Preparation and properties of C/C-SiC brake composites fabricated by warm compacted-in situ reaction

Carbon fibre reinforced carbon and silicon carbide dual matrix composites(C/C-SiC) were fabricated by the warm compacted-in situ reaction.The microstructure,mechanical properties,tribological properties,and wear mechanism of C/C-SiC composites at different brake speeds were investigated.The results indicate that the composites are composed of 58wt%C,37wt%SiC,and 5wt%Si.The density and open porosity are 2.0 g.cm~(-3) and 10%,respectively.The C/C-SiC brake composites exhibit good mechanical properties.The ...     

Tribological properties of SiC/Cu composite at high temperature

SiC/Cu composites were prepared by hot pressing. The high temperature tribological properties of the composites were investigated. XRD, SEM techniques were carried out to characterize the samples. It is found that the friction coefficient of SiC/Cu composites increases with the increasing SiC content. The SiC reinforcement particles are worn down other than removed by pulling out during the wear test. Oxidation of Cu debris leads to the smooth contacting surface. Ring crack is formed under the cyclic wear test. The crack propagates through the damaged matrix and along the brittle interface between SiC particles and Cu matrix.     

纳米填料增强UHMWPE–橡胶水润滑摩擦学性能

为了研究水润滑条件下试验载荷和速度对纳米填料（Nano-SiC）改性超高分子量聚乙烯（UHMWPE）/橡胶复合材料摩擦学性能的影响,通过高温混炼、热压成型制备Nano-SiC辅以聚四氟乙烯（PTFE）填充改性UHMWPE/橡胶复合材料。采用MRH-3型环-块摩擦实验机探究四种不同载荷条件下改性复合材料的摩擦磨损性能,采用光学显微镜（OM）、扫描电子显微镜（SEM）和非接触光学三维轮廓仪对试样微观磨损表面形貌分析,从微观层面探究改性复合材料的摩擦机理。试验结果表明：在定载变速条件下,速度由0.02m/s升到3.59m/s时,改性复合材料的动摩擦系数波动幅度与静摩擦系数均呈现大幅下降趋势,粘-滑现象（Stick-Slip Phenomenon）减弱,摩擦系数波动归于平稳;试验载荷和纳米粒子含量的变化与试样摩擦磨损程度呈负相关,在水润滑条件下,随着纳米粒子含量增加,摩擦系数与磨损率均出现明显降低,填充比例为5%的复合材料摩擦学性能最佳,摩擦系数整体较UHMWPE/橡胶材料降低35%,磨损率降低46.6%,磨损表面形貌也随之发生改变;随着载荷的增加,复合材料的磨损率从1.25×10-6mm3/(Nm)降至0.4×10-6mm3/(Nm)。Nano-SiC的含量与工况载荷压力对摩擦磨损均存在一定影响,即填充适量Nano-SiC的UHMWPE/橡胶复合材料与一定工况压力下的对偶钢环组成的摩擦配副能改善摩擦环境,减轻粘-滑现象,有利于减小材料的磨损。     

载荷对Kevlar/PTFE纤维混杂织物摩擦学性能的影响

采用电子小样织机机织Kevlar/PTFE纤维混杂织物,借助于MMU-5G端面摩擦磨损试验机,激光扫描共聚焦显微镜（CLSM）,考察了Kevlar/PTFE纤维混杂织物在高速、干摩擦时不同载荷下的摩擦磨损性能。结果表明,在转速为300 r/min下,载荷越高,稳态摩擦系数值越低,随着载荷的不断增加,稳态摩擦系数下降趋势变缓;织物磨损深度随载荷增加而增加,但磨损率反而降低,织物的摩擦磨损与织物结构有关,磨损方式主要为磨粒磨损,以及PTFE在法向载荷挤压和摩擦剪切作用下发生塑性变形。     

AlTiC增韧补强氧化铝基陶瓷材料磨擦磨损性能

采用热压烧结方法制备了氧化铝／碳化钛复合陶瓷，对材料的摩擦因数和磨损率进行测量，研究了AlTiC中间合金增韧补强氧化铝陶瓷摩擦磨损行为与机制，探讨了氧化铝基精密结构陶瓷的摩擦磨损特性以及力学性能和微观结构对摩擦磨损特性的影响。结果表明，在室温和干摩擦条件下，滑动摩擦因数随法向载荷和转速的增加有下降趋势，室温下新型氧化铝基复相陶瓷材料的磨损机制以微观切削为主。     

AlTiC增韧补强氧化铝基陶瓷材料磨擦磨损性能

采用热压烧结方法制备了氧化铝/碳化钛复合陶瓷,对材料的摩擦因数和磨损率进行测量,研究了AlTiC中间合金增韧补强氧化铝陶瓷摩擦磨损行为与机制.探讨了氧化铝基精密结构陶瓷的摩擦磨损特性以及力学性能和微观结构对摩擦磨损特性的影响.结果表明,在室温和干摩擦条件下,滑动摩擦因数随法向载荷和转速的增加有下降趋势.室温下新型氧化铝基复相陶瓷材料的磨损机制以微观切削为主.     

Effect of infiltrating Si on friction properties of C/C composites

In order to improve the friction-wear properties of the C/C composites for aircraft brake pairs, the friction behavior of samples with infiltrating Si was investigated. The influence of Si smearing thickness on friction properties was studied in detail. The results show that with the increase of Si smearing thickness and β-SiC content, the friction coefficient reduces from 0. 40 to 0. 30; the linear wear of stators increases from 2. 0 μm to 18. 9 μm per cycle, and that of rotors increases from 1. 4μm to 22. 6 μm per cycle; mass wear of stators increases from 20. 6 mg to 126. 9 mg per cycle, and that of rotors increases from 13. 7 mg to 166. 2 mg per cycle. On the other hand, when a large number of inhomogeneous β-SiC particulates are performed, friction surfaces of the samples flake off layer by layer and many nicks are observed.     

Automatic brush-plating technology for component remanufacturing

An automatic brush-plating system was developed for component remanufacturing. With this system, Ni/nano-alumina composite coatings from an electrolyte containing 20 g/L nano-alumina particles were prepared. Microstructure, surface morphology, microhardness and wear resistance of automatically plated coating and manually plated coatings were investigated comparatively. The results show that the automatically plated coatings are relatively dense and uniform and have lower friction coefficient of 0.089 under lubricant condition, when compared with manually plated coatings with friction coefficient of 0.14. Foundation item: Project(50235030) supported by the National Natural Science Foundation of China; Project(G1999065009) supported by the National Basic Research Program of China     

ZM6镁合金的摩擦性能研究

以ZM6镁合金为试验材料,利用正交试验方法和方差分析方法研究了粗糙度、转速和载荷对摩擦系数影响的权重顺序以及其对摩擦性能的影响.结果表明:各因素对摩擦系数影响的权重顺序依次为粗糙度、转速、载荷; 转速为30 r/min时,摩擦系数随着载荷的增加而增大,随着粗糙度的增大先减小后增大; 转速为45 r/min时,摩擦系数随着载荷和粗糙度的增大均先减小后增大; 转速为60 r/min时,摩擦系数随着载荷的增加而减小,随着粗糙度的增大先增大后减小; 载荷为35 N时,摩擦系数随着转速的增大先增大后减小; 载荷为50 N时,摩擦系数随着转速的增大而增大; 载荷为65 N时,摩擦系数随着转速的增大逐渐减小.     

Effects of Electric Potentials on Tribological Properties of SiC/HT200 Pairs in NaOH Solutions

On a self-developed circular-translation polishing machine, the influence of different electric potentials on the friction coefficient and wear properties of SiC/HT200 friction pair, which contacted as one electrode, were studied in NaOH solutions. The results show that the friction coefficient of SiC/HT200 pair is 0.25 under no externally applied potential; but it decreases to 0.23 while applying +3 V polarization potential on the pair; in contrast, it increases to 0.30 when applying -3 V polarization potential on the pair. And the polished SiC surface under +3 V potential is much smoother, while there are clear ploughing marks and adhesive region on the polished SiC surface under zero and -3 V potential, respectively. The mixed tribo-electrochemical friction model has been proposed and the mechanisms of the electric effects on the tribological properties of SiC/HT200 friction pair in NaOH electrolyte are addressed. Results and discussion show that the anodic passivation technique may be used for hastening the running-in process of SiC/Fe friction pairs, as well as for polishing SiC to increase its materials removal efficiency while maintaining good surface quality.     

GCr15球-盘点接触摩擦副的滑滚摩擦磨损特性研究

选用GCr15钢盘和GCr15球作为摩擦副,在NGY‐6纳米润滑膜测量仪上开展球‐盘点接触摩擦副在润滑状态下的滑滚摩擦磨损实验,研究不同接触应力、钢球转速、滑滚比等参数对摩擦副的摩擦因数、磨损形貌的影响规律．结果表明：当接触应力和钢球转速一定时,摩擦因数随着滑滚比的增大而逐渐增加后达到稳定状态;当滑滚比一定时,摩擦因数随接触应力的增大而逐渐增大;当钢球转速低于300 r／min时,摩擦因数随着钢球转速的增大而减小;当钢球转速高于300 r／min、接触应力大于0．84 GPa时,摩擦因数随着钢球转速的增大而呈增大趋势．Stribeck曲线表明：当滑滚比为0．01时,摩擦副处于流体动压润滑状态;当滑滚比为0．03时,润滑状态随Sommerfield参数的增加而从边界润滑过渡到混合润滑;当滑滚比分别为0．05、0．1、0．3、0．5时,润滑状态为边界润滑．滑滚比较小时,磨损机制以疲劳磨损为主,随着滑滚比的增大,磨损机制转变为磨粒磨损．     

Microstructural characterization and mechanical property of Fly Ash/Al-25Mg composites

Fly ash/Al-Mg composites are fabricated by powder metallurgical method. The morphology and structure of fly ash/A l-Mg composites are characterized by scanning electron microscope （SEM） and X-ray diffraction, respectively. The influences of different fly ash content on the friction and wear behavior of the composites are investigated at a constant sliding velocity of 400 r/min and the worn mechanism of composites is discussed. The results indicate that the friction coefficient is steadily lower than that of Al alloy matrix at the lower fly ash content and loads. For the fly ash/Al-Mg composites, the wear mechanism is characterized as abrasive wear and adhesive wear under small normal load and at low fly ash content, and it is characterized as delamination wear and abrasive wear transferred onto the counterpart under high normal load and at high fly ash content.     

微米氧化铝/尼龙复合材料煤泥润滑条件下滚滑摩擦磨损行为

使用微米氧化铝(Al2O3)为增强剂,以尼龙1010为基体,进行氧化铝/尼龙复合材料在煤泥润滑条件下的滚滑动摩擦磨损实验.通过实验发现,水能降低氧化铝/尼龙复合材料的摩擦系数,但增大了磨损量.煤泥润滑时尼龙1010材料的摩擦系数为0.096;氧化铝/尼龙复合材料的平均摩擦系数为0.089,只有纯尼龙的92.7%.尼龙磨损量是3.32mm3;Al2O3/尼龙复合材料的磨损量平均为15.73mm3;Al2O3/尼龙复合材料的平均磨损量平均是尼龙的4.74倍.     

GF/MoS2改性PTFE密封唇片材料的力学及摩擦学性能

采用玻璃纤维(GF)微粉与MoS₂复合改性聚四氟乙烯(PTFE)密封唇片材料,考察复合材料的力学、干摩擦磨损性能及其磨损机理。结果表明:当GF质量分数为15%时,PTFE/GF试样的回弹率达到最大值92.5%,摩擦因数为0.29,相比纯PTFE有所增加,而磨损率大大降低,仅为1.8×10?6mm3/(N·m);在此基础上,当MoS₂添加量为5%时,PTFE/GF/MoS₂试样的回弹率略有降低,但仍然保持在90%以上,其摩擦因数为0.31,体积磨损率进一步降低到1.25×10?6mm3/(N·m)。磨损面SEM分析表明:纯PTFE呈现出严重的塑性变形和粘着磨损特征,而PTFE/GF主要表现为磨粒磨损行为;适当MoS₂含量的PTFE/GF/MoS₂试样在摩擦过程中磨粒磨损特征消失,仅有非常轻微的粘着磨损行为。     

SiC颗粒增强PTFE基复合材料摩擦磨损特性研究

利用冷压烧结法制备了不同含量的SiC颗粒填充聚四氟乙烯(PTFE)复合材料，采用M-200环块试验机进行摩擦磨损试验，研究了SiC颗粒增强PTFE基复合材料在干摩擦条件下的磨损特性，并利用扫描电子显微镜对复合材料的磨损表面形貌进行了观察，对复合材料的磨损机制进行了分析．结果表明：SiC颗粒增强复合材料的耐磨性能显著提高，但其摩擦系数有所增大；随SiC颗粒含量的增加复合材料的磨损机理由粘着磨损占主导逐渐转变为显微切削占主导；复合材料中增强相SiC颗粒有3种流失形式：整体脱落、磨损、碎裂．     

GF增强尼龙1010复合材料的磨擦学性能研究

制备了玻璃纤维（GF）增强尼龙1010复合材料,在环一块磨损试验机上研究了复合材料的摩擦学性能。结果表明：GF含量对复合材料的摩擦学性能有显著影响,GF质量分数为35％时增强效果较好;随着滑速的增加,GF增强尼龙1010复合材料的摩擦系数和磨损量持续上升。干摩擦下的复合材料磨损以疲劳断裂和粘着为主,且纤维出现磨损、断裂及从基体中剥落的现象。在油润滑下材料向对偶产生轻微的转移,与干摩擦相比复合材料的摩擦系数和磨损量大为降低;水润滑下的尼龙以化学腐蚀磨损和磨粒磨损为主,此时复合材料摩擦系数也有较大程度的降低,但磨损量较干摩擦增大。     

High temperature tribological behaviors of nano-diamond as oil additive

The tribological behaviors of the nano-diamond particles including the nano-diamond and the nano-diamond modified were studied at high temperature using SRV multifunctional test system. The worn steel surfaces were analyzed by means of X-ray photoelectron spectroscopy (XPS). The results show that nano-diamond particles can obviously improve the antiwear and friction reducing properties of the base oil at high temperature and the high load. The friction coefficient of the nano-diamond is very low at 200 °C when the test load is not more than 20 N. This tribological behaviors should attributed to the similarly to “ball bearing” lubrication action of the nano-diamond particles, so the movement between tribological pairs become sliding/rolling. The nano-diamond modified by dimer ester possesses excellent antiwear and friction reducing performance at 500 °C and load 500 N. The tribochemical reaction film between the nano-diamond particles and the renascent wear surface plays dominating lubrication role and the presence of the dimer ester on the rubbing surface can be propitious to form lubrication film containing nano-diamond on the worn surface at high temperature and high load. Foundation item: Project (51489020605JS9105) supported by National Key Laboratory for Remanufacturing     

Wear behavior of Cu matrix composites reinforced with mixture of carbon and carbon nanotubes

In order to improve wear resistance and decrease the cost, carbon and carbon nanotubes reinforced copper matrix composites were fabricated by the power metallurgy method. The effects of carbon (carbon and carbon nanotubes) volume fraction and applied load on the friction coefficient and wear rate under dry sliding of the composites were investigated at room temperature. By scanning electron microscopy (SEM), the worn surfaces and debris were observed, and wear mechanism was also analyzed and discussed. The experimental wear process consists of the run-in, steady wear and severe wear process with the increasing of sliding distance. Both the friction coefficient and wear rate of the composites first decrease and then increase with the increasing of carbon volume fraction. The minimum friction coefficient and wear rate are obtained when carbon is 4.0vol%. The wear mechanisms of the composites change from the adhesive wear and delamination wear to abrasive wear with the increasing of carbon volume fraction. Funded by the National Natural Science Foundation of China (50873047) and the Natural Science Foundation of Gansu Province (3ZS061-A25-039)     

混杂增强AZ91复合材料的制备及其显微组织和性能

采用挤压铸造方法制备了以AZ91镁合金为基体、Al2O3短纤维(Al2O3f)和石墨颗粒(Grp)混杂为增强体的复合材料。观察了不同复合材料的显微组织,测试了其力学性能,并对其摩擦磨损性能进行了研究。结果表明:用此法制备的镁基复合材料增强相分布均匀,与基体结合紧密。硬度随Grp体积分数的增加而降低,Al2O3f的加入能提高复合材料的硬度。抗拉强度和伸长率都随Grp体积分数的增加而减小。Grp体积分数增加,磨损质量损失和摩擦系数都降低。随着摩擦过程的进行,在试样表面逐渐形成一层黑色连续的润滑膜。     

稀土镁合金的摩擦磨损性能

采用MMS-2A型环块式摩擦磨损试验机对稀土镁合金GW103K进行了摩擦磨损试验.试验结果表明:GW103K体积磨损量随着磨损时间和外载荷的增大而增大,当磨损时间超过30min,外载荷超过400N时,体积磨损量增大明显;摩擦因数在0.26~0.28之间变化.对摩擦副环块,转速与体积磨损量成正比,与摩擦因数成反比.