毫米波缝隙天线的三维非硅微加工制造技术

讨论了面向毫米波缝隙天线集成制造应用的三维非硅微加工技术方案,重点解决多种材料兼容、多层复杂微结构集成和大悬空高度等独特难题。针对天线器件中金属和介质材料的结合,提出了加法工艺、减法工艺以及一种通用型图形化微加工工艺,其中通用型图形化工艺为各种非硅薄膜材料在MEMS体系中的灵活运用创造了条件;为了实现多层复杂微结构的加工,提出工艺整合和工艺兼容性设计,针对天线器件中的悬空结构对牺牲层工艺进行了研究;最后以一种单向宽带毫米波平面缝隙天线为例,阐述其具体工艺流程,验证了上述工艺的可行性。     

Effect of fatty acid positional distribution and triacylglycerol composition on lipid by-products formation during heat treatment: I. Polymer formation

Effects of the fatty acid positional distribution and of the triacylglycerol (TG) composition on polymerization of TG during heat treatment were studied. Diacid TG molecules, acylated only with linoleic acid or linolenic acid along with palmitic acid, and positioned either in the central position (PLP and PLnP, respectively) or in one of the two outer positions (PPL and PPLn, respectively) were synthesized. Monoacid TG, i.e., trilinolein and trilinolenin, were also synthesized and mixed with tripalmitin in a 1:2 ratio. These model TG were also compared to TG models that consisted of a canola oil and its randomized counterpart, whose fatty acid positional distribution and TG composition were determined by means of high-performance liquid chromatography (HPLC). After heating, the polymer content and composition were evaluated by HPLC-size exclusion chromatography. Both pure TG and the canola oil models showed that acylation of polyunsaturated acids in the central position was protective against polymerization, although the effect was mainly observed with linolenic acid. The synthetic-TG study showed that the monoacid TG species exhibited higher sensitivity toward polymerization than the diacid species. The slight differences in the TG species between both canola oils did not allow observation of such a relationship with regard to TG composition.     

ArcGIS-based evaluation of geo-hazards at Yaozhou County,Shaanxi,China

In conventional susceptibility evaluation of geo-hazards,there are some limits,such as unreasonable division of evaluated region,difficulty in quantifying evaluation indicators,time-consuming calculation.To address these problems,we try to employ the software ArcGIS to evaluate geo-hazards susceptibility.The study area of Yaozhou County is automatically divided into 3562 units.Based on the spatial overlay analysis function of ArcGIS,quantitative evaluation of geo-hazards susceptibility is implemented in the study area,and the geo-hazards susceptibility zoning is mapped.It is observed that the evaluation results match well with field investigations.     

Degradation of reactive dyes in wastewater from the textile industry by ozone: Analysis of the products by accurate masses

The present work describes the use of ozone to degrade selected reactive dyes from the textile industry and the analysis of the resulting complex mixture by liquid chromatography/mass spectrometry (LC-MS). To allow certain identification of the substances detected in the wastewater, the original dyes were also investigated either separately or in a synthetic mixture of three dyes (trichromie). Since the reactive dyes are hydrolyzed during the dyeing process, procedures for the hydrolysis were worked out first for the individual dyes. The ozonated solutions were concentrated by solid-phase extraction, which separated very polar or ionic substances from moderately polar degradation products. The latter, which are the primary degradation products, were investigated by liquid chromatography/mass spectrometry with a tandem quadrupole time-of-flight mass analyzer. Accurate masses, which in most cases could be determined with a deviation of ≤5 ppm from the exact value, were also measured. In addition, a diode-array detector was placed before the mass analyzer to provide UV-vis spectra of the products in the same run. With retention times, mass spectra, accurate masses, UV-vis spectra and, of course, knowledge of the structures of the original dyes, plausible structures could be proposed for most of the components of the moderately polar fraction. These structures were confirmed by ¹H NMR in cases where it was practical to isolate the degradation products by preparative HPLC.     

酸化井产油量时间序列的混沌特征识别

现有的油气井产量预测方法以传统技术经济预测的惯性原理为基础。混沌理论的产生与发展对这种预测原理提出了挑战。目前有关酸化井产量变化混沌特征识别与预测的相关研究还鲜有公开报道。采用相空间重构和关联维数提取技术,对西部某油田一油井酸化后60 d的产油量时间序列研究发现,此井产油量时间序列的饱和嵌入维数和对应的吸引子维数分别为11和2.64,由此说明该井酸化后的生产系统动态演化规律为高维空间中的奇异吸引子,因而产油量变化表现出混沌特征;并且说明影响该井产油量变化的基本变量为3～11个。从而为单井生产系统动力学模型的建立,特别是人工神经网络预测模型的输入层节点数量的确定提供了定量的参考。     

Dynamic extension - A new principle for a vacuum primary standard for UHV-range (10-10 Pa) calibration of hot cathode ionisation gauges

The main obstacle in the construction of primary vacuum standards for very low pressures - ultra-high vacuum (UHV) - is outgassing from the walls of the apparatus. Thus, principles utilising a higher pumping rate in the calibration chamber, e.g., the pressure ratio technique, seem to be more useful for this range. However, a serious problem is inherent in this method, namely, that the gas in the calibration chamber is not in equilibrium and thus cannot be characterised by a single scalar pressure value, although such a value is then used to evaluate the measurement. This discrepancy can be overcome by using a hot cathode ionisation gauge as a transfer standard calibrated by the dynamic extension method.The dynamic extension method is explained and compared with the pressure ratio technique. The basic conditions for achieving acceptable uncertainty values are considered.     

A Lagrangean heuristic for a two-echelon storage capacitated lot-sizing problem

In this paper, we study a structure issued from a real case. Raw materials (RMs) are sent by suppliers to a distribution center (DC) and then transported to a unique plant where they can be stored. The inventory capacity is limited in the plant as well as in the DC. The transportation capacity between the DC and the plant is also limited. The objective is to determine the flows between suppliers and the DC, and from the DC to the plant in order to satisfy the demand during the planning horizon while minimizing the global cost. A mixed-integer programming (MIP) formulation is presented and a Lagrangean relaxation solution procedure is proposed. Computational experiments are carried out.     

Theoretical and experimental thermal-hydraulic analysis of a new sodium cooled fast breeder reactor core

This paper presents the experimental and theoretical results of the thermal-hydraulic design of a new fast breeder reactor core concept. The main feature of this concept is the omission of fuel element cans.The hydraulic function of these fuel element cans is substituted by a winding flow path through the radial blanket and a ring chamber without tubes.A computer code based on the quasi-continuum-theory and especially adapted to the features of the new core concept is developed for theoretical investigations. The pressure drop of the rod bundles is specified by a resistance tensor.The experimental investigations are realized in a test facility, where sodium is simulated by water. Pressures and velocities are measured.Theoretical and experimental results show good agreement. The aim of flattening of the coolant outlet temperature distribution can be reached with satisfying accuracy.     

Genotypic characterization of seven strains of Mycoplasma fermentans isolated from synovial fluids of patients with arthritis

We performed a genotypic characterization of seven strains of Mycoplasma fermentans which have been isolated from the synovial fluid of patients with rheumatoid arthritis (n = 2), spondyloarthropathy (n = 1), and unclassified arthritis (n = 4). We compared them to three reference strains (strains PG18 and K7 and incognitus strain) and to a clinical isolate from the urethra of a patient with nongonococcal urethritis. The characterization methods included electrophoresis of native DNA, arbitrarily primed PCR, and restriction fragment length polymorphism analysis following conventional and pulsed-field gel electrophoresis. Southern blot analysis with a probe internal to an insertion sequence was performed with the restriction products produced by the last two techniques. No extrachromosomal DNA sequences were detected. The M. fermentans strains identified by these methods did not present a unique profile, but they could be separated into two main categories: four articular isolates were genetically related to PG18 and the three other isolates, the urethral isolate, and the incognitus strain were related to K7. We also looked for the presence of the bacteriophage MAV1 (associated with the arthritogenic property of Mycoplasma arthritidis in rodents) in the M. fermentans strains. MAV1 DNA was not detected in either the clinical isolates or the reference strains of M. fermentans.     

The Synergistic Effect Between Phosphonocarboxylic Acid Salts and Fatty Amines for the Corrosion Protection of a Carbon Steel

This work was carried out to have a better understanding of the synergistic effect between phosphonocarboxylic acid salts (PCAS) and fatty amines (FA) for the corrosion protection of a carbon steel in a 200 mg l^–1 NaCl solution. These compounds, combined with a biocide at low dosage, are used for water treatment in cooling circuits. First, electrochemical impedance measurements were performed to verify the inhibitive properties of the mixtures. Among the different concentrations tested, maximum efficiency was reached for the mixture containing 200 mg l^–1 PCAS + 50 mg l^–1 FA. Then, electrochemical measurements (current—voltage curves and impedance diagrams) were combined with surface analysis (X-ray photoelectron spectroscopy) for each compound at the optimized concentrations and for the mixture. In the presence of amines, the iron oxide/hydroxide layer remained porous and the inhibition efficiency was relatively low. The FA acted by repelling the water molecules from the interface. PCAS sealed the pores of the oxide layer by forming a chelate. Thus, the growth of the inhibitive layer was limited but the efficiency was higher than for the FA alone. For the optimized mixture, the formation of the chelate was enhanced and the protective properties of the layer improved. A competitive adsorption mechanism was proposed to account for the synergistic effect observed in the presence of both compounds.