共查询到19条相似文献,搜索用时 62 毫秒
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从柑桔皮中提取色素联产果胶的新工艺 总被引:7,自引:0,他引:7
用乙醇浸取柑桔皮经石油醚萃取和乙醇精制得油溶性色素和水溶性色素,残渣经酸水解、醇沉析制取果胶。果胶收率6%,质量符合GBn246-85标准,色素收率117%,含砷量≤0.00015%,含铅量≤0.0003%。 相似文献
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The extraction of pectin from orange peels has been studied using microwave and conventional extraction, with operating conditions including different extraction periods, different solvent pHs, and different types of solvent systems. The extracted pectin from orange peels was initially precipitated with concentrated ethanol and was quantified by the carbazole assay. For microwave extraction, the greatest total amount of pectin yield was found to be 5.27% on a dry basis for 15 minutes of extraction, although the greatest amount of material per unit time (%/min) was obtained after 5 minutes. This amount was the same as that extracted using Soxhlet extraction for three hours. The 15-minute microwave extraction period was further investigated at pH values of 1.5, 2.0, 5.5, and 10.0. The greatest amount of pectin was extracted from orange peels at the most strongly acidic condition of pH 1.5. The effect of a solvent system containing ethanol and EDTA (ethylenediamine tetraacetic acid) with a 15-minute extraction period and a pH of 1.5 was studied, giving approximately double the amount of pectin extracted using distilled water. 相似文献
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The extraction of pectin from orange peels has been studied using microwave and conventional extraction, with operating conditions including different extraction periods, different solvent pHs, and different types of solvent systems. The extracted pectin from orange peels was initially precipitated with concentrated ethanol and was quantified by the carbazole assay. For microwave extraction, the greatest total amount of pectin yield was found to be 5.27% on a dry basis for 15 minutes of extraction, although the greatest amount of material per unit time (%/min) was obtained after 5 minutes. This amount was the same as that extracted using Soxhlet extraction for three hours. The 15-minute microwave extraction period was further investigated at pH values of 1.5, 2.0, 5.5, and 10.0. The greatest amount of pectin was extracted from orange peels at the most strongly acidic condition of pH 1.5. The effect of a solvent system containing ethanol and EDTA (ethylenediamine tetraacetic acid) with a 15-minute extraction period and a pH of 1.5 was studied, giving approximately double the amount of pectin extracted using distilled water. 相似文献
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液膜法提取单质金的迁移机理及其应用 总被引:6,自引:0,他引:6
本文研究了用磺化煤油作稀释剂时磷酸三丁酯从王水溶液中萃取Au的萃合比,证明了溶液中HNO或NO^-3在酸度小于3.0mol/dm63时对TBP萃取Au的萃合比没有影响,分析了液膜选择性迁移Au的机理;研究了以TBP为载体的乳状液膜以王水为介质的含Au,Cu,Ni的电镀废水中的选择性回收Au,内水相得到纯度99.95的黑色粉末单质Au,一级回收率为99.9%。. 相似文献
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从表面化学的观点浅析涂膜内物料流动引起表面张力梯度的出现是产生汽车面漆桔皮缺陷的根本原因,提出了解决漆膜桔皮缺陷需要从材料、工艺、设备着手,并重点指出手工喷涂中排除桔皮的方法。 相似文献
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