共查询到16条相似文献,搜索用时 187 毫秒
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为了研究热迟滞性对工业铂电阻温度计测量不确定度的影响,选取了8支高精度铂电阻温度计进行实验。在-50~150℃内,选择3个温度区间,采用两种标准方法(IEC 60751,ASTM E644)测量水三相点(0.01℃)和所选温度范围内的中间点的迟滞性变化。实验结果表明:4支薄膜铂电阻温度计在两种标准方法测量下,随着温度区间跨度增大,热迟滞性影响增大,IEC 60751标准方法测量的热迟滞性最大值为14.2mK,ASTM E644标准方法测量的热迟滞性最大值为20.5mK;选取4支铂丝铂电阻温度计在温度范围为-50~150℃测量时,IEC 60751和ASTM E644标准方法测量的热迟滞性数据最大值分别为1.1mK和0.9mK;铂丝铂电阻温度计热迟滞性明显小于薄膜铂电阻温度计。 相似文献
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针对两种不同类型的工业铂电阻温度计(IPRTs),使其在-80℃和300℃下恒温一定时间后再测量其0℃下的电阻偏移,由此来确定其在该温度下的热迟滞性。试验结果表明:薄膜型铂电阻温度计在0℃的热迟滞性远大于铂丝型铂电阻温度计,并且随着测量次数的增多,热迟滞性会逐渐减小。 相似文献
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精密铂电阻温度计是介于标准铂电阻温度计与工业铂电阻温度计之间的测温传感器,利用ITS-90国际温标定义的固定点分度精密铂电阻温度计可以提高测温准确性和稳定性,但经常会出现超出内插方程所规定的温度范围以致无法用定点法分度的问题.本文对精密铂电阻温度计利用水三相点及镓熔点进行分度,调研了通过0~29.7646℃温区内插方程直接外推到70℃的可行性.实验以两支精密铂电阻温度计为对象,对定点法外推结果与直接比较法进行比较,结果显示:外推结果与标准值最大差值为1.5mK,表明精密铂电阻温度计利用水三相点及镓熔点进行分度并外推至70℃在一定的测量水平要求下是可行的. 相似文献
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本文以最常用的温度段(0-429.527)℃,以一等标准铂电阻温度计检定二等标准铂电阻温度计为例来分析标准铂电阻温度计的测量结果不确定度。 相似文献
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The stability and interpolation characteristics of some industrial-grade platinum resistance thermometers have been investigated between 77 K and 273 K. Seven sensors were thermally cycled many times between 77 K and 373 K and were found to suffer reversible changes in ice-point resistance. After some tens of cycles between 77 K and 273 K the ice-point resistances of the thermometers stabilised to within a few milliohms, provided that the thermometers were not heated above 300 K. A two-point calibration method for these thermometers is described. Using resistance values at the ice-point and the oxygen boiling point, a measurement accuracy of 35 mK can be obtained over the range 77 K to 273 K. Interpolation data for 27 thermometers are given. 相似文献
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We have investigated the optothermal property and decomposition characteristics of PtO(x) ultrathin film protected by ZnS-SiO2 layers and effects of the constituent phases of PtO(x) on super-resolution capability and read stability of the super-RENS disk. All the ZnS-SiO2/PtO(x)/ZnS-SiO2 multilayers exhibited a steep reflectivity drop at the temperature range between 265 and 350 degrees C, corresponding to the decomposition of PtO(x). The decomposition temperature of the 4-nm-thick PtO(x) ultrathin film protected by ZnS-SiO2 layers was much lower than those obtained in thick PtO(x) films without protection. The activation energy for thermal decomposition was approximately 1.3 eV. Both the decomposition temperature and activation energy for thermal decomposition were unaffected by the constituent phases of PtO(x). Carrier to noise ratios (CNR) of over 40 dB for mark size of 150 nm were achieved in all super-resolution near-field structure (super-RENS) disks, while the super-resolution readout was limited to 2.5 x 10(3) approximately 4.5 x 10(4) cycles. The effect of constituent phases of PtO(x) on the super-resolution capability of super-RENS disk with a PtO(x) mask layer was minimal. However, as the constituent phases of PtO(x) mask layer transformed from a mixture of Pt and PtO, to pure PtO, and then to a mixture of PtO and PtO2, the readout stability of super-RENS disk increased dramatically since less heat was absorbed by the PtO(x) mask layer composed of PtO and PtO2 during the readout process, prohibiting the diffusion of materials inside the bubble to the GeSbTe phase change layer. 相似文献
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以含高岭石、一水硬铝石、黄铁矿的高岭土为原料,经过压块烘干后,在真空(15~50 Pa)、不同加热温度下,采用同步热分析仪(DSC-TGA)、X射线衍射(XRD)等分析手段对高岭土在真空下的热分解进行研究。DSC-TGA的结果与高岭石、一水硬铝石、黄铁矿三种矿物常压下的热力学计算出的分解温度相符。实验产物的XRD结果表明:在真空条件(15~50 Pa)下,一水硬铝石AlO(OH)在100~200℃之间脱水,300℃时脱水完全;黄铁矿FeS2在500~600℃分解,分解产物为FeS和S2,在700℃时,黄铁矿FeS2分解完全;高岭石Al2Si2O5(OH)4在实验煅烧过程中,在200~300℃之间脱水,生成非晶态的偏高岭石,比该矿在常压的脱水温度提前200℃左右。继而转变成A-lSi尖晶石,最后形成莫来石与方石英。实验结果与热力学计算符合,充分说明真空条件对高岭土中各种矿物分解产生气体的反应有较大的促进作用。在本实验三种矿物分解产生气体的过程中,先进行的反应对后一反应的发生影响不明显。 相似文献
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Pt/YSZ氧传感器的电极电阻和响应特性 总被引:3,自引:1,他引:2
应用两电极直流极化法测定了氧传感器在380~800℃中的Pt,空气/YSZ电极电阻,从交流低频阻抗测量外推法测得YSZ的体电阻,可以将YSZ的直流极化从电极的过电位中区分出来.Pt,空气|(ZrO2)0.93(Y2O3)0.07|空气,Pt,电池的直流极化1gI-η作图得出,电极电荷传递系数为2.YSZ体电阻、Pt,空气/YSZ电极电阻和电极交换电流对温度的Arrhenius图,在600℃和570℃附近存在着类似的活化能变化.测量表明;700℃时,氧传感器的测量响应时间≤2.5s. 相似文献
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Corrosion‐Activated Chemotherapeutic Function of Nanoparticulate Platinum as a Cisplatin Resistance‐Overcoming Prodrug with Limited Autophagy Induction 下载免费PDF全文
Hsien‐Jen Cheng Te‐Haw Wu Chih‐Te Chien Hai‐Wei Tu Ting‐Shan Cha Shu‐Yi Lin 《Small (Weinheim an der Bergstrasse, Germany)》2016,12(44):6124-6133
Despite nanoparticulate platinum (nano‐Pt) has been validated to be acting as a platinum‐based prodrug for anticancer therapy, the key factor in controlling its cytotoxicity remains to be clarified. In this study, it is found that the corrosion susceptibility of nano‐Pt can be triggered by inducing the oxidization of superficial Pt atoms, which can kill both cisplatin‐sensitive/resistance cancer cells. Direct evidence in the oxidization of superficial Pt atoms is validated to observe the formation of platinum oxides by X‐ray absorption spectroscopy. The cytotoxicity is originated from the dissolution of nano‐Pt followed by the release of highly toxic Pt ions during the corrosion process. Additionally, the limiting autophagy induction by nano‐Pt might prevent cancer cells from acquiring autophagy‐related drug resistance. With such advantages, the possibility of further autophagy‐related drug resistance could be substantially reduced or even eliminated in cancer cells treated with nano‐Pt. Moreover, nano‐Pt is demonstrated to kill cisplatin‐resistant cancer cells not only by inducing apoptosis but also by inducing necrosis for pro‐inflammatory/inflammatory responses. Thus, nano‐Pt treatment might bring additional therapeutic benefits by regulating immunological responses in tumor microenvironment. These findings support the idea that utilizing nano‐Pt for its cytotoxic effects might potentially benefit patients with cisplatin resistance in clinical chemotherapy. 相似文献