are sensitive to interference from various environmental factors. In this way, the spectral data of various rhodamines reported by different research groups under different test conditions lacked comparability, sometimes even lacked accuracy. In order to meet the requirements for the accuracy and uniformity of spectral data in the research of single molecule imaging and dye structure-fluorescence relationship study, we have tested the spectra of fifteen rhodamine dyes that cover the visible and near-infrared regions under exactly the same conditions. By studying the dependence of the spectra on dye concentrations, it was confirmed that 1 μmol/L was ideal for detection less from the interference of dye molecule aggregation. We provide comprehensive and reliable spectral data of these fifteen dyes, which are expected to be used as references for future research. And the direct comparison of different rhodamine spectra would help to understand the structure-fluorescence relationship of rhodamines. 相似文献
66.
Solubility of methane in octane + ethanol was measured at temperatures ranging from 303.15 K to 333.15 K and pressures ranging
from 2.60 MPa to 12.01 MPa. Experimental data were analyzed using the Soave-Redlich-Kwong equation of state with three types
of mixing rules, and the estimated average deviation from the experimental solubility data was less than 3.5 %. 相似文献
67.
Xiaoji Cao Jingfang Qiao Liping Wang Xuemin Ye Lebin Zheng Nan Jiang Weimin Mo 《Rapid communications in mass spectrometry : RCM》2012,26(7):740-748
A powerful ionic liquid‐based ultrasonic‐assisted extraction (ILUAE) method combined with ultra‐performance liquid chromatography coupled to electrospray ionization quadrupole time‐of‐flight tandem mass spectrometry (UPLC/ESI‐QTOFMSn) was employed in the rapid simultaneous screening of iridoid glycosides, phenylethanoid glycosides, and cucurbitacin glycosides from P. scrophulariiflora. The ILUAE procedure was optimized over several ultrasonic parameters, including the ultrasonic power, concentration of the ionic liquid, and solid–liquid ratio. A comparison with conventional heat‐reflux extraction and regular UAE demonstrated that the optimized approach yielded a high extraction efficiency (Picroside I, 2.84%; Picroside II, 3.57%; 6‐O‐E‐feruloyl catalpol, 2.20%) within a short extraction time of 30 min. Negative ion mode ESI‐QTOFMS2 analysis of the fragmentation reactions of the [M–H]– ions was conducted to characterize the diagnostic ions related to the glycosyl moieties, aglycone units, and the type and substituted position of the ester groups. Interestingly, the positional isomers of the iridoid glycosides could be easily discriminated based on the characteristic ions. A total of 15 glycosides, including three groups of iridoid glycoside isomers and two groups of phenylethanoid glycoside isomers, were conveniently identified within 13.5 min. Moreover, 6'‐O‐vanilloyl catalpol was identified in P. scrophulariiflora for the first time. The method developed here was further validated by measuring the recovery, correlation coefficient (R2), and reproducibility (RSD, n = 5) of three iridoid glycosides: 89.60%–109.02%, 0.9991–0.9998, and 0.93%–1.44%, respectively. This study demonstrated the capabilities of ILUAE combined with UPLC/ESI‐QTOFMSn for the rapid screening of glycosides in P. scrophulariiflora. This method offers an approach to similar studies on other natural plants. Copyright © 2012 John Wiley & Sons, Ltd. 相似文献
68.
Mei Tian Huan Huan Sun Xiao Wei Tian Zhi Xin Xu Feng Qiao Wang Dan Shu Yao 《Liquid crystals》2013,40(3):298-308
A series of side-chain liquid crystal (LC) polysiloxanes were synthesised with Poly(methylhydrogeno)siloxane, 4?-(undec-10-enoyloxy) biphenyl – 4 – yl 4- (trifluoromethyl) benzoate (Mth) and a chiral nematic (N*) LC monomer 1-allyl 10-(cholesteryl)-decanedioate (Mch). The chemical structures and LC properties of the monomers and polymers were characterised by FTIR, 1H-NMR, differential scanning calorimetry, thermogravimetric analysis, POM and X-ray diffractometer. Mch is monotropic N* LC. The homopolymer derived from monomer Mch is enantiotropic N* LC. Monomer Mth is a smectic A liquid crystal. The copolymers derived from Mch and Mth are N* LCs. The temperatures at which 5% weight loss occurred are greater than 300°C for all the fluoro-containing polymers, and the residue weights of the samples at 600°C increased slightly as the content of trifluoromethyl mesogens increased in the polymers. The glass transition temperatures of the polymers increased as trifluoromethyl mesogens increased, too. The N*–I phase transition temperatures show a negative deviate from ideal or linear behaviour. The values of the enthalpy changes for the cholesteryl containing polymers are rather low and this is attributed to the biaxiality of cholesteryl moiety which tends to reduce the change in the orientational order at the N*–I transition. Compared to the monomers, the polymers show wider mesophase region. 相似文献
69.
Hongxia Guo Yuechun Qiao Guohua Liu Jingqing Gao 《Russian Journal of Electrochemistry》2013,49(4):396-399
Single-phased nanosized LiFePO4 with thinner thickness along [010] crystallographic direction were successfully fabricated under solvothermal condition by using glycerol as co-solvent. The as-obtained product with thinner thickness is beneficial for fast migration of Li ions in the olivine-structured LiFePO4, hence exhibiting excellent electrochemical performance. 相似文献
70.