共查询到18条相似文献,搜索用时 93 毫秒
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New models for describing hydrodynamics and mass transfer performance in supercritical fluid extraction columns were proposed.Those models were proved by experimental data,which were obtained in supercritical fluid extraction packed column,spray column and sieve tray column respectively.The inner diameter of those columns areΦ25mm,These experimental systems include supercritical carbon dioxideisopropanol-water and supercritical carbon dioxide-ethanol-water,in which supercritical carbon dioxide was dispersed phase,and another was continuous phase.The extraction processes were operated with continuous countercurrent flow.The predicted values are agreed well with experimental data. 相似文献
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超临界流体萃取技术的应用及研究进展 总被引:7,自引:0,他引:7
超临界流体萃取技术近年来被广泛应用于中草药、食品、香料、化工及环境保护等领域。介绍了超临界流体萃取技术与传统的萃取方法相比所具备的优势及其发展前景。 相似文献
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超临界流体萃取技术的发展及应用 总被引:1,自引:0,他引:1
超临界流体萃取技术(Supercritical fluid extraction technology,简称:SFE)是利用流体在超临界状态下具有选择性溶解能力的特性对不同的物料进行分离。超临界流体萃取技术在天然有机物质的提取方面有着巨大的优势。随着现代化工业工程技术的发展,超临界流体萃取技术在食品、石油、化工、医药等各个领域显示出广阔的发展前景。 相似文献
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超临界流体抽提技术是一项新型、绿色、环保的技术,超临界流体抽提技术应用于煤焦油研究的主要目的分为超临界条件下提取其中成分,使煤焦油轻质化,本文介绍了超临界流体抽提技术应用于煤焦油的研究进展,指出了今后的研究方向. 相似文献
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A preparative-scale supercritical fluid extraction/supercritical fluid chromatography (SFE/SFC) procedure has been developed
for the removal of oil from corn bran to obtain fractions enriched with free sterols and ferulate-phytosterol esters (FPE).
Operational parameters from an analytical-scale supercritical fluid fractionation technique were translated to and optimized
on a home-built, preparatory-scale SFE/SFC apparatus. SFE was performed at 34.5 MPa and 40°C using supercritical carbon dioxide.
These conditions did not result in exhaustive extraction of the corn bran, but yielded about 96% of the available oil. SFC
was conducted in three steps, followed by reconditioning of the sorbent bed. Preparative-scale SFE/SFC of corn bran produced
a fraction enriched greater than fourfold in free sterols and 10-fold in FPE, suggesting that such a scheme could be used
industrially to produce a functional food ingredient. 相似文献
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Willam E. Artz Robert M. Sauer Jr. 《Journal of the American Oil Chemists' Society》1992,69(4):309-313
An improved supercritical fluid micro-extraction cell of increased reliability was designed for on-line supercritical fluid
extraction and chromatography (SFE/SFC) of food and other lipid-related samples. The key components in the modified cell include
a Swagelok stainless steel reducing union with a dual ferrule as the cell, with polyetherether-ketone (PEEK) ferrules and
nuts to connect the cell to the control valve. The new cell did not leak under all conditions examined (100–500 atmospheres,
40–80°C), even after numerous extractions (>250). The quantitative performance of the cell was evaluated with fatty acid standard
solutions, technical grade fatty acid sources and wheat flour. The percent relative error (%RE) for the fatty acid standards
and technical-grade fatty acid samples was ≤6.0% for oleic, linoleic and linolenic acid. The %RE for oleic and linoleic acid
in the whole-wheat samples was ≤10%. The results demonstrate that the new extraction cell can be used for quantitative extractions
and that the sensitivity of the SFE/SFC technique is excellent. Similar SFE/SFC methods could prove useful in studying the
interaction of free fatty acids with various food components such as enzymes, amylose and proteins. 相似文献