镍基合金涂层的加工工艺研究

通过对镍基涂层的机加工性能分析，选择合理的切削用量和刀具几何角度，经实验验证表明使用国产硬质合金刀片ＹＤ０５可以加工镍基涂层，并达到以车代磨的效果。     

动态再结晶晶粒尺寸同Zener—Holloman参数间的理论模型

本文推导了稳定动态再结晶晶粒尺寸同形变Ｚ参数间的理论模型，证实了Ｓｅｌｌａｒｓ等人的经验公式Ｄ＝ＣＺ＾－ｎＤ。研究表明，Ｃ参数为几乎不受温度影响的常数。建立了ｎＤ的预测模型，ｎＤ理论值同实验值相一致。     

镍基合金——碳化铬复合涂层材料界面扩散研究

对真空熔烧法制作的镍基合金－－碳化铬复全涂层界面两侧合金元素的扩散问题,提出了电子探针与最小二乘法相结合的研究方法,结果证明,界面扩散是决定复合材料界面结合状况的关键。     

镍基合金喷熔层组织及其抗高温冲蚀性能的研究

用氧—乙炔火焰喷熔法制取镍基合金喷熔层,通过高温冲蚀模拟试验机对镍基合金喷熔层和其他表面强化层进行高温冲蚀磨损对比试验。结果表明:镍基介金喷溶层具有最佳的抗高温冲蚀性能,比20钢提高4～5倍,其冲蚀行为表现为塑性材料特征,最大冲蚀率攻角约为30°。     

超低碳贝氏体钢形变奥氏体静态再结晶行为研究

在MMS-200热模拟试验机上进行了双道次热压缩变形实验,研究了超低碳贝氏体钢的静态再结晶软化规律.利用应力补偿法（0.2%）计算了不同形变温度下的静态再结晶软化率。试验结果表明：形变温度和形变道次间隔时间对超低碳贝氏体钢的静态再结晶行为影响非常大。根据相关试验数据以及静态再结晶动力学方程,经计算得出超低碳贝氏体钢的静态再结晶激活能为292.42 kJ/mol。     

镍基合金——碳化钨复合涂层脆性的测估

采用显微硬度法结合声发射技术，对在４５钢表面上用真空熔烧法制得的镍基合金－－碳化钨复合涂层的脆性进行了测估，结果表明，这种涂层的声发射能量累积计数值Ｅｎ与所加坟入负荷Ｐ之间存在线性关系；可用Ｅｎ－Ｐ直线Ｋ来评价涂层的脆性，不同在碳化钨含量的涂层的Ｅｎ－Ｐ直线的Ｋ不同；Ｋ值愈大，涂层的脆性愈大。     

稀土对镍基合金耐蚀性能的影响

根据腐蚀理论，设计了一种含稀土元素的镍基耐蚀合金，利用SEM、OM、XRD等技术研究了合金的特性．探讨了稀土元素对镍基合金性能的影响．试验结果表明，加入稀土元素可以获得致密化程度较高、分布均匀的组织，改变了试样表面的微观结构，从而提高了镍基合金的耐磨耐蚀性能。     

改型In718镍基合金析出相的热力学模拟计算

采用Thermo-Calc热力学计算软件与相应的镍基高温合金数据库,计算了改型In718合金在960~1020℃固溶加二次时效后可能析出的平衡相,研究了不同固溶温度的变化对主要析出相的影响,分析了各相的析出规律,为进一步调整合金成分,改善合金力学性能提供了理论依据.     

Static recrystallization behavior of Inconel 718 alloy during thermal deformation

The softening behavior of Inconel 718 alloy at different temperatures was studied using twostage interrupted compression method on Gleeble1500D thermal stimulator, and the 2% offset method was applied to analyze the experimental dates. Finally, the static recrystallization fraction was obtained. At the same times, optical microscope(OM) and transmission electron microscopy(TEM) were employed to investigate the microstructure characteristic. The experimental results showed that the recrystallization was more sensitive to temperature than holding time. The recrystallization process finished quickly above 1 050 ℃, and significantly prolonged below 1 025 ℃. Additionally, the dynamical model of static recrystallization follows the Avrami equation. The nucleating mechanism was characterized by bulging at grain boundary and merging of sub-grain.     

The Effects of Aging Precipitation on the Recrystallization of CuNiSiCr Alloy

The interaction between precipitation and recrystallization and its effect on the properties of the Cu-Ni-Si-Cr alloy during aging were discussed. The results show that the deformation results in much more dispersed precipitation of the phases. The precipitations have accelerating or retarding effects on the recrys allization. On the formation and growth of recrystallization, the precipitated phases are coarsed or dissolved in front of grain boundaries following a re-precipitation in the recrystallization area.     

Modeling of microstructural evolution during dynamic recrystallization in coarse Nb microalloyed austenite

The aim of the current study was to investigate the microstructural evolution during dynamic recrystallization in coarse Nb microalloyed austenite in thin slab direct rolling （TSDR） processing. A model was developed to predict the change of the austenite grain size during the dynamic recrystallization, by using the law of mixtures. The equations initially developed for partial static recrystallization were used for partial dynamic recrystallization, by adjusting the value of the constant. The results show that the change of the austenite grain size can be reasonably described by using the equations developed according to the law of mixtures.     

Dynamic recrystallization during hot torsion of Al-4Mg alloy

Binary Al-4Mg alloy have been deformed by hot torsion at 300-500℃ and strain rates of 0.006-1.587 s of 5.5. The specimens were annealed in vacuum for 1.5 h at 500℃ and then water quenched. The study indicates that the dynamic recrystallization occurs during hot torsion of Al-4Mg alloy in a certain range of Z parameter (Zener-Hollmon Parameter), i.e. 19.3 ≤ InZ ≤ 24.8. Increasing the strain rate at higher deformation temperature or reducing the strain rate at lower deformation temperature accelerates the occurrence of dynamic recrystallization in the alloy.     

Simulation of dynamic recrystallization for aluminium alloy 7050 using cellular automaton

The prediction of microstructure evolution plays an important role in the design of forging process. In the present work, the cellular automaton (CA) program was developed to simulate the process of dynamic recrystallization (DRX) for aluminium alloy 7050. The material constants in CA models, including dislocation density, nucleation rate and grain growth, were determined by the isothermal compress tests on Gleeble 1500 machine. The model of dislocation density was obtained by linear regression method based on the experimental results. The influences of the deformation parameters on the percentage of DRX and the mean grain size for aluminium alloy 7050 were investigated in details by means of CA simulation. The simulation results show that, as temperature increases from 350 to 450 °C at a strain rate of 0.01 s⁻¹, the percentage of DRX also increases greatly and the mean grain size decreases from 50 to 39.3 μm. The mean size of the recrystallied grains (R-grains) mainly depends on the Zener-Hollomon parameter. To obtain fine grain, the desired deformation temperature is determined from 400 to 450 °C. Foundation item: Project(2005CB724105) supported by the Major State Basic Research Program of China; Project(IRT0549) supported by Program for Changjiang Scholars and Innovative Research Team in University     

电磁水平连铸1560镍基合金的组织与性能研究

为提高1560镍基合金圆形铸锭的质量,采用电磁水平连铸方法对其进行生产实验,并对圆锭及其坯料再进一步轧制和冷拉所生产系列棒线材产品的组织与性能进行了研究。结果表明,该方法生产的1560镍基合金电磁铸锭的芯部由中心等轴晶组成,其溶质元素偏析程度明显降低,且常规水平连铸过程中常见的芯部裂纹、缩孔和疏松等缺陷也得到有效消除。该方法不仅取消了传统工艺中的铸坯退火、锻造及打磨等工序,而且还缩短了工艺流程,其产品成材率也由传统工艺时的70％提升到90％以上。     

Incoloy 825镍基合金的低周疲劳行为

为了研究Incoloy 825镍基合金的循环应力响应行为和低周疲劳行为,在室温和760℃下进行外加总应变幅控制下的疲劳实验,确定了合金在不同温度下的应变疲劳参数.利用透射电子显微镜和扫描电子显微镜分析了合金疲劳变形后的位错亚结构与断口形貌.结果表明,室温下合金呈现先循环硬化后循环软化的特征,而在760℃下合金则呈现先循环硬化后循环软化或循环稳定的特征.在不同温度下合金的塑性应变幅、弹性应变幅与断裂时的载荷反向周次之间均呈现单斜率线性关系,并分别服从Coffin-Manson和Basquin公式.在室温和760℃下合金的低周疲劳变形机制主要为平面滑移,且疲劳裂纹均以穿晶方式萌生和扩展.     

4J29膨胀合金晶粒长大倾向的研究

针对在电子器件中常作为密封材料的4J29合金在生产时出现粗大晶粒造成工件开裂问题,采用热处理和单因素优选实验方法研究4J29合金的再结晶温度、预先变形率与晶粒度之间的关系。研究表明,4J29膨胀合金晶粒聚集长大是由大于70%预先变形率所造成。在实际生产中尽可能采用合理的预先变形率可以提高材料的再结晶温度和二次再结晶温度,可以防止合金晶粒聚集长大,从而保证了工件质量和使用性能。     

Kinetics of recrystallization for twin-roll casting AZ31 magnesium alloy during homogenization

The kinetics of recrystallization for twin-roll casting AZ31 magnesium alloy with different thicknesses during homogenization was analyzed.It is shown that fine grains are first formed at the boundaries of deformed bands in the twin-roll casting slab.The recrystallized grains with no strain are gradually substituted for the deformed microstructure of twin-roll casting AZ31 magnesium alloy.The incubation temperature and time for the recrystallization of a twin-roll casting AZ31 magnesium alloy strip with a thickness of 3 mm are lower and shorter than those of the 6-mm thick strip,respectively.The 3-mm thick twin-roll casting magnesium alloy has finer grains than the 6-mm thick strip.The activation energies of recrystallization for twin-roll casting AZ31 magnesium alloy slabs with the thickness of 3 and 6 mm are 88 and 69 kJ/mol,respectively.The kinetics curves of recrystallization for twin-roll casting AZ31 magnesium alloy were obtained.