Microstructure and mechanical properties of laser welded S960 high strength steel

S960 steel is an advanced low carbon and low alloy ultra-high strength steel (with a minimum yield strength of 960 MPa) developed by Tata Steel. At present, there is a scarcity of data for laser welding of such a material. In this study, 8 mm thick hot rolled and quenched S960 high strength low alloy (HSLA) steel plates were welded using a 16 kW fibre laser system. The microstructure, microhardness, and tensile properties were characterised, Charpy impact testing and three-point bending testing were carried out, and fracture surfaces were investigated. Preliminary results suggest that the laser welding process can produce single-pass welds which are free of macroscopic defects. The microstructures in the fusion zone and heat affected zone were predominately martensite and some self-tempered martensite, with grain size variation in different sub-zones. The tensile properties of the laser welded joint matched those obtained for the base material, with failure occurring in the base material away from the weld. While the welded joint performed well when subjected to bending, the impact toughness was reduced when compared with that of the base material.     

Design and construction of a high pressure xenon time projection chamber

The design and construction of a 300 1 high pressure xenon gas time projection chamber (TPC) is discussed. This detector has been built to perform a sensitive search for double beta decay of ¹³⁶Xe.     

船用高压组合机械密封装置的设计

水下舰艇武器推进泵的机械密封装置的工作压力波动、使用频率小,并要求可靠性高。根据这些使用要求和技术要求,对高压组合机械密封装置进行研究,分析了关键技术,给出结构设计方法、关键参数的选择以及设计计算方法,并对密封环受力变形问题采用有限元法分析。介绍了专门针对船用高压机械密封进行可靠性试验的试验装置,并对所设计的机械密封装置进行了试验,试验结果表明该密封装置能够很好地满足使用要求。     

Microstructure evolution and mechanical properties at high temperature of selective laser melted AlSi10Mg

In this study,the microstructure and tensile properties of selective laser melted AlSilOMg at elevated temperature were investigated with focus on the interfacial region.In-situ SEM and in-situ EBSD analysis were proposed to characterize the microstructural evolution with temperature.The as-fabricated AlSilOMg sample presents high tensile strength with the ultimate tensile strength(UTS)of~450 MPa and yield strength(YS)of~300 MPa,which results from the mixed strengthening mechanism among grain boundary,solid solution,dislocation and Orowan looping mechanism.When holding at the temperature below 200℃for 30 min,the micro structure presents little change,and only a slight decrement of yield strength appears due to the relief of the residual stress.However,when the holding temperature further increases to 300℃and 400℃,the coarsening and precipitation of Si particles inα-Al matrix occur obviously,which leads to an obvious decrease of solid solution strength.At the same time,matrix softening and the weakness of dislocation strengthening also play important roles.When the holding temperature reaches to 400℃,the yield strength decreases significantly to about 25 MPa which is very similar to the as-cast Al alloy.This might be concluded that the YS is dominated by the matrix materials.Because the softening mechanism counteracts work hardening,the extremely high elongation occurs.     

Sol-gel-derived sensor materials that yield linear calibration plots,high sensitivity,and long-term stability

Novel O2-sensing materials based on spin-coated n-octyltriethoxysilane (Octyl-triEOS)/tetraethylorthosilane (TEOS) composite xerogel films have been synthesized and investigated. These sensors are based on the O2 quenching of tris(4,7-diphenyl-1,10-phenanthroline)ruthenium(II) ([Ru(dpp)3]2+) sequestered within the xerogels. Scanning electron microscopy and luminescence measurements (steady state and time resolved) have been used to investigate the structure of these films and their analytical figures of merit and determine the underlying reasons for their observed performance. The results show that certain [Ru(dpp)3]2+-doped Octyl-triEOS/TEOS composites form uniform, crack-free xerogel films that can be used to construct high-sensitivity O2 sensors that have linear calibration curves and excellent long-term stability. For example, an 11-month-old sensor based on 50 mol % Octyl-triEOS exhibits more than 4-fold greater sensitivity in comparison to an equivalent sensor based on pure TEOS. Over an 11-month time period, the sensitivity of a pure TEOS-based sensor drops by more than 400% whereas a sensor based on 50 mol % Octyl-triEOS remains stable (RSD = 4%).     

热处理对激光选区熔化成型高速钢组织和力学性能的影响EI北大核心CSCD

基于激光选区熔化(selective laser melting,SLM)技术,采用加热打印基板和低功率慢扫描的打印策略,制备了近全致密、低缺陷的高速钢样品;对比分析了固溶淬火及1~4次高温回火等热处理工艺对高速钢显微组织及力学性能的影响。结果表明:SLM极高的熔融/冷却速率产生了细晶奥氏体组织,解决了高速钢中常见的粗大莱氏体组织和网状碳化物问题。固溶淬火处理后高速钢组织由马氏体和残余奥氏体组成。随后在数次高温回火过程中,高速钢逐渐向回火马氏体转变,并析出大量微米级和纳米级MC型碳化物。在马氏体相变强化和MC型碳化物沉淀强化作用下,固溶淬火+3次回火的Tempered-Ⅲ样品硬度60HRC,抗弯强度3621 MPa,弯曲断裂应变为10.1%,获得硬度、强度和韧性匹配较佳的综合性能。继续增加回火次数则导致部分碳化物长大,使得高速钢弯曲断裂应变有所降低。通过SLM技术结合固溶淬火+高温回火,能够充分发挥细晶强化、相变强化和沉淀强化效果,为高强高韧复杂形状高速钢零件的快速制备提供了新途径。     

Microstructure and mechanical properties of high power diode laser (HPDL) treated cast aluminium alloys

The appliance and development of modern technologies in the areas of surface engineering can be extended by laser surface treatment, especially using high power diode laser (HPDL) for remelting, feeding and/or alloying. The purpose of this work was to determine technological and technical conditions for tungsten carbide (WC) ceramic powder feeding into the surface layer of the laser treated Al–Si–Cu cast aluminium alloys with high power diode laser, as well as to investigate the microstructure and ceramic powder particle distribution in the surface layer. Special attention was devoted to monitoring of the layer morphology of the investigated material and on the particle occurred. Light and scanning electron microscopy as well as X‐Ray diffraction were used to characterize the microstructure of the remelted zone. A wide range of laser powers was choose and implicated by different process speed rates. Also one powder in form of tungsten carbide was used for feeding with the middle particle size of 80 µm. As the main findings there was found that, the obtained surface layer is without cracks and defects as well as has a comparably higher hardness value compared to the non remelted material. The hardness value increases according to the laser power used so that the highest power applied gives the highest hardness value in the remelted layer. Also the distribution of the tungsten carbide particles is good, but there are still possibilities for further modelling. The major purpose of this work is to study the effect of a high power diode laser melting on the cast Al–Si–Cu alloys structure to provide application possibilities for automotive and aviation industry.     

激光在垂直度误差测量中的应用

文章介绍了用激光测量垂直度误差的原理和方法，并用千分表进行了对比测量。结果表明，用激光测量垂直度误差，具有测量装置简单、操作方便、测量结果精确度高等优点。采用不同的附件，可实现面对面、面对线、线对线、线对面垂直度误差的测量。     

Linear diffraction grating interferometer with high alignment tolerance and high accuracy

We present an innovative structure of a linear diffraction grating interferometer as a long stroke and nanometer resolution displacement sensor for any linear stage. The principle of this diffractive interferometer is based on the phase information encoded by the ±1st order beams diffracted by a holographic grating. Properly interfering these two beams leads to modulation similar to a Doppler frequency shift that can be translated to displacement measurements via phase decoding. A self-compensation structure is developed to improve the alignment tolerance. LightTool analysis shows that this new structure is completely immune to alignment errors of offset, standoff, yaw, and roll. The tolerance of the pitch is also acceptable for most installation conditions. In order to compact the structure and improve the signal quality, a new optical bonding technology by mechanical fixture is presented so that the miniature optics can be permanently bonded together without an air gap in between. For the output waveform signals, a software module is developed for fast real-time pulse counting and phase subdivision. A laser interferometer HP5529A is employed to test the repeatability of the whole system. Experimental data show that within 15?mm travel length, the repeatability is within 15?nm.     

大尺寸工件量规的公差和设计

研究大尺寸工件量规的公差和设计等有关问题，提出了大尺寸工作量规设计的精度等级法，列举了实例计算，为大尺寸工件量规研究和设计提供了重要资料。     

The hydrostatic extrusion of linear polyethylene at high temperatures and high pressures

An account is given of a series of hydrostatic extrusion experiments which has been carried out on linear polyethylene over a wide range of extrusion temperatures and environmental pressures. The results of pressure-to-pressure hot extrusions, which have been performed on melt crystallised polyethylene and also on pressure crystallised extended chain polyethylene, are discussed, with particular reference to the physical properties of the extruded products.     

退火温度对激光熔化沉积TC31高温钛合金组织与性能的影响

为改善激光熔化沉积TC31高温钛合金力学性能,本文通过光学显微镜、SEM、TEM和力学性能测试的方法研究了退火温度对合金中组织演化行为的影响,及其与合金室温和650 ℃高温力学性能的关系。结果表明:组织中初生α相含量随着退火温度升高而降低,其溶解主要发生在950 ℃以上,980 ℃退火后含量仅为29%。当退火温度超过930 ℃时,初生α相片层宽度明显增加。随着退火温度升高,α/β界面处析出的(Ti, Zr)₆Si₃相尺寸增加,且进入α相片层内部。合金在800~1 000 ℃退火时,合金室温拉伸屈服强度随退火温度升高趋于降低。受相界面析出的硅化物聚合长大及α相片层尺寸增加等因素影响,合金高温屈服强度随退火温度升高先降低后增加。合金经过1 000 ℃退火后,呈现良好的高温性能,其650 ℃下抗拉强度达657 MPa、屈服强度约为466 MPa、延伸率27%。     

Peculiarities of using laser diodes in linear measurements

The position of the emitting region of a laser diode depends on the working current. This phenomenon, as well as the polarization of radiation, may influence the accuracy of linear measurements using such lasers.     

光学计量用高速线阵CCD数据采集系统设计

介绍一种采用高速线阵 CCD 数据采集系统的设计过程。通过一片 MicroChip 公司的在线可编程微控制器对采集系统进行控制,并用标准 RS232 串行接口与外部进行数据通信和控制。在时序逻辑设计中,较好地解决了数据的存储、读取和点像元数据连续监测。实际应用表明该系统能满足光学干涉计量中线阵 CCD 数据采集要求。由于可以对线阵 CCD 进行单点、多点和整块数据的读取处理,因而可适应于不同周期、不同像素数目的线阵 CCD 传感器,以满足多种不同需求。     

Density and viscosity of linear perfluoropolyethers under high pressures

New experimental data on the density and viscosity of linear, unbranched perfluoropolyethers are presented at temperatures from 273 to 333 K and pressures up to 180 MPa. The measurements were carried out by a high-pressure burrette apparatus and a falling-cylinder viscometer. The uncertainties of the measurements are estimated to be less than 0.09% for the specific volume and 2.5% for the viscosity. The P-V data at each temperature are correlated satisfactorily by the Tait equation. The viscosity data are also analyzed and correlated with pressure or molar volume by several empirical and theoretical equations.     

Optimal method of linear regression in laser remote sensing

Remote lidar sensing in the photon-counting mode is now the commonly accepted method for studying atmospheric processes in the lower and free atmosphere. However, when processing signals obtained from lidar measurements, investigators necessarily face the problem of achieving accuracy in reconstructing the atmospheric parameters despite the presence of inhomogeneous noise in the measured signals. We propose an optimal method of linear regression (OMLR) of signals. The accuracy of the the method for the reconstructed signal is estimated. An example of application of the OMLR to the reconstruction of the temperature profile from the data obtained with a Raman lidar at the Siberian Lidar Station of the Institute of Atmospheric Optics (Tomsk, Russia) is given. The proposed method is distinguished by simplicity of interpretation of the criteria used, based on careful adherence to statistical principles. This method is shown to be an efficient auxiliary tool for the processing of measured data.     

Stress curves and mechanical properties of high performance concrete

Abstract

In this research, high performance concrete (HPC) was designed by the minimum void ratio method, and slag and silica fumes partially replaced cement, as well as fly ash replacing about 15% of sand. Stress curves for compressive, splitting and flexure strengths of HPC specimens were measured and indicated the experimental concretes had better pastes to void ratios than control batches ratio N=V_p /V_v =1.3. The result indicates that pozzolanic materials provide not only a chemical strength effect, but also a physical packing effect. The compressive stress curves may keep growing as the concrete ages.     

Hygrothermal and mechanical model of concrete at high temperature

A computational model allowing for the thermohygrometric and mechanical analysis of concrete structures at high temperature by means of the finite element method is presented. The model includes creep coupled with damage and related cross-effects due to hygrothermal behaviour. A comparison between experimental tests performed by Bažantet al. on concrete cylinders at high temperature and the numerical results obtained from the model presented are shown.

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Résumé On présente un modèle pour l’analyse thermohygrométrique et mécanique des structures en béton à haute température au moyen de la méthode des éléments finis. Ce modèle inclut le fluage associé à l’endommagement et les effets reliés au comportement hygrothermique. On présente une comparaison entre des résultats des essais réalisés par Bažantet al. sur des cylindres en béton à haute température et les résultats numériques obtenus du modèle.

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Editorial Note Dr. Carmelo Majorana is a RILEM Senior Member and a corresponding member of TC 114-CCS on Computer Programmes for Creep and Shrinkage Prediction. Prof. Bernhard Schrefler is a RILEM Senior Member.     

Morphology and mechanical property relationship in linear low-density polyethylene blown films

Linear low-density polyethylene (LLDPE) blown films fabricated under two different processing conditions, namely a non-stalk bubble configuration and a stalk bubble configuration, were investigated. Morphological characterization was performed using small-angle X-ray scattering, transmission electron microscopy, infrared dichroism, and differential scanning calorimetry. The findings on crystal orientation characteristics of the films suggest that modification on the widely accepted row orientation model of Keller and Machin may be needed. In comparison to the conventional non-stalk bubble geometry for LLDPE film blowing, the stalk bubble configuration can produce a more randomly orientated lamellar texture, resulting in less anisotropy in mechanical properties and a higher dart impact resistance. A good correlation between mechanical properties and morphological features was found.