金属-有机骨架材料NH_2-MIL-53(Al)对水中双氯芬酸钠的吸附性能

采用溶剂热法合成了金属-有机骨架材料NH_2-MIL-53(Al),对活化后的产物进行了粉末X射线衍射(PXRD)、扫描电子显微镜(SEM)及傅里叶变换红外光谱(FTIR)等表征,研究了其在水溶液中对双氯芬酸钠的吸附性能.实验结果表明,NH_2-MIL-53(Al)对双氯芬酸钠具有良好的吸附性能,对5 mg/L的双氯芬酸钠能在40 min内达到吸附平衡,且吸附动力学结果符合准二级动力学曲线,利用Langmuir模型和Freundlich模型拟合吸附等温线,结果表明Langmuir模型拟合效果更好.循环吸附实验结果表明NH_2-MIL-53(Al)具有良好的重复利用性.此外,结合ζ电位测试结果以及p H值对吸附效果的影响,对可能的吸附机理进行了阐述.     

玉门原油润滑油馏分的性质

本文记述了对玉门原油各润滑油馏分性质的研究结果.各馏分是由脱沥青的玉门全润滑油镏分经过实沸点蒸馏,高真空蒸馏,酚精炼,丙酮、甲苯、苯脱蜡及白土处理等步骤而取得的窄馏分.另外对各阶段处理后的油的性质进行了分析.这些结果阐明了玉门原油在制取润滑油上有它的一些有利条件,作为普通的各种润滑油的原料是很合适的;但另一方面,也有它的缺点,就是粘度指数较低.平均分子结构的分析表明,玉门润滑油主要是由多环而侧链短之成分所组成的;经溶剂分析也得知其中高粘度指数成分较少,只有在低收率时方可获得一部分粘度指数为84—88的航空机油.唯此时一部分抽出油质量很好,可用作普通的机油.     

“老师,我的解法比你的更好!”——记数学试卷讲评课上的一次风波

1背景描述新课程改革在广东已开展多年.2007年9月至今,我在自己任教的两个理科班开展了在高中数学教学中开展数学交流活动的实验研究.在这实验研究中,结合数学新课程改革理念,我不断加强理论学习、反思实验过程,收获颇多:学生的数学学习兴趣大     

Angular distribution of ~6He+p elastic scattering

The angular distribution of ¹H(⁶He,p)⁶He elastic scattering has been measured at E_c.m.=4.3 MeV by using a thick-target inverse kinematic method. The experimental differential cross sections are reproduced by the distorted-wave Born approximation calculation utilizing the CH89 global optical potential parameter set. The real part of CH89 is reduced comparing with other potentials, which may be attributed to the couplings necessary for the weakly bound nuclei.     

Excited States in ^18Ne Studied via ^17F＋p

The elastic resonance scattering of ^17F＋p is studied in inverse kinematics via a thick-target method. The excitation function for ^17F＋p elastic scattering is obtained within the energy interval of Ec.m ≈ 0.4-1.7 MeV. The experimental excitation function is analyzed with a multilevel R-matrix code MULTI7, and the proton widths are deduced. The α decay from 6.15 MeV 1- state in 18Ne is observed, which is critical to the 14O（α, p）17F reaction as the main breakout route from CNO cycle to rp-process in supernovae and x-ray bursts.     

PET共混改性研究

综述了国内外PET共混改性的研究现状 ,并介绍了近年来PET共混研究的新发展     

L形通道布线的展开法

本文提出将L形通道展成直通道的布线方法，对展开后的直通道定义了水平约束、垂直约束、拐角约束、走线约束，利用赋权的混合图反映这四种约束、并逐步将图中的无向边转变成有向边，按照有向图的线网上下关系，完成直通道布线，再收缩冗余布线区变成L形通道布线.     

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为了研究等离子体与自由液态锂表面相互作用的物理过程,建立了用氩气驱动的液态锂回路装置。介绍了建立的液态锂回路装置的组成部分、技术参数及运行原理。此回路主要由主回路、等离子体与液态锂相互作用试验段和单阴极高密度等离子体发生装置三部分组成。目前,此回路已取得一些初步的模拟结果和实验结果。     

聚合物纳米复合体系中聚合物结构及动力学研究进展

从计算模拟及实验角度系统总结了聚合物结构、 聚合物构象、 聚合物扩散及聚合物多尺度动力学的研究进展, 阐述了各影响因素及其变化规律, 并对聚合物动力学的未来研究进行了展望.     

Morphological and structural damage investigation of nanostructured molybdenum fuzzy surface after pulsed plasma bombardment

Steady high-flux helium (He) plasma with energy ranging from 50 eV to 90 eV is used to fabricate a fiber-form nanostructure called fuzz on a polycrystalline molybdenum (Mo) surface. Enhanced hydrogen (H) pulsed plasma in a wide power density range of 12 MW/m²-35 MW/m² is subsequently used to bombard the fuzzy Mo, thereby simulating the damage of edge localized mode (ELM) to fuzz. The comparisons of surface morphologies, crystalline structures, and optical reflectivity between the original Mo and the Mo treated with various He⁺ energy and transient power densities are performed. With the increase of He ion energy, the Mo nano-fuzz evolved density is enlarged due to the decrease of filament diameter and optical reflectivity. The fuzz-enhanced He release should be the consequence of crystalline growth and the lattice shrinkage inside the Mo-irradiated layers (~200 nm). The fuzz induced by lower energy experiences more severe melting damage and dust release under the condition of the identical transient H plasma-bombardment. The H and He are less likely to be trapped due to aggravated melting evidenced by the enhanced crystalline size and distinct lattice shrinkage. As the transient power density rises, the thermal effect is enhanced, thereby causing the fuzz melting loss to aggravate and finally to completely disappear when the power density exceeds 21 MW/m². Irreversible grain expansion results in huge tensile stress, leading to the observable brittle cracking. The effects of transient thermal load and He ion energy play a crucial role in etching Mo fuzz during ELM transient events.