Thermisch‐mechanisches Ermüdungsverhalten der partikelverstärkten Aluminiumknetlegierung EN AW‐6061‐T6 und die Entwicklung von Eigenspannungen im Matrixwerkstoff unter thermisch‐mechanischer Beanspruchung

Thermal mechanical fatigue behaviour of particle reinforced EN AW‐6061‐T6 and development of residual stresses in the matrix material by thermal mechanical loading The behaviour of non reinforced and 15 Vol.‐% α‐alumina particle reinforced wrought aluminium alloy EN AW‐6061‐T6 in thermal mechanical fatigue loading was investigated at different maximum temperatures. The tests were performed in strain controlled mode by means of an electro‐mechanical testing machine. Alternating load deformation and life cycle behaviour either materials were compared. It came out, that the reinforcement leads to an decreasing thermal mechanical fatigue life cycle while keeping constant the maximum temperature and mechanical loading. The two materials showed softening behaviour due to high maximum temperatures of 573 K to 673 K. However, there is an intense scatter of the number of cycles to failure of the non reinforced alloy aggravating the interpretation of the results. On the other hand the thermal mechanical life cycle increases in combination with increasing maximum temperatures. Simultaneously the part of plastic deformation in mechanical loading increases for both materials, while for a constant total strain range the effective maximum and minimum stresses are decreasing. Furthermore, the development of residual stresses in the matrix of the reinforced alloy by thermal mechanical fatigue loading was analysed. It was observed that only small absolute values of residual stresses will be obtained for these loads. Nevertheless, tendencies of mounting tensile residual stresses can be identified in the direction of thermal mechanical fatigue loading and subsequently reduction of the residual stresses.     

Aspects of residual thermal stress/strain in particle reinforced metal matrix composites

The influence of inclusion geometry and thermal residual stresses and strains on the mechanical behaviour of a 20 vol% Al₂O₃ particulate reinforced 6061-T0 Al alloy metal matrix composite is investigated through finite element analysis. The introduction of residual thermal stresses/strains prior to external loading leads to a decrease of the proportional limit, 0.2% offset yield stress and the apparent stiffness. The residual stresses/strains are shown to have a greater effect on the composite behaviour under compressive loading than tensile loading. The residual stresses/strains have little effect on the cyclic behaviour of the composite. In only the second cycle, the difference between the cyclic curves, with and without a thermal history, was 2 MPa. Use of a cube shaped particle, with sharp corners and edges, in the unit cell model led to much greater initial hardening behaviour than spherical inclusions, and therefore a greater 0.2% offset yield stress due to stress/strain localisation at the particle corners and edges. This results in regions of constrained plasticity and high stress triaxiality in the matrix around the particle, producing improved load transfer in the composite. It is shown that inclusion aspect ratio, in the range of 0.5–2.0, has an impact on the yield stress. A minimum yield stress occurred at an aspect ratio of approximately 0.9 with significant increases on either side of this point. The influence of residual stress/strain had a similar effect throughout the aspect ratio range except tensile loading, following thermal treatment, on unit cells with inclusion aspect ratios greater than 1.5 resulted in the highest yield stresses.     

Fatigue behaviour of carbon fibre-reinforced aluminium laminates

A new hybrid composite (CARALL), consisting of thin layers of carbon fibre/ epoxy prepreg sandwiched between aluminium sheets, has been developed. It is shown that this class of materials offers higher modulus, higher tensile strength and lower density than 2024-T3 alloy in the longitudinal direction. Under tension-tension fatigue loading, the hybrid laminates showed superior fatigue crack propagation resistance in the longitudinal direction, which may be attributed to the bridging effect imposed by the intact fibres in the crack wake. It has also been shown that the effectiveness of fatigue crack growth reduction increases with the thickness of the carbon fibre/epoxy layer. The resistance to fatigue crack propagation can be further improved by introducing compressive residual stresses in the aluminium layer by postcure stretching the laminate in the plastic region of the aluminium alloy.     

SiC whiskers-aluminium 6061 composite: microstructure and mechanical characteristic anisotropy

The correlation has been studied between the microstructure and the tensile and compressive properties of composite extruded bars of aluminium 6061 alloy matrix reinforced with silicon carbide whiskers. The material was tested before and after being subjected to T6 heat treatment. Different degrees of alignment and breakage in the whiskers and the texture of the metal matrix were observed, corresponding to different ratios of extrusion. The material also showed marked anisotropy in its mechanical characteristics: its compressive strength in the longitudinal direction was considerably higher than in the transverse direction.     

Microstructure,tensile properties and fracture behaviour of Al2O3 particulate-reinforced aluminium alloy metal matrix composites

The tensile deformation and fracture behaviour of aluminium alloy 2014 discontinuously-reinforced with particulates of Al₂O₃ was studied with the primary objective of understanding the influence of reinforcement content on composite microstructure, tensile properties and quasi-static fracture behaviour. Results reveal that elastic modulus and strength of the metal-matrix composite increased with reinforcement content in the metal matrix. With increase in test temperature the elastic modulus showed a marginal decrease while the ductility exhibited significant improvement. The improved strength of the Al-Al₂O₃ composite is ascribed to the concurrent and mutually interactive influences of residual stresses generated due to intrinsic differences in thermal expansion coefficients between constituents of the composite, constrained plastic flow and triaxiality in the soft and ductile aluminium alloy matrix due to the presence of hard and brittle particulate reinforcements. Fracture on a microscopic scale initiated by cracking of the individual or agglomerates of Al₂O₃ particulates in the metal matrix and decohesion at the matrix-particle interfaces. Failure through cracking and decohesion at the interfaces increased with reinforcement content in the matrix. The kinetics of the fracture process is discussed in terms of applied far-field stress and intrinsic composite microstructural effects.     

Development of Some Fundamental Research of SiC_W/Al Composites in HIT PartⅠ Microstructure and SiC/Al Interface of SiC_W/Al Composites

The microstructure of SiC whisker reinforced aluminium alloy (SiC_w/Al) composite is reviewed,andthe SiC-Al interface in SiC_w/Al composite is especially discussed,The main contents aremorphology of the aluminium matrix in SiC_w/Al composite;microstructures and defects of SiCwhiskers in SiC_w/Al composite and bonding mechanisms of the SiC-Al interface in SiC_w/Al com-posite.     

Influence of heat treatment processes on fatigue performance of particle reinforced aluminium alloys

Abstract

The fatigue performance of particle reinforced metal matrix composites improves as the matrix strength is increased. However, the heat treatment required for high matrix strength induces residual stresses into the material, which need to be balanced against potential distortion during machining of components. This paper reports results showing the fatigue behaviour of a 2124 aluminium alloy reinforced with 25 vol.-% of silicon carbide particles. The effect of quench medium on tensile and rotating bend fatigue strength is reported. Results are correlated with residual stress profiles measured in quenched plates of the material.     

Tensile properties and thermal expansion of discontinuously reinforced aluminium composites at subambient temperatures

The effects of temperature on the mechanical properties and thermal expansion of two discontinuously reinforced aluminium composites have been determined over the range 300–100 K. Silicon carbide particulate-reinforced 2009 and 6092 aluminium alloys were studied by tensile testing, in which both longitudinal and transverse strains were recorded, and by thermal expansion measurements. The test results clearly show that cooling to 100 K induces plastic flow in the aluminium alloy matrices due to the thermal expansion difference between aluminium and silicon carbide. At very low temperatures, the linear region of the stress-strain curve is greatly reduced or eliminated and the Poisson’s ratio, ν, increases. For the higher yield strength 2009 matrix composite, ν increases from a room-temperature value of 0.28 to 0.35 at 100 K. For the lower-strength 6029 matrix composite, ν increases from a room-temperature value of 0.33 to a value of 0.5 at 100 K. A Poisson’s ratio of 0.5 is the value characteristic of plastic flow in an incompressable material. Changes in yield strength, Young’s modulus and thermal expansion with decreasing temperature are also consistent with thermally induced plastic flow in the composite matrix. This revised version was published online in November 2006 with corrections to the Cover Date.     

Predicting crack initiation in composite material systems due to a thermal expansion mismatch

Residual stresses due to curing and thermal stresses due to differences between the thermal expansion coefficients of the matrix and fiber may have a major effect on the micro-stresses within a composite material system and must be added to the stresses induced by the external mechanical loads. Such microstresses are often sufficient to produce micro-cracking even in the absence of external loads, example during the cooling process. In this investigation, a micro-mechnics approach is used in which the fibers of a composite material system are modeled as cylindrical inclusions that are embedded into a matrix plate. The model is then used to predict, analytically, the residual stresses due to a thermal expansion mismatch, e.g. during a cooling process. Additionally, some critical effects due to a load transverse to the direction of the fibers are examined. The analysis provides a better understanding of how residual stresses are developed and how they may be controlled in material systems where small strains are present. Moreover, the results are used to identify locations of possible crack failure and to derive a fracture criterion for crack initiation at the local level. Comparison with experimental evidence for matrix cracking in intermetallic composites caused by thermal expansion mismatch shows a good agreement. This revised version was published online in July 2006 with corrections to the Cover Date.     

Artgleiche und artverschiedene reibrührgeschweißte Verbindungen aus AA2124+25 % SiC und AA2024

Similar and dissimilar friction stir welded joints made from AA2124+25 % SiC and AA2024 An aluminium matrix composite (AMC) consisting of an AA2124 matrix reinforced by 25 vol.% SiC particles was used to produce similar AMC+AMC and dissimilar AMC+2024‐T3 joints by friction stir welding. When the particle reinforced composite was located on the retreating side, material mixing was less intense for dissimilar joints. Nevertheless, a higher strength has been determined for this arrangement due to a hook‐like interlocking of both materials. Tensile test and S‐N fatigue behaviour is shown to be compromised by alignment of the reinforcement particles perpendicular to loading direction already in the particle reinforced base material. Welding residual stresses were determined through the cut‐compliance method in terms of stress intensities acting at the crack tip. The underlying residual stress distribution in the un‐cracked structure was calculated by the weight function method. Longitudinal tensile residual stresses were found to be higher in the monolithic material as compared to the particle reinforced composite. This held true both for similar and within dissimilar joints. Growth behaviour of cracks crossing the joint line was described and correlated with residual stresses for similar joints.     

SiCw／Al复合材料拉伸强化机理研究

对压铸法制造的ＳｉＣｗ／Ａｌ复合材料拉伸强化机理进行了研究，分析了晶须尺寸和基体合金对Ｓｉ／Ｃｗ／Ａｌ复合材料拉强度的影响规律，随晶须长径比的增大，复合材料拉伸强度提高。ＴＥＭ观察发现复合材料的基体合金中晶粒细小，并且位错密度较高，使基体合金与没有晶须增强的相同分成铝合上比强度有较大提高，这是复合材料高度较原高，使基体合金与没有晶须增强的相同成分铝合金相比强度有较大提高，这是复合材料高强度的原因之     

Finite-element modeling of initial matrix failure in CFRP under static transverse tensile load

The failure of transversely loaded unidirectional CFRP has been investigated by the use of mechanical and thermo-mechanical test methods and finite-element analysis. The case considered here is characterized by a high interfacial strength between fiber and matrix, so that matrix failure governs the fracture process of the composite. On the basis of the experimental results, the parabolic and other failure criteria were applied to the FE calculations. The failure dependence of the resin on the actual stress state could be described. Furthermore, the influence of thermal residual stresses on the initial matrix failure has been investigated, and the actual stiffnesses and thermal expansion changes of the epoxy resins and the composites as a function of temperature have been determined experimentally. The results of the mechanical and thermo-mechanical tests performed on the pure resins and on the composites were incorporated into a finite-element analysis and compared with the transverse tensile properties of the composite laminates. In the FE analysis, the local fiber-volume fraction was varied over a wide range in order to investigate its influence on the thermal residual stresses and transverse composite strength. The results could explain the low strain to failure of transverse laminates under tensile loading.     

Distortion Behaviour and Mechanical Properties of AlCu4Mg1 Sheet Components after High‐Pressure Gas Quenching in Comparison to Liquid Quenching

The quenching process after solution annealing of age hardenable aluminium alloys is necessary for an improvement of the mechanical properties, but also tends to result in distortion, especially in thin or complex shaped parts, and requires a costly reworking. High‐pressure gas quenching can reduce distortion compared to liquid quenching, because of the better temperature uniformity during quenching. A determination of the distortion behaviour of different serial parts of the aluminium wrought alloy 2024cl (AlCu4Mg1,clad) points out, that high‐pressure gas quenching offers predominantly excellent values regarding the dimensional accuracy after quenching compared to liquid quenchants. In comparison to the conventional heat treatment, similar values in strength, hardness and electrical conductivity have been determined after gas quenching and aging of different aluminium alloys (2024, 6013, and 7075), Furthermore, the residual stresses have been investigated and could be clearly reduced after gas quenching.     

Microstructure,tensile properties and fracture behaviour of an Al-Cu-Mg alloy 2124

The microstructure, tensile properties and fracture behaviour of aluminium alloy 2124 were studied. Detailed optical and electron microscopical observations were made to analyse the as-received microstructure of the alloy. It is shown that microstructural characteristics have a profound influence on tensile properties and quasi-static fracture behaviour of the alloy. Tensile test results indicate that the alloy has uniform strength and ductility in the longitudinal and transverse orientations. The elongation and reduction in area are higher in the transverse direction of the extruded plate. No change in fracture mode was observed with direction of testing. Fracture, on a microscopic scale, was ductile, comprising of void nucleation, growth and coalescence. The fracture process is discussed in terms of competing influences of intrinsic microstructural features, deformation characteristics of the matrix and grain-boundary failure.     

In situ synthesis of porous ceramics with a framework structure of aluminium borate whisker

New porous ceramics with a framework structure of aluminium borate (9Al2O3 · 2B2O3) whiskers, in which the whiskers are distributed uniformly and randomly, can be synthesized in situ by firing of a green powder compact of a mixture of aluminium hydroxide, boric acid and an additive of nickel oxide above 1100°C. During firing, the whiskers of aluminium borate grow in situ in the compact, and are bonded together by sintering. The porous aluminium borate consists solely of whiskers, has a porosity of 85%–50%, which corresponds to a volume fraction of whiskers of 15%–50%, and a flexural strength of 2.2–56.1 MPa. Because the whiskers are strongly bonded to other whisker(s), the problem of whiskers scattering, that can be an inhalation hazard, is solved. The aluminium alloy matrix composite using this porous aluminium borate as reinforcement was fabricated by the squeeze-casting method. The tensile strength of the composite material with a whisker volume fraction of 20% can be improved by up to about 90% compared with the unreinforced matrix alloy at 350°C. © 1998 Chapman & Hall     

Interfacial reaction and its effect on strength of Al18 B4O33 /Al composites

Abstract

Aluminium alloy 6061, AC8A, Al–1Mg, Al–9Cu and pure aluminium composites reinforced with aluminium borate whiskers were fabricated by a squeeze casting process. The interfacial reaction in the composites and its effect on the bending strength are discussed, together with the results from SEM, TEM, and X-ray diffraction. A slight interfacial reaction is favourable for composite strength as it has the effect of anchoring the whiskers. A T6 treatment can enhance the strength of an Al–9Cu matrix composite, but is not efficient for magnesium containing 6061 and AC8A matrix composites. Furthermore, if heated at temperatures higher than 793 K for a long time, the composite strength drops rapidly owing to whisker damage and shortening during the interfacial reaction. It is suggested that the interface in an Al₁₈ B₄O₃₃ /Al alloy composite is stable below 623 K which is the temperature requirement for automobile engine components.     

Influence of heat treatment on the tensile properties and fracture behaviour of an aluminium alloy-ceramic particle composite

The tensile deformation and fracture behaviour of aluminium alloy 2124 reinforced with different amounts of silicon carbide particulates was studied, in the as-extruded and heat-treated conditions, with the objective of investigating the influence of heat treatment and composite microstructural effects on tensile properties and quasi-static fracture behaviour. Results indicate that for a given microstructural condition, the elastic modulus and strength of the metal-matrix composite increased with reinforcement content in the metal matrix. For a given volume fraction of reinforcement, the heat-treated composite exhibited significantly improved modulus and strength-ductility relationships over the as-extruded counterpart. The increased strength of the Al-SiC composite is attributed to the competing and synergistic influence of strengthening precipitates in the matrix metal, residual stresses generated due to intrinsic differences in thermal expansion coefficients between components of the composite and strengthening from constrained plastic flow and triaxiality in the ductile matrix due to the presence of brittle reinforcement. Fracture on a microscopic scale is initiated by cracking of the individual or clusters of SiC particles present in the microstructure. Particle cracking was dominant for the as-extruded composite microstructure. For both the as-extruded and heat-treated conditions, particle cracking increased with reinforcement content in the matrix. Final fracture of the composite resulted from crack propagation through the matrix between clusters. Although these composites exhibited limited ductility on a macroscopic scale, on a microscopic scale the fracture mechanism revealed features reminiscent of ductile failure.     

On the local elastic–plastic behaviour of the interface in titanium/silicon carbide composites

The purpose of this study is to conduct a high-resolution nonlinear finite element analysis of the elastic–plastic behaviour of titanium/silicon carbide composites subject to transverse loading. This class of metal matrix composites is designed for the next generation of supersonic jet engines and deserves careful assessment of its behaviour under thermo mechanical loads. Three aspects of the work are accordingly examined. The first is concerned with the development of a representative unit cell capable of accurately describing the local elastic–plastic behaviour of the interface in metal matrix composites under thermal and mechanical loads. The second is concerned with the determination of the influence of mismatch in the mechanical properties between the inhomogeneity and the matrix upon the induced stress fields and the plastic zone development and its growth. The third is concerned with unloading and the role played by the interface upon residual stresses. It is found that the maximum interfacial stress in the matrix appears in the case involving cooling from the relieving temperature with subsequent applied compressive loading. It is also found that the mismatch in mechanical properties between the matrix and the inhomogeneity introduces significant changes in the stress distribution in the matrix. Specifically, it is observed that the maximum radial and tangential stresses in the matrix take place at the interface. The plastic deformation of the matrix leads to a relaxation of these stresses and assists in developing a more uniform interfacial stress distribution. However, the matrix stresses and the resulting equivalent plastic strains still reach their maximum values at that interface. The results show similarities in the patterns of the interfacial stress distribution and plastic zone development for all ranges of fibre volume fractions and loading levels examined. However, they also show marked differences in both the magnitude and patterns of matrix stress distribution between the adjacent inhomogeneities as a result of interaction effects between the fibres.     

Fabrication of 6061 aluminium alloy/Al18B4O33(w) composite by using sol–gel alumina binder

Abstract

For fabrication of aluminium borate whisker (Al₁₈B₄O_33(w)) reinforced 6061 aluminium alloy composites, a sol–gel alumina binder instead of conventional silica binder was used for preparing the whisker preforms of the squeeze cast composites. The results show that a sound whisker preform and a uniform composite can be made by this method. Unlike the reactive silica binder, the sol–gel alumina binder is rather stable throughout the entire high temperature fabrication process. Under appropriate conditions, the sol–gel alumina binder can also serve as a thermal barrier for minimising interfacial reactions between aluminium borate whiskers and the matrix alloy. With a binder concentration of 0.6 mol L^-1, the ultimate tensile strength of the composite is as high as 277.6 MPa at room temperature and moderate at elevated temperatures. The tensile fracture of the alumina bound composite shows a mixed mode of dimple fracture and interface debonding.     

Exceeding average rule of mixtures stiffness in composite materials with interconnected fibres as reinforcement

Abstract

In the present study, a galvanised iron wire mesh structure of two different types was used to reinforce aluminium alloy 1050. The composite was synthesised using conventional casting followed by hot extrusion. Microstructural characterisation of the composite specimens showed good interfacial integrity between the matrix and the reinforcement wire. Thermomechanical analysis demonstrated that the average coefficient of thermal expansion of the composites was decreased below the values predicted by theoretical models. Tensile tests conducted on the composite specimens revealed that the average elastic modulus of the composites exceeded the rule of mixtures predictions. The average values of 0.2 yield strength and ultimate tensile strength of the composites were found to be higher than those of the monolithic aluminium alloy irrespective of a low volume fraction 0.049 of reinforcement. This unusual variation in the properties clearly reflects the uniqueness of using interconnected wires as reinforcement in the metallic matrix. An attempt is made in the present study to rationalise particularly the tensile behaviour, especially the stiffness of the composite material, according to the type of reinforcement preform in the aluminium alloy matrix.