Optical dating of Chinese loess using sand-sized quartz: Establishing a time frame for Late Pleistocene climate changes in the western part of the Chinese Loess Plateau

The Chinese Loess Plateau (CLP) is of major interest to Quaternary geologists because it represents an important terrestrial archive of palaeoclimatic fluctuations. Previous multiple-aliquot luminescence dating studies of Chinese loess mainly used thermoluminescence (TL) and infrared stimulated luminescence (IRSL) signals of polymineral fine-grains; these are known to be subject to anomalous fading and thus will tend to yield age underestimations. In this paper we investigate whether the blue-light stimulated luminescence (BLSL) signals from 63 to 90 μm quartz grains extracted from three western Chinese loess sites (Zhongjiacai, Le Du and Tuxiangdao) can be used to establish a reliable chronology. The single-aliquot regenerative-dose (SAR) procedure is used for the equivalent dose (D_e) determinations and the suitability of our measurement protocol is confirmed by dose recovery tests. The influence of an IRSL signal on the quartz D_e measurements derived from BLSL has been investigated. From these results we conclude that an IRSL contamination, expressed as an IRSL/BLSL ratio, of up to 10% can be accepted before the values of D_e are significantly affected. All three sites yield stratigraphically consistent and spatially highly reproducible optical ages up to about 50–70 ka. At the Tuxiangdao site a marked hiatus in the record is identified between ∼20 and ∼30 ka; this remained undetected in previous studies and clearly highlights the importance of high-resolution optical dating in Chinese loess research. The optical ages presented in this work provide more evidence for episodic loess deposition and varying loess accumulation rates in the western part of the CLP. Our study seems to confirm the potential of optically stimulated luminescence (OSL) dating using the SAR procedure applied to the very fine sandy quartz fraction in Chinese loess back to ∼40–50 ka (∼120–150 Gy).     

Timing for high lake levels of Qinghai Lake in the Qinghai-Tibetan Plateau since the Last Interglaciation based on quartz OSL dating

Qinghai Lake is situated in the northeast of the Qinghai-Tibetan Plateau (QTP). Its size and proximity to the junction of three major climate systems make it sensitive to climate changes. Some investigations on shorelines of Qinghai Lake suggested highstands during MIS 3, but to what extent the lake level was higher than today is yet undetermined. Others proposed that the maximum highstands probably dated to MIS 5. It has also been shown that the lake level 120 m higher than today occurred at around 12 ka. Most of these previous ages were obtained using ¹⁴C dating or multiple-aliquot IRSL/OSL dating. For ¹⁴C dating, because of the dating limit (<40 ka) and the lack of suitable dating materials in this arid area, it is difficult to establish reliable chronological control. In the present study, seven samples collected from lacustrine deposits (five samples) and sand wedges (two samples) were dated using quartz optically stimulated luminescence (OSL) with the single aliquot regenerative-dose (SAR) protocol. OSL dating results showed that (1) the lake had experienced two high lake levels, one was in MIS 5 and another in early to middle MIS 3; (2) no evidence of high lake levels in MIS 4 has been found; (3) the alluvial gravels, whose surface is at an elevation of ～3246 m, were formed at least 28.8 ± 2.3 ka ago, and the widespread sand wedges within the alluvial gravels were formed during the period of 15.1–28.8 ka, which implied that the lake level had not reached an elevation of ～3240 m after 28.8 ± 2.3 ka.     

High resolution OSL dating back to MIS 5e in the central Sea of Okhotsk

Marine sediments contain important archives of past ocean and climate changes, but at high latitudes the absence of carbonate has prevented the construction of accurate chronological models. We have begun a study to (1) determine the accuracy of luminescence ages in deep-sea marine sediments, e.g. by comparison with marine oxygen isotope stratigraphy where possible, (2) describe changes in sedimentation rate through time, and (3) test whether it is possible to date back to marine isotope stage 5e (MIS 5e). We show here that optical dating of fine grains of quartz from the central Sea of Okhotsk is able to provide an accurate and precise chronology for the reconstruction of the palaeoceanic and palaeoclimatic environment at our site. The upper 6.5 m of the 18.42 m long core MR0604-PC07A is believed, based on its magnetic susceptibility and the oxygen isotope (δ¹⁸O) records to contain the last ～150 ka. Forty OSL samples were taken from this upper part of the core. The single-aliquot regenerative-dose (SAR) procedure is used for equivalent dose (D_e) determination. The luminescence characteristics of fine-grained quartz (4–11 μm) extracted from the core are described. The OSL signal is dominated by the fast component and a dose recovery test shows that we can accurately measure a known dose given in the laboratory prior to any heat treatment. Dose rates were determined using high-resolution gamma spectrometry, and vary between 0.4 and 1.6 Gy/ka. The OSL ages from this section lie between ～140 ka and ～15 ka and are in very good agreement with the δ¹⁸O stratigraphy up to MIS 5e. A clear change in sedimentation rate is identified: between ～139 and 110 ka, the sedimentation rate was ～0.09 m/ka, but then from ～110 to 15 ka, the sedimentation rate decreases to a constant value of ～0.04 m/ka. Our data confirm that OSL dating using widely distributed fine-grain quartz has great potential for dating deep-sea sediments. Because luminescence methods use clastic materials, they do not depend on the presence of biogenic carbonate. As a result it is now likely that we can establish a chronology in regions of the ocean that were previously undatable.     

Dating the Kawakawa/Oruanui eruption: Comment on “Optical luminescence dating of a loess section containing a critical tephra marker horizon,SW North Island of New Zealand” by R. Grapes et al.

An IRSL age of 17.0 ± 2.2 ka (and a “mean age” of ca. 19 ka) reported by Grapes et al. [Grapes, R., Rieser, U., Wang, N. Optical luminescence dating of a loess section containing a critical tephra marker horizon, SW North Island of New Zealand. Quaternary Geochronology 5(2-3), 164–169.] for the Kawakawa/Oruanui tephra, and other ages associated with a loess section in New Zealand are untenable: age data presented are inconsistent, no formal statistical treatments or error determinations were undertaken in age analysis, and the ages proposed are seriously at odds with multiple radiocarbon age determinations on tephra sequences bracketing the Kawakawa/Oruanui tephra and with palaeoenvironmental evidence elsewhere for the time period concerned. We suggest that the bulk polymineral IRSL ages on the tephra and encapsulating loess deposits were underestimated in part because of contamination of the loess by the integration of younger materials during slow deposition and continuous modification by upbuilding pedogenesis. Single-grain luminescence assays may reveal such contamination. A ¹⁴C-based age of ca. 27 ± 1 ka cal BP (2σ), reported in 2008, currently remains the best estimate for the age of eruption of the Kawakawa/Oruanui tephra.     

Optical luminescence dating of a loess section containing a critical tephra marker horizon,SW North Island of New Zealand

A new IRSL dataset is presented for the age and setting of a critical Late Glacial Maximum tephra isochron marker. The rhyolitic tephra, known as the Kawakawa Tephra, occurs as a 14 cm thick layer within a 5.9 m thick loess section overlying alluvial gravels in the Rangitikei River valley, SW North Island of New Zealand. Ages range from 21 at the base to 5 ka near the top of the loess and bracket an age of 17.0 ± 2.2 for the tephra. The new IRSL ages are in agreement with published and unpublished luminescence ages from other localities of loess, sand and ash above and below the tephra and of the tephra itself, that indicate an age of ca. 19 ka for the Kawakawa Tephra. This age is considerably younger than the generally accepted ¹⁴C 27.1 ka cal yrs BP age of the Kawakawa Tephra and highlights an unresolved discrepancy between the two dating systems.     

OSL chronology for lacustrine sediments recording high stands of Gahai Lake in Qaidam Basin,northeastern Qinghai–Tibetan Plateau

The Qaidam Basin in the northeastern Qinghai–Tibetan Plateau (QTP) is one of the largest hyper-arid intermontane basins in the northern hemisphere, and has abundant records for the study on palaeo-lake level fluctuations and palaeoclimatic changes. Significant efforts have been invested to define the timing of shoreline deposits using radiocarbon dating. However, due to the dating limit, the absence of organic materials and carbon reservoir effects for radiocarbon dating in arid areas, it is difficult to establish a reliable chronology for shoreline deposits. Therefore, controversy exists regarding the chronology for the high lake level in the Qaidam Basin, as well in the QTP. Some proposed that high lake levels occurred during late Marine Isotope Stage (MIS) 3, while others recently argued that the highest lake level in the QTP and adjacent regions existed in MIS 5. In Gahai Lake (now a salt lake), we investigated a section comprising lacustrine and shoreline deposits, which was about 25 m above the present lake level. Seven samples were collected for quartz optically stimulated luminescence (OSL) dating. A sample collected from a fine sand layer (the bottom of the section, and 12 m above the present lake level), which was assumed to have been deposited underwater, gave an OSL age of 82 ± 8 ka. It suggested that the lake level was at least 12 m higher than present in late MIS 5. The high lake level could maintain till about 73 ± 6 ka, and then decreased. This lake level decrease resulted in a gravel layer deposit between 73 ± 6 and 63 ± 6 ka (roughly during MIS 4). The lake level rose again (about 24 m above the present lake level) between 63 ± 6 and 55 ± 5 ka (roughly in early MIS 3). No lacustrine or shoreline deposits higher than the top of the current section were found around Gahai Lake. Thus, higher than present lake levels in Gahai Lake occurred in both late MIS 5 and early MIS 3.     

Evaluating a SAR TT-OSL protocol for dating fine-grained quartz within Late Pleistocene loess deposits in the Missouri and Mississippi river valleys,United States

The Mississippi and Missouri river valleys in the midcontinental United States contain extensive loess-paleosol sequences that are used to constrain the timing of expansion and retreat of the Laurentide Ice Sheet. Previous studies have been unsuccessful in producing finite ages for sediments older than ∼150 ka due to saturation of luminescence emissions. The thermally transferred optically stimulated luminescence (TT-OSL) dating technique is tested on the fine-grained (4–11 μm) quartz fraction of these loess deposits because the TT-OSL signal has been shown to grow with high (kGy) radiation doses. The TT-OSL signal continued to increase with radiation dose above 900 Gy. The optical and thermal stabilities of this TT-OSL signal are evaluated. Equivalent dose values are highly sensitive to preheat temperatures. Recycling ratios, zero-dose response values, and dose recovery tests all yield acceptable values for samples with burial doses >∼200 Gy. The apparent TT-OSL ages for the Roxana Silt (∼52–63 ka), Teneriffe Silt (∼66 ka), and Loveland Silt (∼133–192 ka) agree at 1σ level with previously published TL and IRSL ages derived from the same samples. For the oldest unit, the Crowley's Ridge Silt, TT-OSL ages (∼167–200 ka) are younger than IRSL or TL ages by ∼20%. This is interpreted as underestimation related to TT-OSL signal contamination, which can be avoided by isolating the fast component of the TT-OSL. Preliminary fast component TT-OSL ages for the Crowley's Ridge Silt (∼197–241 ka) favor deposition during marine oxygen-isotope stage (MIS) 7 or 8, contrary to a previous inference of a MIS 12 deposition.     

High-precision U-series measurements of more than 500,000 year old fossil corals

Robust, independent age constraints on the absolute timing of climate events based on the U-series dating of fossil coral are sparse before the last glacial cycle. Using multiple-collector inductively coupled plasma mass spectrometry with multiple-Faraday protocols, we are able to date ～ 600 ka samples with an uncertainty of better than ± 15 ka (2σ), representing a three-fold improvement in precision compared with previous techniques. Using these methods, we report U-series measurements for a suite of > 500 thousand year old (ka) corals from Henderson Island, an emergent atoll in the south-central Pacific Ocean. The fossil corals show extraordinarily little diagenetic alteration for their age and the best-preserved sample yields a U-series age of 600 ± 15 ka (2σ), which overlaps with the timing of the warm Marine Isotope Stage (MIS) 15 interglacial. The open-system model of Villemant and Feuillet [Villemant B. and Feuillet N. (2003) Dating open systems by the ²³⁸U–²³⁴U–²³⁰Th method: application to Quaternary reef terraces. Earth and Planetary Science Letters 210(1–2), 105–118.] and the linear regression (or open-system isochron) is clearly limited for such old samples. However, the open-system model developed by Thompson et al. [Thompson W.G., Spiegelman M.W., Goldstein S.L., and Speed R.C. (2003) An open-system model for U-series age determinations of fossil corals. Earth and Planetary Science Letters 210(1–2), 365–381.] appears to reliably correct for open-system effects in roughly half of the corals, giving a MIS 15 origin for these. Thus the data provide evidence that the systematic addition of ²³⁰Th and ²³⁴U through α-recoil is a dominant open-system process occurring in the Henderson Island fossil reef system. Several coral samples yield significantly older Thompson et al. open-system ages between 650 and 750 ka. The uncertainty on these ages (typically ± 30 kyrs) is too great for precise assignment but most data overlap with the MIS 17 interglacial. The reliability of these ages is currently unclear. It is shown that separate aliquots of the same coral can yield different Thompson model ages. Therefore, there appear to be additional diagenetic mechanisms that create further anomalous excursions in the U-series systematics, limiting the reliability of the Thompson et al. open-system model.     

Luminescence dating of the top of a deep water core from the NESTOR site near the Hellenic Trench,east Mediterranean Sea

In the present study, the uppermost 3 cm of muddy, seabed sediment was collected from a deep-sea sediment core, drilled from a water depth of 4 km, near the deepest site of the Mediterranean Sea, outside Pylos, Greece. The core was divided into 7 layer samples, each 3–4 mm thick, in order to get an independent age assessment for each one using luminescence dating; from polymineral coarse grains in the range 30–60 μm. Between 11 and 22 aliquots were measured for each sample using the optically stimulated luminescence, single-aliquot regenerative-dose analysis. The estimated mean equivalent dose values had an uncertainty less than 3% and resulted in optical ages ranging from 3.5 to approximately 5 ka, with uncertainties lying between 5.5 and 7.4%. Multiple-aliquot, thermoluminescence-based, additive-dose, total bleaching approach provided equivalent doses with typical errors of 10–15% and ages in the range of 3.6 and 9.4 ka, with uncertainties up to 17%. Single-aliquot optical ages are shown to be relatively successful, due to their consistency with AMS ¹⁴C radiocarbon ages, obtained from Planktonic foraminifera from the same core. Luminescence dates for the topmost 1.5 cm indicate a substantial mix and post burial disturbance of the surface sediment. Below the topmost 1.5 cm, both luminescent approaches indicate ages which increase smoothly with depth. The concordant OSL and TL age estimates for the sample O5, in conjunction with specific luminescence properties and its major-element geochemical chemistry content, suggest that it was heated during the Santorini volcanic eruption. Deposition rates of 8.6–18.9 cm over 10 ka below the sample O5, provided by optical ages, exhibit an excellent level of agreement with the accumulation rate of 7–18 cm over 10 ka at the sea bottom, already reported for the site under study.     

Luminescence dating of archaeosediments: A comparison of K-feldspar and plagioclase IRSL ages

IRSL single-aliquot dating of three feldspar fractions from a Howieson's Poort (SA) industry site has been investigated. In the case of the plagioclase fraction (ρ > 2.62 g cm^?3) equivalent dose is similar to that of the other fractions (i.e. ρ < 2.58 g cm^?3, high-K-feldspar; and 2.58 < ρ < 2.62 g cm^?3; low-K-feldspar). However, the g values measured for this fraction is such that the fading-corrected age is overestimated. The K content of each fraction was estimated by SEM. The DRC-corrected ages for the two lighter feldspar fractions are consistent with the archaeological interpretation. This study shows that reliable single-aliquot luminescence ages can be obtained using K-feldspar and Na-plagioclase.     

Optically stimulated luminescence dating of sediments from the Yellow River terraces in Lanzhou: Tectonic and climatic implications

The stratigraphic chronology of Yellow River terraces was investigated and studied in Lanzhou Basin, western Chinese Loess Plateau. The optically stimulated luminescence (OSL) dating results show that terraces T₁, T₂ and T₃ formed at 8 ka, 20 ka and 70 ka, respectively. Lateral accretion of the riverbed facies gravel sediments occurred during interglacial periods while vertical aggradations of the terrace sediments deposited predominantly under cold and dry glacial period. A thick layer of aeolian loess with a basal age about 35 ka indicates a remarkable drop of air temperature and a dry, cold climate. The temporal correlation between terrace formation and tectonic movement has not yet been established in this research, but the stratigraphic chronology of the terrace sections provides the timing of the terrace formation, the incision rate of the Yellow River, and the slip rate of the fault horizon.     

Luminescence characteristics of coastal sediments in Langhovde,East Antarctica

The Late Pleistocene sea-level history of Antarctica is key to understanding and predicting the responses of icesheets, which significantly contribute to the global sea level, to changing climates. Coastal sediments at Lützow-Holm Bay, East Antarctica, have yielded radiocarbon ages of Holocene and Marine Oxygen Isotope Stage (MIS) 3 from deposits above the present sea level, suggesting that there have been two episodes of sea-level highstand. However, radiocarbon dating is likely to be less accurate for dating sediments close to or older than 40–50 ka, the upper limit of its application. We thus explored the applicability of luminescence dating to coastal sediments newly sampled from Langhovde on the eastern coast of Lützow-Holm Bay. Samples were collected from a trench <1 m deep and at several meters above the present sea level. Quartz coarse and fine grains, K-feldspar coarse grains, and polymineral fine grains were extracted from the samples. Quartz coarse and fine grains both showed very low optically stimulated luminescence sensitivity and no fast component and thus were not considered further. Dose-recovery tests on post-infrared infrared-stimulated luminescence (post-IR IRSL) signals of K-feldspar and polymineral grains yielded variable results and suggested acceptable measurement conditions for each grain size fraction and expected equivalent dose. Preliminary measurements revealed that the trench section can be divided into the upper and lower layers, corresponding to the Holocene and MIS 7, respectively. Further application of post-IR IRSL dating to coastal sediments, including to previously radiocarbon-dated sections, could refine our understanding of the late Quaternary relative sea-level history in East Antarctica.     

A long-term rock uplift rate for eastern Crete and geodynamic implications for the Hellenic subduction zone

The island of Crete in the forearc of the Hellenic subduction zone has a rugged topography with local relief exceeding 2 km. Based on the elevation of marine shorelines, rates of rock uplift during the Late Holocene were previously estimated to range between 1 and 4 mm/a in different parts of the island. These rates may, however, not be representative for longer timescales, because subduction earthquakes with up to 9 m of vertical coseismic displacement have affected Crete in the Late Holocene. Here we use a well preserved sequence of marine terraces near Kato Zakros in eastern Crete to determine the rate of rock uplift over the last ∼600 ka. Field investigations and topographic profiles document a flight of more than 13 marine bedrock terraces that were carved into limestones of the Tripolitza unit. Preliminary age constraints for the terraces were obtained by ¹⁰Be exposure dating of rare quartz-bearing sandstone clasts, which are present on some terraces. The ¹⁰Be ages of these samples, which have been corrected for an inherited nuclide component, yielded exposure ages between ∼100 ka and zero. Combined with geomorphologic evidence the two oldest ¹⁰Be ages suggest that the terraces T₄ and T₅, with shoreline angles at an elevation of ∼68 and ∼76 m above sea level, respectively, formed during the marine isotope stage 5e about 120 ka ago. The correlation of the higher terraces (T₆ to T₁₃) with regional sea-level highstands indicates sustained rock uplift at a rate of ∼0.5 m/ka since at least ∼600 ka. As normal faulting has dominated the tectonics of Crete during the last several million years, upper crustal shortening can be ruled out as a cause for rock uplift. We argue that the sustained uplift of the island results from the continuous underplating of sediments, which are transferred from the subducting African plate to the base of the crust beneath Crete.     

Luminescence from glacimarine sediment-trap samples at the Antarctic Peninsula

Radiocarbon (¹⁴C) dating yields variable and high reservoir and core-top ages for glacimarine sediments around Antarctica. To test the suitability of luminescence as an alternate dating method we investigated the effectiveness of clock zeroing (by daylight) within fine-silt-size siliciclastic sediments from year-long vertical-array sediment traps in Andvord Bay and Brialmont Cove at the Antarctic Peninsula. Both long-bleach and short-bleach multi-aliquot IR-PSL (infrared photon stimulated luminescence) and single-aliquot, post-IR blue-PSL dating tests were conducted. As well, dual-bandwidth-bleaching thermoluminescence (TL) tests were performed on samples from Brialmont Cove. These TL bleaching tests indicate that silt from the middle and bottom traps at this site has had little or no exposure to daylight, but that silt from the top trap has had some exposure. All 24 samples (representing different seasons and different trap depths) exhibit anomalously old apparent ages (12 ka–60 ka) across annual seasons and depths of deposition when either long-bleach multi-aliquot or late-background-subtraction single-aliquot PSL procedures were employed. Thus regional bottom silts would be unsuited for dating by these two luminescence dating approaches. However, a short-bleach multi-aliquot IR-PSL procedure yields the expected zero ages for several samples, a promising result that requires further exploration.     

Dating Holocene lavas on Stromboli,Italy using cosmogenic He

In-situ cosmogenic ³He exposure ages of pyroxene phenocrysts from basalts from the Upper Neostromboli formation in southwest Stromboli date its eruption at 7.0 ± 0.3 ka (1σ, n = 3, Ginostra site) and 6.8 ± 0.2 ka (1σ, n = 10, Timpone del Fuoco site) respectively. Correlation of our new data to previous K/Ar and palaeomagnetic ages from the northwestern Neostromboli phase suggests that it erupted within a confined period between roughly 6 and 14 ka. The low uncertainty on the ³He_cos ages as well as on individual exposure ages (4.4–8.7%) demonstrates that ³He_cos exposure dating is a viable tool for dating Holocene basalt lavas. The ages compare favourably to uncertainties obtained for radiocarbon dating of similar rocks.     

Non-steady long-term uplift rates and Pleistocene marine terrace development along the Andean margin of Chile (31°S) inferred from 10Be dating

Pleistocene uplift of the Chilean coast is recorded by the formation of wave-cut platforms resulting from marine erosion during sea-level highstands. In the Altos de Talinay area (~ 31°S), we have identified a sequence of 5 wave-cut platforms. Using in situ produced ¹⁰Be exposure ages we show that these platforms were formed during interglacial periods at 6, 122, 232, 321 and 690 ka. These ages correspond to marine isotopic stages (MIS) or substages (MISS) 1, 5e, 7e, 9c and 17. Shoreline angle elevations used in conjunction with our chronology of wave-cut platform formation, illustrate that surface uplift rates vary from 103 ± 69 mm/ka between 122 and 6 ka, to 1158 ± 416 mm/ka between 321 and 232 ka. The absence of preserved platforms related to the MIS 11, 13 and 15 highstands likely reflects slow uplift rates during these times. We suggest that since 700 ka, the Altos de Talinay area was predominantly uplifted during 2 short periods following MIS 17 and MISS 9c. This episodic uplift of the Chilean coast in the Pleistocene may result from subduction related processes, such as pulses of tectonic accretion at the base of the forearc wedge.     

MET-post-IR IRSL luminescence dating of cobbles buried in fluvial terraces in the Northern Chinese Tian Shan

Cobbles can be used as an alternative to the conventionally employed sand-sized mineral luminescence dating. In piedmont environments, cobbles are much more abundant than sand-sized material. The IRSL₅₀ signal has been widely used in previous studies due to its greater sensitivity to exposure events. However, it is well known that the low temperature IRSL signal is more prone to fade than elevated temperature post-IR IRSL signal. In this study, to test the reliability and applicability of cobble sub-surface elevated temperature IRSL luminescence dating, six light-color granite cobbles and two sand-sized samples from silty sand lens were collected from a high terrace of Manas River on the northern piedmont of Chinese Tian Shan. A modified multi-elevated-temperature post-infrared infrared stimulated luminescence (MET-post-IR IRSL) protocol was applied. The age-temperature (A-T) plateau of MET-post-IR IRSL measurement was combined with the conventional age-depth (A-D) plateau in luminescence-depth profile to evaluate the resetting and fading of MET-post-IR IRSL signals. Uncertainties of grain-sizes of K-feldspar within solidified slices were also explored by μ-XRF mapping of potassium content. The A-T plateau was identified between MET-post-IR IRSL₁₇₀ and MET-post-IR IRSL₂₂₅ signals of one cobble, which suggested completeness of bleaching before burial and negligible anomalous fading during burial. This cobble yielded MET-post-IR IRSL₂₂₅ ages of 15.8 ± 2.6 ka and 19.0 ± 3.2 ka for top and bottom side, respectively. These MET-post-IR IRSL₂₂₅ ages were consistent with independent coarse-grained quartz MAM OSL ages (15.7 ± 3.6 ka and 14.8 ± 2.6 ka) of two sand-sized samples. The MET-post-IR IRSL₂₂₅ age of 16.0 ± 1.2 ka for the bottom side of another cobble was also consistent with the independent age, even without the A-T plateau. It was inferred to be caused by anomalous fading of MET-post-IR IRSL signals other than that stimulated at 225 °C by refering to the A-D plateau observed. Our results show that MET-post-IR IRSL measurement can be employed to determine the burial ages of cobbles. The A-T plateau, complemented with the A-D plateau, could be used to assess the reliability of burial ages of cobble luminescence dating from the view of bleaching and fading.     

Luminescence dating of baked earth and sediments from the Qujialing archaeological site,China

The Qujialing site is a representative Neolithic archaeological site in the middle reaches of the Yangtze River, China. Absence of suitable material for radiocarbon dating in this region makes the timing of the similar sites difficult. Here we applied optically stimulated luminescence (OSL–SAR) and thermoluminescence (TL–SAR) techniques to date the archaeological and natural deposits from the Qujialing site with known age, testing the techniques on samples at archaeological sites in this region. The results showed that the luminescence properties of quartz from sediment and baked earth samples are very similar. The quartz OSL ages obtained for a sediment sample and a baked earth sample from the cultural layer are 5.4 ± 0.3 and 5.1 ± 0.3 ka, respectively. The quartz TL age of the baked earth sample is 5.6 ± 0.5 ka. These dates are consistent with the calibrated radiocarbon ages (4.9 ± 0.1 and 5.1 ± 0.1 ka cal BP (±1σ)) of the two charcoal samples from the cultural layer at a nearby locality, and are also in agreement with the age of Qujialing culture period. The results indicate that the OSL dating techniques can be applied to date similar archaeological sites in the middle reaches of the Yangtze River, China.     

U–Pb dating of speleothems from Spannagel Cave,Austrian Alps: A high resolution comparison with U–series ages

U–Pb dating is increasingly used to date speleothems that are too old for precise U–Th disequilibrium dating; however there is little data that can independently validate its application to such material. This study presents U–Pb ages for speleothems from the Spannagel Cave in the Austrian Alps including a detailed comparison with U–Th ages from an unusually U–rich sample that yields precise ages by both methods. Sample SPA4 is a flowstone with three growth phases separated by distinct hiatuses. For the youngest growth phase the U–Pb and U–Th ages are 267 ± 1 ka and 267 ± 5 ka respectively; the middle growth phase is 291 ± 1 versus 295 ± 11 ka while for the oldest growth phase a single sub-sample, assuming the same initial Pb composition as for the younger phases, yields an age of 340 ± 2 ka compared to 353 ± 9 ka by U–Th. Correlation of these ages with the marine isotope stages confirms that these speleothems grew during glacial stages as suggested by previous work on the same sample. Sample SPA 15 has U–Th isotopic compositions indistinguishable from secular equilibrium; the U–Pb data on the main growth phase of this sample give an age of 551 ± 10 ka, whereas a single analysis from the oldest phase suggests it may be on the order of 40 ka older. This detailed comparison of U–Pb and U–Th ages provides important support for the potential validity of the U–Pb method in older samples beyond the range of U–Th.     

Quartz OSL dating of archaeological sites in Xiao Qaidam Lake of the NE Qinghai–Tibetan Plateau and its implications for palaeoenvironmental changes

In the past decades, archaeologists have found evidences for prehistorical human activity in the Qinghai–Tibetan Plateau (QTP). In 1982, some Paleolithic stone tools were found in a section from a terrace of the Xiao Qaidam Lake in the Qaidam Basin, NE of the QTP. The age of this Paleolithic site has remained unknown by far. Some believed that the age of human inhabitation in this Paleolithic site was about 30 ka. In this study, quartz optically stimulated luminescence was used to date 10 samples collected from four sections in the Xiao Qaidam Lake, using the single-aliquot regeneration-dose protocol. The two samples from section XCDH2, which is from a lake terrace about ～7–8 m above the present lake level and in which the top gravel layer contains stone tools, were not well-bleached before deposition. Their ages (>101 and >159 ka) determined by SAR should be considered minimums. OSL dating results of six samples from two sections (XCDH1 and XCDH3) of an adjacent lake terrace, which is ～12 m above the present lake level, suggest two possibilities for the age of the tool-bearing gravel layer: (1) younger than ～3 ka if the lake terrace of XCDH2 is younger than the terrace represented by XCDH1 and XCDH3; or (2) between ～3 and 11 ka if these two terraces are part of the deposit of the same time period. In either case, the age of the archaeological layer should be much younger than the previously proposed ～30 ka. As the climate in the early Holocene after 11 ka was increasingly warm and the Xiao Qaidam Lake area could be suitable for human inhabitation then, we deduce that the age range of ～3–11 ka is more likely the time frame for this archaeological site. The age of 3.1 ± 0.3 ka for the surface of terrace XCDH1/XCDH3 suggests a significant lake level decrease after this time and a corresponding arid event at ～3 ka; the lake level did not reach this level again after that time. Section XCDH4 is more than 40 m above the present lake level, and two samples gave ages of 37 ± 4 and 51 ± 4 ka. These two dates and the dates from the other sections demonstrate that two lake levels higher than present existed for Xiao Qaidam Lake, one at ～12 m and dated ～3–11 ka and the another at >40 m and dated ～37–51 ka.