真空镓固定点黑体辐射源研制

为满足红外遥感载荷实验室辐射定标需求,实现红外遥感辐射量值溯源到ITS-90国际温标,研制了真空镓固定点黑体辐射源.黑体腔开口直径为25 mm,深度220 mm,内部喷涂高发射率涂层,通过仿真计算黑体腔的发射率优于0.9999.在真空下测试了镓固定点相变坪台的复现性为4.4 mK,坪台稳定性优于2 mK.测量了镓固定点...     

100～400K真空红外亮温标准黑体辐射源研制

介绍了中国计量科学研究院研制的100~400K真空红外亮温标准黑体辐射源的工作原理、结构、性能测试方法及测试结果。黑体辐射源通过液氮制冷与3温区控制实现了100~400K范围内的温度控制。在真空环境下,测试了其在温度范围100~400K轴向温度均匀性、底部温度稳定性等技术指标,结果表明均匀性优于0.120K,控温稳定性优于0.020K/20min;在室温大气环境下,利用基于控制环境辐射的发射率测量方法测量了黑体空腔发射率,空腔法向发射率为0.9998。采用基于蒙特卡罗黑体发射率仿真计算方法分析轴向温度均匀性对空腔发射率的影响,分析了标准黑体辐射源的不确定度来源,在8~16 μm波长亮度温度的合成标准不确定度优于0.030K。     

空间环境下超大型红外定标用辐射屏蔽门的研制

为满足我国大口径星载遥感器在空间环境下的专项红外定标试验,研制了本套大型辐射屏蔽门。本文综合考虑了辐射屏蔽门的功能特性和应用环境,从材料选择、低温实现、辐射屏蔽、固体润滑及测量控制等方面进行分析和设计。本辐射屏蔽门的成功研制解决了红外定标过程中遥感器、定标黑体以及空间试验环境之间辐射热相互干扰的问题,进一步提高了红外定标精度。该辐射屏蔽门配合国内最大的"超大辐射面真空定标黑体"顺利完成了专项大口径红外相机的红外定标试验,标志着我国大口径红外辐射定标技术达到国际一流水平。     

自校准红外光谱仪的辐射定标与外场应用

为精确获取目标场地的光谱发射率和场地地表温度,研制了具有自校准能力的傅里叶变换红外光谱仪,用于外场地表光谱辐亮度和大气下行辐亮度的测量。开展实验室定标工作,将面源黑体作为标准辐射源,选取观测地面目标热辐射最理想的8～14μm波段,对仪器进行两点法和线性多点法的辐射定标,确定两点法可满足仪器自定标需求。分析光谱仪测量过程中的不确定来源,得到合成不确定度优于0.22 K。开展外场实验,结合光谱迭代平滑温度和发射率分离算法(ISSTES)实现了地表温度和光谱发射率的分离,将获取的光谱发射率与多通道红外辐射计在同一场地下测得的光谱发射率进行比较,进一步验证了自校准红外光谱仪在外场应用时的测量精度和稳定性。     

深低温星上定标黑体源研究

为匹配红外空间载荷低温光学镜头的光学性能,降低背景噪声,实现载荷高精度星上定标,研制了一种基于制冷机主动制冷的深低温星上定标黑体源装置（低温100 K工作）,该星载黑体源装置由面黑体辐射体、低温制冷机主动制冷系统、冷量传输热管及精密测控温系统组成,通过载荷级真空辐射定标实验校验,最终实现红外遥感器对星上定标黑体源宽光谱（2～16μm）、高发射率（0.987）、深低温（100 K）的高精度定标源需求。该深低温星上定标黑体源可用于对极远极冷极弱目标探测的红外载荷星上辐射定标,其高精度、低功耗、通用性的工程化设计方法,为后续相关研究及推广提供技术支撑。     

H500型红外遥感定标高精度真空黑体辐射源的研制

对中国计量科学研究院研制的温度范围覆盖-93~220℃的H500型红外遥感定标高精度真空黑体辐射源进行了介绍。采用圆柱圆锥黑体腔和双层4段PID控温,在真空低背景(液氮冷却)环境下对该黑体进行了性能测试,在大气室温环境下,利用控制环境辐射反射比发射率测量方法测量了黑体空腔发射率和利用红外标准辐射温度计测量空腔底部温度均匀性等指标。实验结果表明,该黑体辐射源升温速率为1℃/min下,控制到温度点的稳定时间优于50 min,并且10 min内的温度稳定性在0.01℃以内;黑体温度设置在20℃、30℃和50℃下空腔发射率的测量结果分别为0.9965、0.9966和0.9963;其黑体底部温度均匀性优于0.03℃;在整个温度区域内扩展不确定度优于0.1℃(k=2)。     

对黑体炉有效发射率值标定的探讨

目前在辐射温度计和热像仪温度的定标上,都缺乏对用于定标黑体的有效发射率的定标,而黑体炉在温度测量及量值传递中处于重要的地位.为了避免温度计量量值的混乱,克服由于没有统一方法及设备造成确定黑体炉有效发射率值不统一的问题,需要尽快明确黑体炉有效发射率定标的问题,以达到规范黑体炉有效发射率确定的目的,确保温度量值的准确可靠.     

黑体辐射源发射率对辐射测温准确度的影响及修正方法

随着辐射温度计的广泛应用,对准确测量、校准或检定的要求越来越高.尽管黑体辐射源的性能不断提高,但黑体辐射源发射率偏离1仍然是影响辐射温度计校准/检定或相关应用准确度的关键问题.可是目前对辐射温度计的校准常常忽略黑体辐射源发射率偏离1的影响或在分析中采用不适当的计算.针对常见的辐射温度计,阐述了对黑体辐射源发射率的影响进行修正与不确定度评定的一般方法,对复杂的宽带辐射温度计提出可行的近似计算方法,并对最常见的8～14μm宽带辐射温度计给出了计算结果.分析结果表明,对于较长波长的辐射温度计,在中高温区的校准或检定中所经常使用黑体辐射源发射率值所引起的亮度温度误差是显著的,应予以修正.     

自校准地表/水表面红外辐射测温仪的研制

研制了一种具有自校准功能的测量地面或水表面辐射温度的仪器,阐述了该仪器的设计原理、具体结构、测试过程及最终的实验结果。为了验证仪器的性能,进行了定标黑体的发射率测量实验,控温稳定性试验,结果表明黑体发射率高于0.996,控温稳定性优于0.04 K;对各个温度传感器进行了标定校准;完成了控制与数据采集程序的编写;进行了样机的辐射测温实验。最后确定出自校准地水表面红外辐射测温仪的测温范围为223～333 K,测温不确定度为0.2 K。     

氟利昂热管黑体辐射源性能实验研究

为了满足机场、车站等红外筛检仪器辐射温度现场校准的要求,文章介绍了一种氟利昂热管黑体辐射源。黑体辐射源空腔形状为圆柱-圆锥形,空腔长100 mm,锥角为120腔,法向平均有效发射率计算值为0.995。利用TRT2辐射温度计对黑体辐射源腔底进行辐射温度测量,对热管进行不同角度的倾斜,测得的黑体辐射源温度稳定性优于0.2℃,氟利昂热管空腔内均匀性优于0.2℃,可以满足现场校准需求。     

中温区真空标准黑体辐射源研制

介绍了中国计量科学研究院研制的中温区真空标准黑体辐射源的结构设计,工作原理,测试结果和不确定度评定.黑体辐射源工作温度范围为320～500 K,黑体空腔开口直径为50 mm,空腔深度为260 mm,表面喷涂了耐高温漆,空腔发射率优于0.999.真空环境下测试了黑体在335～500K温度范围内的轴向温度均匀性,温度稳定性...     

Facility for Measuring the Spatial Uniformity of the Radiation Power of the Surface of the Large-Area Blackbody

The new stage of the development of space-borne information systems is the creation of the Global Earth Observation System. For the full functioning of such a system, it is necessary to provide the uniformity of measurements of all national systems as members of the global system, with high-quality measurement data. This requires the implementation of a high level of ground (prelaunch) calibration of Earth remote sensing instruments. To solve these problems, there were created calibration facilities on the basis of large vacuum chambers with vacuum reference radiation sources, including sources on the basis of black bodies with a wide aperture of 500 mm in the spectral range from \(3~{\upmu }\hbox {m}\) to \(14~{\upmu }\hbox {m}\). Such a facility was created by FGUP “VNIIOFI” in cooperation with FGUP “TsNIIMash”. The ground calibration of Earth remote sensing instruments is being carried out by using blackbody models as radiation sources with known spectral radiance. Facility for ground calibration of remote sensing devices on spectral radiance is based on the usage of a large-aperture blackbody (LABB) with 500 mm diameter and working temperature range from 213 K to 423 K, as a radiation source. This calibration setup comprises a set of reference blackbodies, such as a blackbody on the phase transition of Gallium, a variable-temperature blackbody with temperature range from 213 K to 423 K, a reference blackbody cooled with liquid nitrogen, and IR Fourier spectrometer utilized as a comparator to perform LABB calibration on spectral radiance. The second important characteristic of LABB is the uniformity of spectral radiance across the radiating aperture of this blackbody. The paper describes the device for measuring the spatial homogeneity of the radiation power of the LABB’s radiating surface. This device is based on the use of two-color InSb-CdHgTe detector equipped with modulator and IR lens, which are mounted on a two-axis translation stage suitable for operation in vacuum and installed in the vacuum chamber against LABB. During the measurement of the radiation uniformity, the modulator sequentially sends probing radiation spot either from the LABB’s surface or from the thermostatic radiation source to the detector input. The principle of operation of the device is described. The results of measurements of the radiation power homogeneity across the LABB’s radiating aperture are presented in wide-temperature range.     

红外高光谱大气探测仪星载固定点黑体辐射源的研制

介绍了中国计量科学研究院为风云三号05星红外高光谱大气探测仪研制的微型镓固定点星载黑体辐射源。设计了黑体辐射源空腔,其有效发射率优于0.997。针对星载固定点黑体辐射源的结构设计和性能测试展开了研究:星载固定点黑体辐射源17 ℃的温度均匀性仿真结果优于0.01℃;黑体辐射源在真空下均匀性优于0.02 ℃,稳定性优于0.002 ℃(90 min内);在通过满足航天应用的力学冲击等实验后,镓固定点的复现性优于0.03 ℃;微型固定点相变温坪复现实验加热功率与拐点值之间存在较好的线性关系。     

An Oil-Bath-Based 293 K to 473 K Blackbody Source

A high temperature oil-bath-based-black-body source has been designed and constructed in the Radiometric Physics Division at the National Institute of Standards and Technology, Gaithersburg, MD. The goal of this work was to design a large aperture blackbody source with highly uniform radiance across the aperture, good temporal stability, and good reproducibility. This blackbody source operates in the 293 K to 473 K range with blackbody temperature combined standard uncertainties of 7.2 mK to 30.9 mK. The calculated emissivity of this source is 0.9997 with a standard uncertainty of 0.0003. With a 50 mm limiting aperture at the cavity entrance, the emissivity increases to 0.99996.     

Design and Evaluation of Large-Aperture Gallium Fixed-Point Blackbody

To complement existing water bath blackbodies that now serve as NIST primary standard sources in the temperature range from 15 °C to 75 °C, a gallium fixed-point blackbody has been recently built. The main objectives of the project included creating an extended-area radiation source with a target emissivity of 0.9999 capable of operating either inside a cryo-vacuum chamber or in a standard laboratory environment. A minimum aperture diameter of 45 mm is necessary for the calibration of radiometers with a collimated input geometry or large spot size. This article describes the design and performance evaluation of the gallium fixed-point blackbody, including the calculation and measurements of directional effective emissivity, estimates of uncertainty due to the temperature drop across the interface between the pure metal and radiating surfaces, as well as the radiometrically obtained spatial uniformity of the radiance temperature and the melting plateau stability. Another important test is the measurement of the cavity reflectance, which was achieved by using total integrated scatter measurements at a laser wavelength of 10.6 μm. The result allows one to predict the performance under the low-background conditions of a cryo-chamber. Finally, results of the spectral radiance comparison with the NIST water-bath blackbody are provided. The experimental results are in good agreement with predicted values and demonstrate the potential of our approach. It is anticipated that, after completion of the characterization, a similar source operating at the water triple point will be constructed. Certain commercial equipment, instruments, or material are identified in this paper to specify the experimental procedures and result adequately. Such identification is not intended to imply recommendation or endorsement by the National Institute of Standards and Technology, nor is it intended to imply that material or equipment identified are necessarily the best available for the purpose.     

真空汞固定点黑体辐射源的设计与研制

介绍了中国计量科学研究院研制的真空汞固定点黑体辐射源的结构、工作原理、性能测试结果和不确定度分析。真空汞固定点黑体辐射源灌注的是纯度为99.9999%的高纯汞,黑体空腔开口直径为25 mm,空腔内径为28 mm,深度为260 mm,表面喷涂了NEXTEL 811-21高发射率涂层,采用基于蒙特卡罗黑体发射率仿真计算的方法,计算了黑体空腔在波长为8~14μm的发射率,结果优于0.9999;在真空环境下,测试了真空汞固定点黑体辐射源的温坪曲线和重复性等主要技术指标,结果表明真空汞固定点黑体辐射源温坪稳定性优于2 mK,多次重复性优于1 mK;分析了真空汞固定点黑体辐射源的不确定度来源,其合成标准不确定度为16 mK。