AZ91D镁合金的热压缩变形行为

在应变速率为0.005～1s~(-1)、温度250-350℃条件下,采用Instron-5500热模拟机对AZ91D镁合金的高温压缩特性进行研究,得到其真实应力-应变曲线.分析挤压温度和应变速率等对曲线的影响,得出本构方程的一系列常数,建立AZ91D镁合金在高温压缩中的本构方程关系式.结果表明:变形过程中AZ91D镁合金的流动应力随温度的升高而降低,随应变速率的升高而升高;该流动应力可以用双曲正弦函数来描述,其双曲正弦值随Zener-Hollomon参数自然对数的升高呈线性增大;AZ91D镁合金是正应变速率敏感材料,其应变速率敏感指数m=0.14.     

半固态AZ91D镁合金的压缩变形研究

利用Gleeble 1500热模拟机对半固态AZ91D镁合金的变形规律进行了研究．结果表明：当应变速率相同时,变形温度越高,半固态AZ91D镁合金试样的变形应力就越低;当应变速率和变形温度相同时,半固态球状晶试样的压缩变形应力明显低于枝晶试样的压缩变形应力;变形量对半固态压缩试样的应力一应变关系的影响很小．当应变速率为0．1,10s^-1和变形温度为48m-556℃时,球状晶和枝晶试样的稳定压缩应力分别为3—17．13MPa和6—31．6MPa．当变形温度为508℃和应变速率为0．01—20s^-1时,球状晶和枝晶试样的稳定压缩应力分别为4．78-9．09MPa和7．87-26．21MPa。     

AZ91D镁合金高温压缩过程中的微观组织演变

采用Gleeble-1500热模拟实验机对AZ91D镁合金在400℃、0．01s^-1的条件下进行不同压缩真应变量（1％、10％、60％、100％）的高温压缩实验，利用光学显微镜、透射电镜观察压缩变形过程中合金的显微组织演变。结果表明：在压缩变形的初始阶段，{101^-2}孪生是主要的变形机制，孪晶的尺寸较大；在随后的变形过程中孪晶发生破碎，尺寸变小；随着变形的进一步进行，孪晶之问相互交叉，在孪晶界及孪晶交叉畸变较大的区域成为再结晶的形核区。     

半固态镁合金AZ91D变形行为研究

对应变诱发法制得的半固态镁合金AZ91D坯料进行了单向压缩实验,研究了不同工艺参数对半固态镁合金的压缩流变应力的影响。流变应力不仅是变形量和变形温度的函数,而且是应变速率的函数,由此采用回归分析法建立了能综合反映热力参数对流变应力影响的半固态AZ91D合金的粘塑性本构方程,为半固态触变成形的数值模拟奠定了理论基础。     

半固态等温热处理AZ91D镁合金的显微组织及压缩变形行为

研究了AZ91D镁合金半固态等温热处理后的组织及其压缩变形行为。结果表明,AZ91D镁合金经570℃×60min半固态等温热处理后,枝晶组织特征已不明显。此外,AZ91D镁合金经570℃×60min半固态等温热处理后,半固态压缩应力在压缩应变近似为0.025时达到最大值,然后随着压缩应变的增加而逐渐减小,最后几乎保持不变;进一步,其半固态压缩变形应力还随着变形温度降低或变形速率增加而增加。     

保温时间对压缩AZ91D镁合金半固态组织的影响

研究了SIMA法制备半固态AZ91D镁合金的组织演变规律。在230℃以36，84％的压缩比压缩后，组织呈现明显的流线状，合金处于热力学不稳定状态。在560℃保温不同的时间，淬火实验显示出固相在液相中的分布及形态，预变形AZ91D镁合金由最初的压缩流线状组织，转变为多边形粒子，最后发生球化。随时间的增加，固相率逐渐降低，30min以后变化很小；固相粒子尺寸先减小，超过一定时间后固相合并发生长大。综合考虑，560℃保温15～30min时可以获得最佳的半固态坯料。     

阻燃镁合金AZ91D的研究

研究了通过添加铍，可得到直接暴露在大气中熔炼的镁合金AZ91D。通过金相组织观察发现：当铍的含量达到0.015%时，合金的晶粒度最好，而且具有很好的阻燃性能；同时研究了采用不同的变质剂AZ91D合金进行变质处理。实验结果表明：变质处理的AZ91D合金，组织明显细化，尤其是时效处理后，其力学性能得以大幅度提高，拓宽了合金的使用范围。     

AZ91D镁合金在北京地区的大气腐蚀行为研究

利用室外大气暴露试验，研究了AZ91D镁合金在北京地区的平均大气腐蚀速率，并与相同条件下A3钢的大气腐蚀情况进行了对比．采用扫描电镜(SEM)、X-射线衍射(XRD)、X射线能谱(EDS)以及红外光谱(IR)等多种现代表面分析技术对腐蚀产物的形貌、组成、结构等进行分析，与A3钢相比，AZ91D镁合金具有良好的耐大气腐蚀性能，具有局部腐蚀的特征。     

压铸态AZ91D镁合金热压缩变形流变应力研究

在应变速率为0.01～10 s1、变形温度250～50℃的条件下,采用Geeble-1500D热模拟机对压铸态AZ91D镁合金进行热压缩变形试验,得到并分析了该材料在不同变形条件下的流变曲线.采用数理统计的方法对实验数据进行处理,建立了用Zener-Hollomom参数描述的该材料的高温塑性变形本构方程为ε=1.41× 1012 [sinh(0.014σ)]5.295 exp (-159 449.509/RT),采用双曲正弦函数确定了该材料的变形激活能Q=159.45 kJ·mol1;与重力铸造态AZ91D镁合金比较显示,其流变应力和变形激活能更低.     

T6热处理对变形AZ91D镁合金的强化作用

对热压缩变形的AZ91D镁合金进行T6热处理(410℃×3 h固溶,分别在150、170、190℃时效16 h)。结果表明:T6热处理大大提高了合金的强度和硬度,但降低了塑性;190℃的时效强化效果较好。     

Dynamic recrystallization of AZ91 magnesium alloy during compression deformation at elevated temperature

High temperature compressive tests of AZ91 Mg alloy were carried out at 573 - 723 K and strain rates of 0. 001 - 1 s^-1 . The microstructures of as-compressed samples were observed by optical microscopy and transmission electron microscopy (TEM), and the microhardness was also tested. It is shown that with the increase of temperature or the decrease of strain rate, the flow stress decreases, at the same time the dynamic recrystallization (DRX) of the alloy is more noticeable. The microstructures reveal that continuous dynamic recrystallization, which develops through conversion of low-angle grain boundaries into high-angle boundaries, occurs preferentially at the grain boundary.     

Dynamic recrystallization kinetics of as-cast AZ91D alloy

The flow behavior and dynamic recrystallization (DRX) behavior of an as-cast AZ91D alloy were investigated systematically by applying the isothermal compression tests in temperature range of 220–380 °C and strain rate range of 0.001–1 s^?1. The effect of temperature and strain rate on the DRX behavior was discussed. The results indicate that the nucleation and growth of dynamic recrystallized grains easily occur at higher temperatures and lower strain rates. To evaluate the evolution of dynamic recrystallization, the DRX kinetics model was proposed based on the experimental data of true stress-true strain curves. It was revealed that the volume fraction of dynamic recrystallized grains increased with increasing strain in terms of S-curves. A good agreement between the proposed DRX kinetics model and microstructure observation results validates the accuracy of DRX kinetics model for AZ91D alloy.     

Uniaxial ratcheting and low-cycle fatigue failure behaviors of AZ91D magnesium alloy under cyclic tension deformation

Uniaxial ratcheting and low-cycle fatigue failure behaviors of hot-rolled AZ91D magnesium alloy were studied by uniaxial cyclic stress-controlling tension deformation experiments. The effects of stress amplitude, mean stress and stress rate on the uniaxial ratcheting response and fatigue life of the hot-rolled AZ91D magnesium alloy were analyzed. Results show that (1) the ratcheting strain and ratcheting strain rate of the hot-rolled AZ91D magnesium alloy both increase with the increase of stress amplitude or mean stress; (2) increasing stress rate will decrease the ratcheting strain and ratcheting strain rate of the hot-rolled AZ91D magnesium alloy; (3) the increase of stress amplitude and mean stress can both reduce the fatigue life of the hot-rolled AZ91D magnesium alloy, while the fatigue life will be prolonged with the increase of stress rate.     

AZ80镁合金的高温热压缩变形行为

在应变速率为0.01-50 s^-1、温度为300-450℃的条件下,在Gleeble-3500热模拟机上对AZ80镁合金的高温热压缩变形特性进行研究。实验得出变形过程中的真应力应变曲线,并利用本构方程对流变应力值进行修正,进而利用修正后的应力值得出本实验本构方程中的系列常量;实验还分析温度、应变速率及应变量对微观组织的影响。结果表明：变形过程中的应力值随温度的升高而降低,随应变速率的升高而升高,且修正后的应力值高于未修正值;变形过程中发生动态再结晶且晶粒平均尺寸随变形参数的不同而改变,其自然对数随Zener-Hollomon（Z）参数的自然对数的升高呈线性降低。     

Microstructures of AZ91D alloy solidified during electromagnetic stirring

With the help of an electromagnetic stirring device self-made and alloy melt quenching technology, the effect of electromagnetic stirring parameters on the microstructures of semi-solid AZ91D alloy was mainly studied at the stirring frequency of 200 Hz. The experimental results show that when the stirring power rises, the primary α-Mg rosettes in the semi-solid melt will bear stronger man-made temperature fluctuation and the root remehing effect of the dendritic arms is promoted so that the spherical primary α-Mg grains become much more and rounder. If the stirring frequency is 200 Hz, the ideal semi-solid microstructure of AZ91D magnesium alloy can be obtained when the stirring power is increased to 6.0 kW. If the stirring frequency is 200 Hz and the stirring power is 6.0 kW, it is found that the lower cooling rate is favorable for the spherical primary α-Mg grains to be developed during the electromagnetic stirring stage. If the AZ91D magnesium alloy billet prepared during electromagnetic stirring at the stirring frequency of 200 Hz and the stirring power of 6.0 kW is reheated to the solidus and liquidus temperature region,the primary α-Mg grain‘s shape will get more spherical, so it is very advantageous to the semi-solid thixoforming process     

AZ91D镁合金屑的固相再生(英文)

利用固相再生技术回收利用AZ91D镁合金屑,具体工艺为先冷压再热挤。结果表明:制备的AZ91D镁合金具有较好的力学性能且晶粒明显细化。在热挤出过程中发生了动态再结晶,且动态再结晶组织受到热挤温度和应变速率的影响,在300-350 °C下基面滑移和孪晶协调变形导致动态再结晶晶粒产生,形成"项链"组织;在 350-400 °C下位错的交滑移控制动态再结晶形核;高于400 °C时位错攀移控制了整个动态再结晶过程,形成均匀的再结晶组织。随着应变速率增加AZ91D镁合金力学性能增大,改善了材料的力学性能,但应变速率过大,制备试样表面出现裂纹,影响材料的力学性能。     

AZ91D薄板搅拌摩擦焊

实现了厚度为2.2 mm铸造镁合金AZ91D薄板的搅拌摩擦焊和钨极氩弧焊,分析了搅拌摩擦焊工艺参数对焊接接头成形的影响和接头组织变化,考察了搅拌摩擦焊接头的力学性能.在搅拌头旋转速度为1 380 r/min时得到了比较理想的焊接接头,而1 960 r/min的转速过大.接头不同区域所受的机械力和热量不同,显微组织明显不同.搅拌区晶粒细小,显微硬度和强度都有所提高.搅拌摩擦焊接头力学性能与热输入有关;与氩弧焊接头相比,搅拌摩擦焊接接头的性能更好.