低辐射卷绕镀膜工艺在线透过率监控技术

介绍了卷绕镀膜生产线中镀膜工艺的透过率在线监控仪原理与实现方法,同时描述了透过率监控仪在低辐射卷绕镀膜中的应用.     

in situ failure detection in thick film multilayer systems

By means of in situ e.m.f.-measurements, leakage current measurements and impedance spectroscopy, it has been possible for the first time to detect spontaneous and forced blistering in thick film multilayers during formation at high temperatures. Also the occurrence of high temperature shorts in Ag-dielectric-Ag multilayers under DC-bias was detectable.     

Influence of insoluble excipients on film coating systems

Insoluble excipients are added to polymeric film coating solutions and dispersions to improve the physical appearance of dosage forms, enhance the stability of photolytic drugs, and aid in processing. These insoluble additives, however, may significantly affect the physical, mechanical, adhesive, and drug-release properties of the films. In this review, the theories of the interactions between polymer and insoluble excipient are addressed. This article also discusses the influence of the concentration, particle size, morphology, and surface chemistry of insoluble excipients on the various polymer properties.     

Effect of a bell-shaped cover in spin coating process on final film thickness

Thin polymer films can be prepared by spin coating with thicknesses ranging from nanometers to micrometers. The film thickness is controlled by concentration of the polymer solution, molar mass of the polymer and spinning speed. The patented GYRSET system for spin coating applications provides a fundamental modification. The bell-shaped cover minimizes air turbulences inside the process chamber; therefore, better uniformity of the layer is produced. This leads to highly reproducible results, uniform coverage, and reliable and uniform material application, in particular at lower spin speeds. We focus on the question how does the GYRSET system change the final film thickness. In particular, we have investigated modifications of the existing spin coat equation for solutions of polystyrene dissolved in toluene using the GYRSET system. In addition, we compare homogeneity of films prepared by open spin coating and GYRSET systems. Received: 9 October 2000 / Reviewed and accepted: 10 October 2000     

镀膜装置蒸发源发射形态与膜厚分布

蒸发源是真空镀膜装置中一个非常重要的部件。在多个蒸发源共存的装置中,如何在设计中正确选择蒸发源与蒸发源、蒸发源与基片之间的距离就显得尤为重要,它直接关系到基板涂层均匀性。本篇文章根据蒸发源与基片之间的物理联系入手,分析基片--蒸发源距离对基片涂层均匀性的影响,进而对蒸发源与蒸发源、蒸发源与基片之间距离的确定,提出了自己的一些观点和看法。     

Optical coating synthesis by simultaneous refractive-index and thickness refinement of inhomogeneous films

A fast, efficient thin-film synthesis technique is described. Dielectric films are subdivided into thin layers whose refractive indices and thicknesses are varied simultaneously. Because of the large number of optimized parameters, speed and accuracy are given special attention. The efficiency of the method is demonstrated by the successful reproduction of several complex nonpolarizing filters synthesized in the past with the needle method, one of the best approaches currently available.     

Optical monitoring of the end point in thin film plasma etching

An in-process optical technique is described for accurately monitoring the end point in plasma etching processes. A grating pattern is lithographed somewhere in the film to be etched. The grating modulation decreases as the film is etched out and the process may be monitored by measuring the diffraction of a low power He-Ne laser beam aimed at the grating. The etching end point is accurately detected by the disappearance of all diffracted orders. The laser beam does not need to be directed at normal incidence and so any available plasma etching equipment is suitable. The detection is carried out with low cost photovoltaic detectors but simple visual inspection is satisfactory also.Comparative experimental results are presented.     

Terahertz paintmeter for noncontact monitoring of thickness and drying progress in paint film

We propose a paintmeter for noncontact and remote monitoring of the thickness and drying progress of a paint film based on the time-of-flight measurement of the echo signal of a terahertz (THz) electromagnetic pulse. The proposed method is effectively applied to two-dimensional mapping of the painting thickness distribution for single-layer and multilayer paint films. Furthermore, adequate parameters for the drying progress are extracted from the THz pulse-echo signal and effectively applied to monitor the wet-to-dry transformation. The THz paintmeter can be a powerful tool for quality control of the paint film on the in-process monitoring of car body painting.     

In situ monitoring of microfracture during plasma spray coating by laser AE technique

Atmosphere plasma spray coating materials include many pores and lamellar boundaries formed by flattened particles during spraying process although high reliability are required in ceramic coatings for turbines. These boundaries become an origin of the microcracks and following crack growth. As it is known that spraying parameters strongly affect the microstructure and strength of coating, it is expected to establish in situ monitoring technique for coating process. However, there is a limit to apply the existing non-destructive evaluation techniques to real-time monitoring at elevated temperature. We have investigated a non-contact measuring system to detect acoustic emission (AE) signals due to microfractures using a laser interferometer, and applied this technique for understanding microfracture process of ceramic coating at elevated temperature. In this paper, we evaluated the effect of several spraying parameters on the initiation and growth process of microcrack by detecting AE signals during coating process using a non-contact laser AE technique.     

In situ monitoring of microfracture during plasma spray coating by laser AE technique

Atmosphere plasma spray coating materials include many pores and lamellar boundaries formed by flattened particles during spraying process although high reliability are required in ceramic coatings for turbines. These boundaries become an origin of the microcracks and following crack growth. As it is known that spraying parameters strongly affect the microstructure and strength of coating, it is expected to establish in situ monitoring technique for coating process. However, there is a limit to apply the existing non-destructive evaluation techniques to real-time monitoring at elevated temperature. We have investigated a non-contact measuring system to detect acoustic emission (AE) signals due to microfractures using a laser interferometer, and applied this technique for understanding microfracture process of ceramic coating at elevated temperature. In this paper, we evaluated the effect of several spraying parameters on the initiation and growth process of microcrack by detecting AE signals during coating process using a non-contact laser AE technique.     

Elimination of cumulative effect of thickness errors in monochromatic monitoring of optical coating production: theory

We propose an algorithm for correcting deposition termination levels that allows elimination of the cumulative effect of errors in previously deposited layers. For the application of this algorithm at least one monitoring signal extremum should be registered during a layer deposition. We also derive a theoretical relation for the estimation of errors in layer refractive indices based on the results of on-line monitoring measurements. At least two monitoring signal extrema are required for its application.     

Optical fibre sensors for health monitoring of bonded repair systems

In the aircraft industry the use of externally bonded composite repairs has become an accepted way of repairing fatigue, or corrosion, damaged metallic structural components. However, current NDI and damage assessment techniques for composite repairs are passive and generally performed on ground. The challenge is to develop new techniques utilising recent analytical and experimental tools. This report examines the use of optical fibre sensors. Optical fibres offer a means of monitoring the load transfer process in these repairs, and can therefore be used to provide an indication of the integrity of the repair. This paper describes the use of an array of fibre Bragg grating strain sensors (FBGs) for the in situ monitoring of bonded repairs to aircraft structures and, in particular, the monitoring of crack propagation beneath a repair. In this work the FBGs have been multiplexed using a combination of wavelength and spatial techniques employing a tunable Fabry–Pérot (FP) filter to track individual gratings. The multiplexed FBGs were then surface-mounted on a boron–epoxy unidirectional composite patch bonded to an aluminium component. The sensors were located so as to monitor the changing stress field associated with the propagation of a crack beneath the patch. The ability of relating experimental results to sensor readings is then confirmed using both a thermo-elastic scan of the patch and 3D finite element analysis.     

Flexible ceramic-reinforced polyurethane composite coatings on synthetic fibres: Process of continuous liquid film coating and its influence on the coating thickness

A concept for the realisation of composite layers on the surface of synthetic fibres by continuous liquid film coating of spread roving or monofilaments with a slurry containing ceramic particles and a polymeric binder is successfully demonstrated. Polyamide 6 monofilaments were coated with alumina particles and a polyurethane elastomer based binder system to achieve higher abrasion resistance. Under frictional load, the coating is abraded in small units consisting of some particles and the surrounding polyurethane matrix, which predetermines it to be used as sacrificial layer. The slurries showed shear thinning behaviour. Increasing the content of the rheological agent (carboxymethylcellulose [CMC]) led to an exponential increase of the viscosity, which therefore can be tailored by varying the CMC content. An increase of fibre radius, slurry viscosity or withdrawal speed led to an increase of the coating thickness, which is in accordance to published results of Newtonian or non-Newtonian coating fluids.     

Out-of-autoclave cure cycle study of a resin film infusion process using in situ process monitoring

Liquid resin infusion (LRI) of textile tailored reinforcements (TRs) is increasingly applied in new processing technologies for manufacturing carbon fibre composites. This work presents a cure cycle study of an out-of-autoclave toughened resin film infusion (RFI) process as part of the examination of an alternative manufacturing process for composites. To successfully produce laminates using resin film infusion in combination with a fast-curing process, the flow behaviour of the selected resin material under changed processing conditions was investigated. The effect of processing parameters, specifically heating rates and dwell times, on resin viscosity and laminate infiltration was evaluated through experimental work and supported by in situ process monitoring. A DC-resistance sensor system was applied to track the change in resin viscosity during cure. Results showed that cure cycles with a relatively short dwell time and higher heating rate compared to an autoclave cure led to enhanced flow properties of the toughened resin system. High quality laminates, comparable to autoclave panels, were manufactured with vacuum pressure only by modifying the original vacuum bagging arrangement.     

Investigation of the effect of accumulation of thickness errors in optical coating production by broadband optical monitoring

We present a theoretical approach enabling one to perform a preproduction investigation of the effect of accumulation of thickness errors in the course of optical coating production using broadband optical monitoring. On the basis of this approach we investigate and compare thickness errors that may be associated with such factors as random and systematic errors in measurement data, instabilities of deposition rates, and inaccuracies of on-line algorithms predicting termination instants for layer depositions.