碳/碳复合材料疲劳损伤失效试验研究

对单向碳/碳复合材料纵向拉-拉疲劳特性及面内剪切拉-拉疲劳特性进行了试验研究; 对三维四向编织碳/碳复合材料的纵向拉-拉疲劳特性及纤维束-基体界面剩余强度进行了试验研究。使用最小二乘法拟合得到了单向碳/碳复合材料纵向及面内剪切拉-拉疲劳加载下的剩余刚度退化模型及剩余强度退化模型, 建立了纤维束-基体界面剩余强度模型。结果显示: 单向碳/碳复合材料在87.5%应力水平的疲劳载荷下刚度退化最大只有8.8%左右, 在70.0%应力水平的疲劳载荷下, 面内剪切刚度退化最大可达30%左右; 三维四向编织碳/碳复合材料疲劳加载后强度及刚度均得到了提高; 随着疲劳循环加载数的增加, 三维四向编织碳/碳复合材料中纤维束-基体界面强度逐渐减弱。      

单向碳/环氧复合材料拉—拉疲劳性能研究

本文采用GB3354-84规定的大标距直条试样对单向碳/环氧复合材料的拉一拉(R=0.1)疲劳性能和剩余静拉伸强度进行了研究。用成组试验法和升降法测定了S-N曲线和疲劳极限。试样疲劳破坏是由于沿纤维方向(纵向)疲劳裂纹的扩展引起的。试样剩余静拉伸强度大于0.7σ_b。     

复杂面内应力状态下平面编织高铝纤维增强氧化铝基复合材料强度及疲劳寿命预测方法

针对平面编织氧化铝基复合材料提出了一种复杂面内应力状态下的强度准则和疲劳寿命预测方法。通过拉伸、压缩及纯剪切试验,分别获得了材料的静强度指标。考虑材料拉、压性能的差异和面内拉-剪联合作用对材料强度的影响机制,提出了修正的Hoffman强度理论。采用该强度理论预测得到的偏轴拉伸强度与试验结果基本一致,偏差不超过10%。开展了偏轴角θ=0°、15°、30°、45°,应力比R=0.1,频率f=10 Hz的拉伸疲劳试验,试验结果表明随着偏轴角的增加,相同轴向拉伸载荷下的疲劳寿命逐渐降低。由于面内剪切应力分量的作用,疲劳失效由纤维主导逐渐过渡到纤维和基体共同主导的模式。基于单轴疲劳寿命曲线,采用Broutman-Sahu剩余强度模型表征剩余强度随疲劳循环次数的变化规律,结合剩余强度演化模型和修正的Hoffman强度理论,提出了一种面内复杂载荷条件下的疲劳寿命预测模型,并引入疲劳剪切损伤影响因子表征拉-剪应力联合作用对材料疲劳行为的影响。采用本文提出的疲劳寿命预测模型,预测不同偏轴角拉伸疲劳寿命,预测结果与试验结果基本一致,偏差在1倍寿命范围内。比较结果表明在给定应力比、温度和疲劳载荷频率条件下,该疲劳寿命预测模型可以用来预测平面编织氧化铝基复合材料拉-剪复杂面内载荷条件下疲劳寿命。      

单向层合板拉-拉及压-压疲劳加载材料退化模型

以刚度退化为基础,并结合正则化疲劳寿命预测方法,推导建立了单层板疲劳累积损伤过程剩余刚度退化模型,同时给出了剩余强度退化模型.本文退化模型适用于拉-拉及压-压疲劳加载任意应力水平和应力比下的单层板疲劳寿命预测,所建立的剩余刚度退化模型显著减少为获得模型参数所必需的试验件数量,经济性好.最后,通过试验研究,建立了材料T300/BMP-316单向层合板疲劳加载各主方向剩余刚度退化表达式、剩余强度退化表达式及疲劳寿命表达式,为层合板结构疲劳损伤分析提供了有力依据.     

单向碳/环氧复合材料拉-拉疲劳寿命分布

通过对同一应力水平上50根试件的大子样疲劳试验结果研究表明:单向碳/环氧复合材料拉-拉(R=0.1)疲劳寿命服从对数正态分布.      

二维编织陶瓷基复合材料偏轴拉伸力学性能预测

基于二维编织C/SiC复合材料的细观结构,建立了碳纤维丝/热解碳界面/SiC基体和纤维束/表层SiC基体两种尺度下的细观单胞模型,通过有限元方法计算碳纤维丝/热解碳界面/SiC基体模型的等效弹性常数和强度,然后代入纤维束/表层SiC基体模型中计算,并引入Tsai-Wu失效准则,考虑不同失效模式的损伤,建立了二维编织C/SiC复合材料的渐进损伤模型,模拟了其偏轴拉伸应力-应变行为。针对该模型,阐述了二维编织C/SiC复合材料单胞模型在复杂应力状态下其纤维束的损伤过程。数值模拟结果与实验数据吻合较好,验证了模型的有效性,为该种材料的力学性能分析提供了一种有效方法。     

基于纤维束/环氧树脂复合材料试验的单向层合板横向拉伸强度预测方法

实验研究表明,纤维束/环氧树脂复合材料试件的横向拉伸强度与工程上常用的单向层合板横向拉伸强度在趋势上具有很好的相关性,但是数值上存在一定差距。本文使用两种碳纤维和两种环氧树脂制备了三种纤维束/环氧树脂复合材料和单向层合板,并分别测量了纤维束/环氧树脂复合材料和单向层合板的横向拉伸强度,以及环氧基体的拉伸强度。在实验基础上,应用Griffith断裂强度理论建立了纤维束/环氧树脂复合材料和单向层合板的横向拉伸强度的关系模型,通过两种复合材料实验的结果拟合了该模型中的参数。利用第三种复合材料实验进行校验,发现该模型预测的单向层合板横向拉伸强度与实测强度之间达到很好的一致性,相对偏差为9%。采用本文提出的方法,可以用较为简单的纤维束/环氧树脂复合材料和环氧基体拉伸试验预测单向层合板的横向拉伸强度。     

橡胶改性对硼纤维/环氧单向复合材料力学性能的影响

对环氧树脂进行液体丁腈橡胶改性, 并采用缠绕无纬布层压成型工艺制备了硼纤维/环氧单向复合材料。测试了环氧树脂液体丁腈橡胶改性前后硼纤维/环氧单向复合材料的力学性能, 研究了硼纤维/环氧单向复合材料的纵向拉伸破坏模式。结果表明, 基体中的10%液体丁腈橡胶使硼纤维/环氧单向复合材料的拉伸强度、 弯曲强度、 层间剪切强度和断裂延伸率分别提高了18.42%、 13.39%、 28.45%和43.40%, 但其拉伸和弯曲模量稍有下降。基体中含10%液体丁腈橡胶的硼纤维/环氧单向复合材料的纵向拉伸破坏模式为界面层的内聚破坏和脱黏破坏共存的混合破坏。      

加载循环数对2D针刺C/SiC复合材料疲劳剩余强度的影响

为研究陶瓷基复合材料的低周疲劳失效机理,通过试验和细观分析对其疲劳特性进行了探讨。研究了室温下加载循环数对2D针刺C/SiC复合材料拉-拉疲劳剩余强度的影响,并采用光学显微镜和扫描电子显微镜对该材料的断口形貌和微观结构进行了观察。结果表明:2D针刺C/SiC复合材料具有较好的抗疲劳特性,在85%极限拉伸强度(UTS)载荷下的循环数超过106;随着加载循环数的增加,剩余强度先增大然后下降。断口分析表明:纤维拔出长度随着加载循环数的增加而增加,说明在疲劳加载过程中,纤维/基体的界面结合强度降低,减缓了材料内部受力的不均匀性,提高了材料的承载能力,使2D针刺C/SiC复合材料出现了疲劳强化现象。      

2D-SiC/SiC复合材料拉伸加卸载行为

为了研究国产2D-SiC/SiC复合材料的拉伸损伤行为以及低周循环载荷作用下的力学性能,通过试验和建立加卸载细观力学模型,对其拉伸加卸载行为进行了探讨。建立了单向连续纤维增强陶瓷基复合材料加卸载细观力学模型,得到了初始加载、卸载和重新加载时的应力-应变关系;利用断裂统计方法得到了基体裂纹数随应力变化的关系和复合材料失效判断条件。经过应力转化,将该模型应用于国产二维编织SiC/SiC复合材料。对单向加载试件,采用正交试验方法和最小二乘法得到基体Weibull模量和界面剪切阻力,通过控制材料失效强度与试验结果一致,得到纤维Weibull模量。由上述参数确定的2D-SiC/SiC复合材料拉伸循环加卸载应力-应变曲线与实测曲线吻合很好。通过Matlab编程得到2D-SiC/SiC复合材料单向加载时基体开裂过程图。结果表明,2D-SiC/SiC复合材料失效时,基体裂纹分布相对比较均匀;基体裂纹数随应力单调增加,未出现持平段,表明材料失效时,基体裂纹还没有达到饱和。     

Influences of thermal cycling and low-energy impact on the fatigue behavior of carbon/PEEK laminates

Effects of low-energy impact and cyclic thermal loading on fatigue behavior of carbon fiber reinforced polyetheretherketone (carbon/PEEK) laminates have been examined. The fatigue behavior of the virginal composites, low-energy impacted composites, and low-energy-impacted and thermally exposed composites were investigated. Cyclic thermal loading was performed in the temperature range between 60 and −60°C. Residual tensile strength was measured to aid in understanding the influence of low-energy impact on the retention of tensile strength. Fatigue testing involved a stress ratio of 0.1, with a frequency of 3 Hz. The Weibull distribution function was used to evaluate the ultimate tensile strength and fatigue life. S–N curves were plotted and the influence of thermal cycling and the low-energy impact on the fatigue sensitivity of the carbon/PEEK laminates was investigated. Stiffness variation during fatigue testing was monitored and differences in stiffness reduction for three test conditions were compared. C-scan was used to investigate the damage zone under different low-energy impacts and to understand damage propagation during fatigue testing. Moreover, scanning electron microscopy (SEM) was used to examine the fracture morphologies of carbon/PEEK composites in both tensile failure and fatigue failure conditions.     

Enhancing both strength and toughness of carbon/carbon composites by heat-treated interface modification

A simple method to increase both strength and toughness of carbon/carbon (C/C) composites is presented. This method is based on the heat treatment of the pre-deposited thin carbon coating, leading to the formation of more orderly pyrolytic carbon (PyC) as a functional interlayer between fiber and matrix that could optimize the interfacial sliding strength in C/C composites. Effects of such a heat-treated PyC layers on the microstructure, tensile strength and fracture behavior of unidirectional C/C composites were investigated. Results showed that although the in-situ fiber strength was deteriorated after the introduction of interfacial layer, tensile strength of the specimen was greatly improved by 38.5% compared with pure C/C composites without any treatment. The interfacial sliding stress sharply decreased, which was interpreted from finite element analysis and verified by Raman spectra. Therefore, the fracture behavior was changed from brittle fracture to multiple-matrix cracking induced non-linear mechanical behavior. Finally, the ultimate strength can be predicted by different models according to the interfacial sliding stress. Our research would provide a meaningful way to improve both strength and toughness of C/C composites.     

Effect of moisture absorption on the mechanical behavior of carbon fiber/epoxy matrix composites

A carbon fiber/epoxy unidirectional laminated composite was exposed to a humid environment and the effect of moisture absorption on the mechanical properties and failure modes was investigated. The composites were exposed to three humidity conditions, namely, 25, 55, and 95 % at a constant temperature of 25 °C. The carbon fiber–epoxy laminated composites for two different carbon fiber surface treatments were used. The results showed that the mechanical properties differ considerably for each fiber surface treatment. The application of a coupling agent enhanced the fiber-matrix adhesion and reduced dependence of the properties on humidity. The damage mechanism observed at micromechanical level was correlated to acoustic emission signals from both laminated composites. The untreated carbon fiber failure mode was attributed to fiber-matrix interfacial failure and for the silane-treated carbon fiber reinforced epoxy laminate attributed to matrix yielding followed by fiber failure with no signs of fiber-matrix interface failure for moisture contents up to 1.89 %.     

单向连续碳纤维-玻璃纤维层间混杂增强环氧树脂基复合材料的力学性能

为了研究连续单向纤维的层间混杂方式对复合材料力学性能及破坏方式的影响,采用碳纤维-玻璃纤维体积比为1∶1,以拉-挤成型法制备了具有不同层间混杂结构的连续单向纤维增强环氧树脂基复合材料,并研究了不同层间混杂结构的连续单向碳纤维-玻璃纤维增强环氧树脂基复合材料的力学性能及破坏形式。结果表明：具有层间混杂结构的复合材料抗拉强度处于纯碳纤维/环氧树脂复合材料和纯玻璃纤维/环氧树脂复合材料之间,复合材料的拉伸断裂方式为劈裂;具有层间混杂结构的复合材料的层间剪切强度均优于纯碳纤维/环氧树脂复合材料和纯玻璃纤维/环氧树脂复合材料,复合材料的剪切断裂方式为层间断裂。     

Monitoring the damage evolution of flexural fatigue in unidirectional carbon/carbon composites by electrical resistance change method

This paper reported simultaneous monitoring damage evolution of flexural fatigue in unidirectional carbon-fiber-reinforced carbon composites (C/C composites) by electrical resistance change (ERC) methods. The degree of irregularity in electrical resistance changes increased with stress levels increasing. The shapes of electrical resistance change rate–fatigue cycle curves can reflect stress levels and damage types of tested samples: sawtooth shapes reflected delamination at a higher stress level; and “peak” shapes reflected inner damages in one fiber bundle at the fatigue limit stress level. In addition, the similarity of initial electrical resistance–fatigue life curve and S–N curve was observed clearly. In summary, ERC methods can monitor the damage evolution and qualitatively estimate the fatigue life of unidirectional C/C composites.     

Evaluation of the transverse flexure test method for composite materials

A preliminary evaluation of the transverse flexure test method was conducted, using unsized AU4 and AS4, and epoxy-sized AS4, carbon fiber/EPON 828 epoxy matrix composite materials. The transverse flexure test yielded significantly higher values of the transverse tensile strength of these unidirectional composites than did the standard transverse tensile test. Furthermore, the transverse flexure test was more sensitive to variations in fiber surface treatment and sizing, indicating its potential as a test for characterization of the tensile strength of the fiber-matrix interfacial bond.     

交变载荷对CFRP复合材料-铝合金粘接接头剩余强度的影响

为了给碳纤维增强聚合物（CFRP）复合材料粘接结构的安全设计及应用提供参考,针对CFRP复合材料-铝合金对接接头,研究了拉-拉交变载荷作用下的疲劳寿命特性及剩余强度变化规律。设计专用夹具,完成接头的制作及固化,并测试其拉伸、剪切准静态失效强度,在此基础上进行不同载荷水平下的疲劳寿命测试。选取特定载荷水平,测试不同循环次数后的接头剩余强度,并对失效形式进行观察分析。结果表明:CFRP复合材料-铝合金对接接头强度-寿命（S-N）曲线在单对数坐标上符合线性函数规律;随着交变载荷循环周期的增加,接头剩余强度呈先慢后快的下降趋势,而且在较大的载荷水平下,下降幅度更为明显;经历交变载荷循环前、后接头失效形式发生改变,由局部CFRP复合材料表层撕裂转变为局部界面破坏。结合试验测试所获得的初始失效准则,并引入疲劳退化因子,建立内聚力模型对交变载荷作用下的粘接接头强度衰减进行数值模拟,结果表明所建立模型能够有效预测交变载荷作用下的接头剩余强度。