共查询到20条相似文献,搜索用时 125 毫秒
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研究了共电沉积法生产铝镁钪合金过程,采用连续脉冲—示波器法监控电解过程中的分解电压、电流强度等参数的计时变化。结果显示,实际分解电压随电流强度的增强而变大,加入0.5%MgO-0.5%Sc_2O_3可使分解电压平均减小0.3V;实际分解电压随着极距的增大而变大,后期增势渐缓,而升高温度可降低实际分解电压;根据实际分解电压随着电解时间的变化判断出加料周期为23min;在720℃、极距3cm、电流强度3A时,电解2h成功制备出Al-2.71%Mg-0.63%Sc合金。 相似文献
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Sm2Fe17是一种性能优异的永磁材料(SmFeN)的前驱体。用循环伏安法研究了三价钐(Sm(Ⅲ))和二价铁(Fe(Ⅱ))在含甘氨酸的水溶液中的电化学行为,在Pt电极上,Fe(Ⅱ)一步还原为Fe,Sm(Ⅲ)能被Fe(Ⅱ)诱导共沉积。在水溶液中成功电沉积出Sm-Fe合金。研究了pH和电流密度对镀层组分的影响,在电流密度为40mA.cm-2时,随着pH升高,镀层中Sm含量增加,在pH=4.5时,随着电流密度的增加,镀层中Sm含量增加。电子显微镜(SEM)显示镀层表面是紧密一致的。镀层在热处理前是非晶态Sm-Fe合金和微晶Fe的混合相,经750℃热处理后,镀层转化为Fe和Sm-Fe合金的混合相。 相似文献
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综述了电沉积镍钨合金的研究现状,分析了镀液成分和工艺条件对电沉积镍钨合金镀层的组成及其性能的影响,并介绍了镍钨合金镀层的各种性能,最后指出了今后的发展趋势和研究意义所在。 相似文献
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电沉积钨钴合金的工艺研究 总被引:1,自引:0,他引:1
研究了W-Co合金电镀工艺,讨论了电流密度、主盐浓度、阳极、pH值和温度对电镀的影响,并对在不同基体材料上的电镀钨合金的难易程度进行了比较。结果表明,电流密度在4~6A/dm2,镀液的pH=4~5.5,室温下就能获得较好的合金镀层。在不同基体金属上电镀W-Co合金时,基体金属的电位要正于镀层金属的电位,才能获得结合力良好的镀层。 相似文献
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以聚氨酯泡沫树脂为基体,采用化学镀、电沉积、热解和氢气还原的方法制备出网状结构的泡沫Ni-Mo合金。对该泡沫合金的形貌、镀液组分与合金组分的关系和合金的抗拉强度、抗腐蚀性、高温抗氧化性进行了分析研究。试验结果表明:合金中Mo含量随着Na2MoO4浓度增加而增加,该泡沫合金骨架平整,泡沫Ni-Mo合金抗拉强度、耐腐蚀性和高温抗氧化性优于泡沫镍,在中性盐雾试验中的抗腐蚀性加强,高温抗氧化性也增强。 相似文献
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研究了三种材质基底上非晶态镍钨合金电沉积过程中阴极析出氢的影响。结果表明,玻璃碳中氢的吸收不可能发生,钯中氢的扩散和吸收是迅速的,镍的行为介乎其间。在玻璃碳上可以生成平整的、厚度较大的、有金属光泽的镍钨镀层,镍是也发现了沉积物,而钯上没有任何新相沉积,由此肯定了氢在镍钨合金诱导共析过程中的重要性。 相似文献
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稀土金属传统制备方法为金属热还原和高温熔盐电解。由于离子液体的出现及迅猛发展,稀土金属的低温电沉积成为可能。回顾了近几十年来国内外在离子液体中电沉积稀土金属用于乏燃料处理、废旧稀土产品中有价金属回收以及功能材料研发三大领域的研究成果以及相关进展,并指出了未来的主要发展趋势和方向。 相似文献
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Electrodeposition of magnesium-yttrium alloys from molten salts was studied by electrochemical techniques.LiF-YF3 was electrolyte system with magnesium oxide and Yttrium oxide as raw materials.It was proved that Mg2+ and Y3+was deposited more prior than other ions during cyclic voltammetry and potential step measurement at 1050 °C.Voltammograms showed Mg2+ could be deposited at-0.5 V,and Y3+ could be deposited at-0.7 V on tungsten electrode compared with platinum electrode.The sedimentation of Mg2+ was more positive about 230 mV than that of other ions in electrolyte.The electrolytic codeposition of yttrium and magnesium was 0.58 V on condition that the weight ratio of Y2O3/MgO was 4:1.Chronopotentiogram indicated that the process of electrodeposition of magnesium-yttrium alloys on tungsten electrode was controlled by diffusion of ions from electrolyte to electrode interface.It was feasible to prepare Magnesium-Yttrium alloys by controlling content of ions in molten salt electrolyte. 相似文献
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Study on the Structures and Properties of Ni-W-B-CeO2 Composite Coatings Prepared by Pulse Electrodeposition 总被引:1,自引:0,他引:1
The aim of this research is to pulse co-deposit nano-CeO2 particles into Ni-W-B alloy coatings in order to improve the surface properties. The influence of pulse frequency and duty circle on deposition rate, microhardness and microstructures, and the influence of heat treatment temperature on phase structures, microhardness and abrasivity of Ni-W-B-CeO2 composite coatings were investigated. The results indicated that the pulse co-deposition of nickel, tungsten, boron and nano-CeO2 particle from the bath which nano-CeO2 particle was suspended by high speed mechanical stirring led to the Ni-W-B-CeO2 composite coatings, possessing better microhardness and abrasion resistance when heat-treated at 400℃ for 1h. The microhardness as-deposited with 636Hz and the deposition rate with 0.0281mm·h-1 was the highest at pulse frequency with 1000Hz and pulse duty circle with 10%. Microstructures analysis displays that decreasing pulse duty cycle leads to refinement in grain structures and the improvement of microstructures. X-ray diffraction shows that the composite coating as-deposited was mainly in the amorphous state and partially crystallized, but when heat treated at 400℃, the crystallization trend was strenthened further. 相似文献
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在有机溶剂中电沉积Er-Co-Fe合金膜 总被引:2,自引:0,他引:2
利用循环伏安法和恒电位电解法研究了室温条件下在有机溶剂DMSO(二甲基亚砜)中Er-Co-Fe合金膜的电化学制备。实验结果表明:在0.1mol·L-1ErCl3-0.1mol·L-1FeCl2-0.1mol·L-1CoCl2-0.1mol·L-1LiClO4-DMSO体系中,当控制电位在-2.00V~-2.60V(vsSCE)范围内进行恒电位电解,可得到表面均匀、附着力强、有金属光泽的黑色非晶态Er-Co-Fe合金膜,其中铒的质量分数可达31.63%~43.15%。 相似文献
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Evolution of Hydrogen Storage Alloys Prepared by Special Methods 总被引:1,自引:0,他引:1
Microstructure characteristics and electrochemical properties of hydrogen storage alloys prepared by gas atomization, melt spinning and strip casting respectively were outlined.The advantages, disadvantages and research development of the above methods for preparing hydrogen storage alloys were explained.The strip casting is a new special means for preparing AB5 rare earth hydrogen storage alloys of high performance and low cost, and the study of the strip casting for preparing hydrogen storage alloys is presented specially. 相似文献