INVESTIGATION ON FATIGUE HYSTERESIS LOOPS MODELS OF FIBRE-REINFORCED CERAMIC-MATRIX COMPOSITES

纤维增强陶瓷基复合材料初始加载到疲劳峰值应力时, 基体出现裂纹, 纤维/基体界面发生脱粘. 在疲劳载荷作用下, 纤维相对基体在界面脱粘区往复滑移使得陶瓷基复合材料出现疲劳迟滞现象. 建立了纤维陶瓷基复合材料疲劳迟滞回线细观力学模型, 采用断裂力学方法确定了初始加载纤维/基体界面脱粘长度、卸载界面反向滑移长度与重新加载新界面滑移长度, 分析了4种不同界面滑移情况的疲劳迟滞回线. 假设正交铺设与编织陶瓷基复合材料疲劳迟滞回线主要受0°铺层、轴向纱线内纤维/基体界面滑移的影响, 预测了单向、正交铺设与编织陶瓷基复合材料在不同峰值应力与不同循环的疲劳迟滞回线, 与试验结果吻合.     

界面脱粘对陶瓷基复合材料疲劳迟滞回线的影响

采用细观力学方法对脆性纤维增强的陶瓷基复合材料拉-拉疲劳载荷下应力-应变迟滞回线进行了研究,将拉梅公式与库仑摩擦法则相结合分析了界面脱粘区以及粘结区复合材料细观应力场.根据卸载与重新加载时纤维相对基体滑移机制,分析了加卸载纤维轴向应力分布,结合断裂力学界面脱粘准则确定了初始加载界面脱粘长度ls、卸载界面反向滑移长度y以及重新加载界面滑移长度z',讨论了界面脱粘能和界面摩擦系数对初始界面脱粘、卸载界面反向滑移、重新加载界面滑移以及加卸载迟滞回线的影响.并与Pryce-Smith模型和试验数据进行对比表明:该文模型与试验曲线吻合的较好.     

基于迟滞行为的2D-SiC/SiC复合材料组份力学性能分析

基于剪滞理论, 建立了单向纤维增强陶瓷基复合材料的加卸载理论模型, 分析了基体长碎块和短碎块对材料迟滞力学行为的不同影响. 通过拉伸循环加卸载试验, 获得了2D-SiC/SiC 复合材料的迟滞应力—应变行为.依据材料基体损伤特点, 将试验结果代入长碎块对应理论推导结果, 计算得到了4 个表征材料组份性能的参数:基体开裂应力为90 MPa, 热残余应力为19 MPa, 界面脱粘能为3.1 Jm2, 界面滑移力为74 MPa. 最后结合少量短碎块的存在对试验结果的影响, 定性分析了计算结果的偏差. 结果表明, 获得的材料组分性能参数具有较小的分散性, 并能够准确表征材料整体的力学行为.      

拉-拉循环荷载作用下的界面脱粘研究

应用弹性力学和断裂力学基本理论，基于剪滞模型，研究了纤维增强复合材料中纤维与基体界面在拉-拉循环荷载作用下的疲劳脱粘特性。建立了描述疲劳裂纹扩展的等效Paris公式，得到了界面疲劳脱粘扩展速率、脱粘应力以及脱粘界面的摩擦系数与循环加载次数的关系式。通过数值模拟计算，进一步分析了界面疲劳脱粘的力学机理。本文分析，考虑了疲劳加载引起的脱粘界面的损伤及损伤分布的不均匀性。同时还考虑了材料泊松比的影响。     

基于弹性-塑性内聚力模型的纤维拔出界面宏观行为分析

用解析法分析了单纤维从聚合物基体中的拔出过程,采用弹性—塑性内聚力模型模拟裂纹的扩展和界面失效,确定了临界纤维埋入长度,该值区分两种不同长度的纤维拔出过程. 在纤维拔出过程,界面经历不同的阶段. 纤维埋长小于临界长度时,界面的脱粘载荷与纤维的埋长成正比;超过临界长度后,界面的脱粘载荷近似为常数. 分析了界面参数对脱粘载荷的影响:增加界面的剪切强度和界面的断裂韧性,或减小界面裂纹萌生位移,均能提高界面的脱粘载荷;界面脱粘后无界面摩擦应力时,拔出载荷—位移曲线的峰值载荷等于界面的脱粘载荷;界面摩擦应力存在时,使峰值载荷大于脱粘载荷,需要较长的纤维埋入长度和较大的界面摩擦应力.      

共晶基陶瓷复合材料的强度模型

根据细观结构内界面的强约束特性,通过纤维-基体内界面切应力确定了共晶陶瓷棒体的细观应力场.然后分析了两相界面处位错塞积产生的应力集中,获得基体内的最大应力,当最大拉应力等于基体理论断裂强度时,得到共晶棒体的断裂强度的解析表达式.考虑共晶陶瓷棒体长度和方位的随机性,根据概率理论得到共晶陶瓷基复合材料的宏观强度的理论模型.结果表明复合材料的宏观强度与亚微米纤维的直径和长度、以及亚微米纤维、基体、共晶陶瓷棒体的弹性常数有关.理论与实验结果十分接近,说明文中理论模型是合理的,同时证明了共晶界面对陶瓷复合材料的重要影响.     

纤维复合材料界面横向拉伸分析

以单纤维十字型横向拉伸试验为研究对象,对纤维/基体界面采用弹性-软化双线性内聚力模型,建立了纤维复合材料在横向拉伸作用下界面法向失效过程的解析模型。得到了沿纤维/基体圆周界面的法向应力分布,纤维/基体界面的状态与界面承载力和单纤维复合材料承载力的关系,以及内聚力参数和试件几何尺寸对它们的影响。结果表明:纤维/基体圆周界面在脱粘前经历全部弹性及弹性+软化两种状态;当界面为弹性状态时,界面法向应力随界面强度线性增加;当界面为弹性+软化状态时,界面软化范围随界面裂纹萌生位移的增加而增大;界面初始脱粘位置与拉伸荷载方向重合;界面初始脱粘时的界面承载力随界面强度及界面裂纹萌生位移的增加而增加,随界面裂纹生成位移的增加而降低;单纤维复合材料的脱粘荷载受基体截面尺寸的影响,当纤维体积含量相同时,沿荷载方向截面尺寸的增大对提高脱粘荷载更显著。     

二维编织陶瓷基复合材料应力-应变行为

对二维编织陶瓷基复合材料拉伸应力-应变行为进行了试验研究和理论模拟. 将二维 编织结构简化为：正交铺层结构和纤维束波动结构. 基于基体随机开裂、纤维随机断裂分布 理论,得到正交铺层结构的应力-应变关系;基于体积平均方法,将纤维束波动部分进行分割, 引入强度分析模型,得到纤维束波动部分的应力-应变关系. 结合正交铺层部分和纤维束波动 部分的应力-应变关系,得到二维编织结构的应力-应变行为,理论与试验吻合较好.     

2D编织陶瓷基复合材料应力-应变行为的试验研究和模拟

本文对2D编织陶瓷基复合材料拉伸应力-应变行为进行了试验研究和理论模拟。将2D编织结构简化为：正交铺层结构和纤维束波动结构。基于基体随机开裂、纤维随机断裂的统计分布理论,得到正交铺层结构的应力-应变关系;基于体积平均方法,将纤维束波动部分分割为若干子单元;由于纤维束的波动使各子单元材料方向与加载方向不一致,因此考虑了各子单元的线性行为和非线性行为对材料响应的影响,同时引入强度分析模型,得到纤维束波动部分的应力-应变关系。结合正交铺层部分和纤维束波动部分的应力-应变关系,得到2D编织结构的应力-应变行为,理论与试验吻合较好。     

单纤维段裂试验评述

单纤维段裂试验作为复合材料界面剪切强度的一种测试方法被沿用至今.但是, 这种方法的可信度已受到一些研究者的质疑.为了明确单纤维段裂试验的问题, 本文首先对试验技术、试验结果分析等方面作了概述, 并指出: 纤维段裂的饱和状态是单纤维段裂试验的终点标志,以及临界长度是由试验得到的唯一数据, 而这二点是这种试验方法独具的特点, 同时也是这种试验方法难以克服的缺陷.在单纤维段裂试验中, 按照纤维段界面端处的局部损伤模式, 有3种界面端应力奇异性分析的问题需要予以考虑:(1)纤维断裂, 基体没有开裂, 和界面没有脱粘;(2)纤维断裂, 基体开裂, 但界面没有脱粘;(3)纤维断裂, 界面脱粘, 基体已开裂或基体未开裂.在单纤维段裂试验的界面端应力奇异性分析的基础上, 本文对单纤维段裂试验的可靠性进行了研究.结论是: 任何纤维和基体组成的复合材料的单纤维段裂试验都存在界面端应力奇异性, 这就排除了用单纤维段裂试验测定界面剪切强度的可能性.      

Influence on fiber inclination and interfacial conditions on fracture in composite materials

Dynamic photoelasticity has been used to study the effect of the fiber-matrix interface and fiber orientation on dynamic crack growth in fiber composites. Two types of fiber-matrix interfaces are considered: well bonded and partly debonded. The fiber-matrix interface is characterized by conducting fiber pullout tests. Partly debonded fibers aligned with the loading direction, result in higher fiber debonded lengths, lower dynamic stress-intensity factorK _ID and lower fracture surface roughness compared to well bonded fibers. Orientation of brittle fibers, with respect to the loading direction, impairs their ability to lowerK _ID , while oriented ductile fibers produce no significant change inK _ID . Misalignment of fibers from the loading direction reduces the fiber debonded length due to kinding of the fiber at the crack face.     

Frequency-dependent random fatigue of panel-type structures made of ceramic matrix composites

The panel-type structures used in aerospace engineering can be subjected to severe highfrequency acoustic loadings in service. This paper evaluates the frequency-dependent random fatigue of panel-type structures made of ceramic matrix composites(CMCs) under acoustic loadings. Firstly, the high-frequency random responses from the broadband random excitation will result in more stress cycles in a deinite period of time. The probability density distributions of stress amplitudes will be different in different frequency bandwidths, though the peak stress estimations are identical. Secondly, the fatigue properties of CMCs can be highly frequency-dependent. The fatigue evaluation method for the random vibration case is adopted to evaluate the fatigue damage of a representative stiffened panel structure. The frequency effect through S-N curves on random fatigue damage is numerically veriied. Finally, a parameter is demonstrated to characterize the mean vibration frequency of a random process, and hence this parameter can further be considered as a reasonable loading frequency in the fatigue tests of CMCs to obtain more reliable S-N curves.Therefore, the inluence of vibration frequency can be incorporated in the random fatigue model from the two perspectives.     

Stress–strain and fracture behaviour of 0°/90° and plain weave ceramic matrix composites from tow multi-axial properties

A computationally economic finite-element-based multi-linear elastic orthotropic materials approach has been developed to predict the stress–strain and fracture behaviour of ceramic matrix composites with strain-induced damage. The finite element analysis utilises a solid element to represent a homogenised orthotropic medium of a heterogeneous uni-directional tow. The non-linear multi-axial stress–strain behaviour has been discretised to multi-linear elastic curves, which have been implemented by a user defined subroutine or UMAT in the commercial finite element package, ABAQUS. The model has been used to study the performance of two CMC composites: a SiC (Nicalon) fibre/calcium aluminosilicate (CAS) matrix 0°/90° cross-ply laminate Nicalon/CAS; and, a carbon fibre/carbon matrix–SiC matrix (C/C–SiC) plain weave laminate DLR-XT. The global stress–strain curves with catastrophic fracture behaviour and effects of fibre waviness have been predicted. Comparisons have been made between the predictions and experimental data for both materials. The predicted results when fibre waviness is taken into account compare well with the experimental data.     

Damage growth by debonding in a single fibre metal matrix composite: Elastoplasticity and strain energy density criterion

A displacement-based finite element-based numerical approach has been employed to study the damage growth in a unidirectional SiC/Al composite containing a pre-existing crack along the fibre/matrix interface. The composite is modeled as a two-material cylinder subjected to uniform displacement. A detailed analysis is made for the stress field in the vicinity of the debond crack tip. This approach incorporates an elastic-plastic analysis combined with a strain energy density criterion to predict debonded crack growth direction, extended stable growth and final termination. The influence of contact taking place between the debonded surfaces is also considered. It is shown that such surface contact leads to reduced stress and strain fields around the crack tip, while the extent of reduction is increased with debonding length. By combining the reduced stress field with the strain energy density criterion, a limiting value for the debonding extension can be calculated for the critical applied displacement that led to fibre fracture.     

Effects of Environmental Degradation on Flexural Failure Strength of Fiber Reinforced Composites

Fiber-reinforced composite laminates are often used in harsh environments that may affect their long-term durability as well as residual strength. In general, environmental degradation is observed as matrix cracking and erosion that leads to deterioration of matrix-dominated properties. In this work, cross-ply laminates of carbon fiber reinforced epoxy were subjected to environmental degradation using controlled ultraviolet radiation (UV) and moisture condensation and the post-exposure mechanical properties were evaluated through elastic modulus and failure strength measurements. Additionally, both degraded and undegraded were subjected to cyclic fatigue loading to investigate possible synergistic effects between environmental degradation and mechanical fatigue. Experimental results show that the degradation results in reduced failure strength. Greater effects of degradation are observed when the materials are tested under flexural as opposed to uniaxial loading. Based on strength measurements and scanning electron microscopy, we identified various damage modes resulting from exposure to UV radiation and moisture condensation, and cyclic loading. The principal mechanisms that lead to reduction in mechanical properties are the loss of fiber confinement due to matrix erosion, due to UV radiation and moisture condensation, and weakened/cracked ply interfaces due to mechanical fatigue. An empirical relationship was established to quantify the specific influence of different damage mechanisms and to clarify the effects of various degradation conditions.     

<Emphasis Type="Italic">In-situ</Emphasis> Full Field Measurements During Inter-Facial Debonding in Single Fiber Composite Under Transverse Load

The fibre/matrix interfacial damage mechanisms of fiber-reinforced composites (FRCs) are investigated for single-fiber composites under transverse load. A stereo microscope setup is used for 3D digital image correlation during in-situ quasi-static tests of single-fiber standard dog-bone specimens. Macro-fibers (0.9 mm diameter) with radically different interfacial bonding with the epoxy matrix are used. Damage appears to initiate with fiber debonding at the free surface along the tensile direction. The crack then propagates around the interface while slightly growing along the fiber until a lateral crack initiates on the debonded free surface, provoking specimen failure. The final failure mechanisms appears to be different for strong and weak fiber/matrix bonding. 3D DIC is used to provide precise measurements of displacements, strains, and out-of-plane displacement during the whole test. Quantitative differences in the displacement fields are measured in the cases of strong and weak bonding between the fiber and matrix. 3D DIC with macro-fibers is shown to be a promising technique to provide a better understanding of the damage mechanisms in a single-fiber composite and to determine interfacial toughness of a specific fibre/matrix couple in order to perform accurate modeling of damage in FRCs. Displacement, strain, and confidence field results for each pixel from each experiment and at each time step are also provided for detailed comparison with simulation results.     

Evaluation of high-cycle fatigue behavior in compact bones at different loading frequencies

This article presents the evaluation of the high-cycle fatigue behavior in bovine compact bones under different loading frequencies. For this objective, rotating bending fatigue testing has been utilized at 10, 20 and 30 Hz of the loading frequency. Cylindrical specimens were obtained from the 12-month old bovine compact bone, considering both tibia and femur. Obtained experimental results indicated that averaged fatigue lifetimes of femur was higher than the ones of tibia. Besides, the effect of the loading frequency on the high-cycle fatigue lifetime was not significant. In addition, scanning electron microscopy images predicted brittle fractures for bones with cleavage marks. Failure mechanisms for tibia were reported as the separation of the fiber (osteon) and the matrix, micro-cracks insides the matrix, and micro-cracks of the fiber (osteon). Failure mechanisms for femur were presented as the separation of lamella layers and micro-cracks in the lamella bone.