粗镁直接熔炼AM50镁合金力学性能及夹杂物分析

为了研究粗镁直接熔炼AM50镁合金中夹杂物对力学性能的影响,对镁合金锭三个取样位置进行金像分析、拉伸及冲击试验.通过扫描电镜对断口形貌进行分析,并用能谱分析夹杂物的成分.结果表明:AM50的拉伸强度达到184.73 MPa,伸长率为1.54%,冲击韧性达到8.311 J/cm²,断裂方式为脆性断裂和韧性断裂两种混合断裂机制.夹杂物的主要类型为金属夹杂物和非金属夹杂物两大类,主要有MgO、Mg₃N₂、MgCl₂、CaCl₂、Al₄C₃和一些富Fe的夹杂物,并且形状各异,以镁的氧化物夹杂最为常见.     

真空熔炼时AZ31中Mg,Zn挥发行为及组织与性能

在分析合金元素的挥发行为及机理的基础上,对金属粉尘进行了分析.观察了合金的铸态微观组织,并着重讨论了提高AZ31力学性能的途径.研究结果表明:真空熔炼过程中,合金熔体中元素的活度影响其挥发速率;真空条件下合金中存在的气体量降低,夹杂物分解,提高了合金的纯度,使合金显现出本身的特性;AZ31的铸态抗拉强度达210 MPa,比熔炼前提高了82.6%;延伸率为5%,提高了31.5%.     

SiC颗粒增强AZ91镁基复合材料的研究

以AZ91镁合金和平均颗粒尺寸2 μm的SiC颗粒分别为基体相和增强相，采用全液态搅拌铸造法制备了SiC颗粒增强镁基复合材料.力学性能测试结果显示，与AZ91基体合金相比，铸态镁基复合材料表现出更高的室温和高温抗拉强度和屈服强度以及更好的室温磨损抗力；经过热处理和热挤压后，镁基复合材料的抗拉强度和屈服强度均有所提高.拉伸断口形貌观察揭示，镁基复合材料在室温下拉伸时呈现明显的脆性断裂特征，而在较高温度下拉伸时则呈现韧脆混合断裂特征.     

挤压比对AZ91镁合金组织及力学性能的影响

研究了挤压比对热挤压AZ91镁合金显微组织和拉伸性能的影响.结果表明：热挤压可以显著细化AZ91镁合金的晶粒，而且随着挤压比的增加，晶粒变得更加细小；增大挤压比也可以提高AZ91镁合金在不同实验温度下的抗拉强度和屈服强度，且经过3种挤压比挤压的AZ91镁合金在150 ℃时均呈现最高的抗拉强度和屈服强度；此外，经不同挤压比挤压的AZ91镁合金的伸长率均随实验温度的升高而增加.通过拉伸断口形貌的扫描电镜分析，确定了热挤压AZ91镁合金在室温拉伸时均表现为解理断裂为主的脆性断裂，而在较高温度下拉伸时则基本呈现韧性断裂特征.     

镁合金缝焊焊接接头组织及断口分析

采用德国进口3GNP400ST交流缝焊机对镁合金AZ31B进行焊接试验,分析了不同焊接电流下熔核区和热影响区微观组织变化情况,得出镁合金缝焊焊接接头组织变化的一般规律及性能变化情况;观察和分析了母材和焊接接头的断口形貌.     

Y和Ce对AZ91D镁合金显微组织和力学性能的影响

为了开发低成本、高强度、耐高温的新型镁合金,研究了微量Y、Ce对AZ91D镁合金显微组织和力学性能的影响。研究结果表明:Y和Ce复合加入AZ91D镁合金,能明显细化组织晶粒,从而改善合金在室温和高温下的力学性能。当加入0.6%Ce-0.3%Y(质量分数)时,合金晶粒细化效果较好,其室温和高温力学性能比较理想。     

应变速率对AZ31B变形镁合金力学性能的影响

为了研究应变速率对AZ31B变形镁合金力学性能的影响,试验温度为室温、150℃时,对AZ31B变形镁合金进行拉伸试验,并记录抗拉强度和屈服强度,计算延伸率.通过扫描电镜观察拉伸断口形貌,结果表明,随着应变速率的提高,AZ31B变形镁合金的抗拉强度和屈服强度都随之提高,而延伸率却逐渐降低;随着温度的升高,同一应变速率下的抗拉强度和屈服强度降低,而延伸率大幅度升高.通过观察扫描断口形貌发现,合金表现为韧性断裂,且随着应变速率的降低,韧窝逐渐增多.     

激光冲击-超声滚压复合工艺对AZ91D镁合金力学性能的影响

采用Nd:YAG激光冲击强化及超声滚压对AZ91D镁合金进行了表面强化处理,并进行了拉伸试验及断口观察,分析了材料的残余应力分布、微观组织、表面粗糙度,研究讨论了复合工艺对AZ91D镁合金拉伸性能的影响。研究表明:激光冲击强化处理后,镁合金原始晶粒得到明显细化,残余应力达到-122 MPa,表面粗糙度增大,极限抗拉强度提升了15.6%,但塑性下降了27%。激光冲击强化复合超声滚压处理后,残余应力的幅值达到了-197 MPa,表面晶粒得到进一步细化,表面粗糙度大幅改善,材料极限抗拉强度提升了27.4%,材料塑性相对激光冲击强化后提高了19.4%。在残余应力、晶粒细化及粗糙度改善三者的共同作用下,复合工艺延缓了裂纹的扩展速度,显著改善了表面应力状态,提升了镁合金的力学性能。     

AZ91D合金的时效分析

通过光学显微观察、扫描电镜等实验手段对AZ91D镁合金在时效处理过程中组织和性能的变化规律进行了研究,结果表明:时效析出相可大大增加合金的硬度值,但当析出达到一定程度后,合金硬度稳定在较高的水平上;时效可使沉淀相大量析出,强化效果明显,可显著提高材料的性能.     

不锈钢丝增强AZ91镁合金复合材料的显微组织及其力学性能

采用渗流铸造法制备了体积分数约为40%、60%、80%的不锈钢丝增强AZ91镁合金复合材料.利用万能试验机对其进行压缩实验;并利用扫描电镜观察复合材料的显微组织以及压缩后的断口形貌.结果表明:不锈钢丝在AZ91镁合金基体中的分布随着其体积分数的增加逐步均匀;不锈钢丝与AZ91镁合金界面润湿性较好.压缩试验表明:复合材料的抗压强度较AZ91镁合金抗压强度明显提高,40%、60%、80%体积分数的复合材料断裂强度分别为371、387、553 MPa;随着不锈钢丝体积分数的增加,材料的破坏方式由剪切破坏转变为劈裂.     

热挤压镁合金AZ91的微观组织及其力学行为

研究了热挤压镁合金AZ91的微观组织以及在不同试验温度和不同的热处理条件下的拉伸力学性能.结果表明：热挤压可以显著减小AZ91合金的晶粒尺寸，其拉伸力学性能与试验温度密切相关；可以通过热处理来改善其拉伸力学性能，其中人工时效及固溶时效工艺均是改善和提高挤压后AZ91镁合金力学性能的有效途径.此外，利用扫描电镜分析了AZ91镁合金拉伸试样的断口形貌，并探讨了其拉伸断裂机制.     

Microstructure and Mechanical Properties of AZ91D Magnesium Alloy Recycled from Scraps by Hot-press/extrusion

A large number of scraps are produced in the fabrication process of magnesium alloy products. It is necessary to recycle these scraps for the development and scale application of magnesium alloys. In this research, a method for recycling AZ91D magnesium alloy scraps fabricated by hot-press/extrusion was studied. Mechanical properties and microstructure of the recycled specimens were investigated. Microstructural analyses were performed by using the techniques of optical microscopy and scanning electron microscopy. Microstructural observations reveal that the recycled specimens consisted of fine grains when adopting the extrusion temperature of 400-450 ~C, the extrusion ratio of （25-100） ： 1 and the extrusion rate of 0. 10-0. 20 mm/s. Ultimate tensile strength and elongation to failure increased with the increase of the extrusion temperature, the extrusion ratio and the extrusion rate, respectively. Recycled specimens reached the highest ultimate tensile strength of average 361.47 MPa and the highest elongation to failure of average 11.55% when adopting the hot-press, the extrusion temperature of 400_＋5 ~C, the extrusion ratio of 100 ： 1 and the extrusion rate of 0. 15 mm/s. The shape of bonding interface was tightly relation with the ultimate tensile strength. When the bonding interface formed continuous curves, the ultimate tensile strength decreased almost linearly with increasing the average width of the bonding interface. When the bonding interface formed discontinuous curves, the ultimate tensile strength increased almost linearly with the increase the proportion of the fine bonding length accounting for the measured interface length. Ultimate tensile strength of the recycled specimens could be calculated by using the forecastable equation.     

Effect of RE on the ignition-proof, microstructure and properties of AZ91D magnesium alloy

The magnesium alloy is prone to burn during die-casting, which limits its applications severely, so the effect of adding rare earth （RE） on the ignition-proof of AZ91D Mg alloy is studied. The results indicate that the addition of mischmetal RE elements has a remarkable influence on the ignition-proof property of the magnesium alloy. It is found that the ignition temperature of the magnesium alloy can be greatly raised by adding a proper amount of RE. When the amount is 0.1wt%, the ignition temperature reaches 877℃ which is 206℃ higher than that of AZ91D without RE and the mechanical properties of the alloy are also improved, However, the amount of RE must be properly controlled because too much RE would induce grain coarsening and reduce the mechanical properties.     

钕对AZ91镁合金组织及机械性能的影响

采用微观分析、机械性能测试及断口分析等方法研究了钕对AZ91-Nd镁合金(w(Nd)=0,0.1%,0.3%,0.5%,1.0%,1.5%)的微观组织和机械性能的影响。结果表明:Nd以固溶和金属间化合物(A l11Nd3)的形式存在时具有细化晶粒、抑制二次β相析出、使不完全离异共晶转化为离异共晶的作用;Nd通过固溶强化、析出强化和细晶强化增加了合金强度和硬度,并改善了塑性;加入Nd后合金的断裂机制从脆性解理断裂转变为准解理断裂。     

离心铸造对AZ91镁合金组织及力学性能的影响

为了研究卧式离心铸造工艺对AZ91镁合金力学性能及显微组织的影响,采用卧式离心铸造方法制备外径为400 mm、厚度为20 mm且长度为1 000 mm的AZ91镁合金管材,并对离心铸造态与自然凝固态AZ91镁合金管材的微观组织及力学性能分别进行了观察与测试.结果表明,离心铸造态AZ91镁合金管材的抗拉强度和伸长率分别为158 MPa和3.4%,与自然凝固态管材相比分别提高了20%和89%.离心铸造态镁合金管材的微观组织得到明显细化.与自然凝固态AZ91镁合金管材相比,离心铸造态AZ91镁合金管材在凝固过程中的共晶转变在很大程度上受到抑制,并形成了以α-Mg为主相的组织.卧式离心铸造方法提高了AZ91镁合金的综合力学性能,并使合金的组织得到细化.     

Effects of rare earth elements on the microstructure and properties of magnesium alloy AZ91D

The effects of rare earth elements on the microstructure and properties of Magnesium alloy AZ91D alloy were studied.The different proportion of rare earth elements was added to the AZ91D and the tensile tests were carried out at different temperatures.The experimental results show that at room temperature or at 120℃ the AZ91D‘s decrease with the increasing amount of the rare earth elements.however,the ductility is improved.The influence of 0.14%Sb(mass fraction)on the AZ91D‘s strength is like that of rare earth elements(0.2%-0.4%)(mass fraction).Microstructure graphs demonstrate that appropriate amount of rare earth elements (0.1%-0.2%) can fine AZ91D‘s grain and improve its ductility.