共查询到18条相似文献,搜索用时 78 毫秒
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为考察狼牙刺花中生物碱的含量,采用酸性乙醇提取生物碱,以苦参碱为对照品,溴甲酚绿为显色剂,在缓冲溶液pH为3.05条件下,用紫外分光光度法于416 nm处测定狼牙刺花中生物碱含量。结果表明,测定在1.1111~5.5556 mg/L范围内,线性关系良好,回归方程为A=0.0861C-0.0303,r=0.9995(n=5);平均加标回收率为96.89%,RSD为2.03%(n=6);狼牙刺花中生物碱的平均含量为0.2159%。该实验验方法操作简便、快速,测定结果准确、可靠。 相似文献
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本文采用紫外分光光度法测定磷酸氯喹注射液的含量。方法简便,重现性较好。平均回收率为100.56%RSD=0.06%。 相似文献
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Guosong Wang Qiue Cao Xiufang Zhu Xueqiong Yang Minghui Yang Zhongtao Ding 《应用聚合物科学杂志》2009,113(5):3049-3058
On the basis of the non‐covalent interaction between template and monomer, porous molecularly imprinted polymers (MIPs) were synthesized by a thermal‐initiated polymerization method using huperzine A as template, acrylamide, or methacrylic acid as function monomer, ethylene glycol dimethacrylate as cross‐linking agent. The interaction between template and functional monomers was studied by UV spectrophotometry, which showed a formation of huperzine A‐monomer complexes with stoichiometric ratio of 1 : 2 in the pre‐polymerized systems. The resultant MIP particles were tested in the equilibrium binding experiment to analyze their adsorption ability to huperzine A, and were characterized by Fourier Transform Infrared (FTIR) study. The recognition properties of MIP were estimated in solid‐phase extraction by selecting four compounds (isolated from the Chinese herb Huperzia serrata) as substrates, and were compared with and prior to those of the NIP. High affinity and adsorption of MIP1 which was prepared in chloroform with huperzine A as imprinted molecule, and acrylamide (AM) as functional monomer, made an attractive application of MIP1 in separation processes. In final, using MIP1 solid‐phase extraction micro‐column, huperzine A was enriched and separated from the real extraction sample of Huperzia serrata. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009 相似文献
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猫眼草不同药用部位总黄酮含量测定 总被引:3,自引:0,他引:3
用60%乙醇超声提取猫眼草根、茎、叶不同部位中的总黄酮,并以芦丁为对照品,用紫外分光光度计在510 nm处测定不同药用部位中总黄酮的含量。结果表明,芦丁标准溶液浓度在12.5~50μg/mL与吸光度呈良好的线性关系,线性回归方程为Y=0.011 5X-0.023 5,r=0.999 4(n=5),全草的平均回收率为99.60%,RSD为1.60%。测得猫眼草根、茎、叶中黄酮含量分别为20.30,16.32,23.53 mg/g,叶中的总黄酮含量比根、茎含量高。 相似文献
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基于紫外分光光度法测定氮含量,建立了酪氨酸手性固定相键合量测定方法。探究了测定干扰因素,探讨了过滤介质、静置时间、沉淀剂用量对测定的影响。结果表明,体系中的硅酸根、碳酸根在220 nm处产生干扰,以氯化镁(氯化钙)沉淀排除。孔径〈0.45μm针式过滤头过滤、静置时间60 min、沉淀剂(1 mol/L)用量3 mL条件下,能准确测定酪氨酸手性固定相键合量,方法 RSD〈2%,加标回收率98.0%~104%,并与元素分析法比较,相对误差3.7%。该方法准确可靠,提供了一种元素分析法之外的参考方法。 相似文献
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分析磷矿石的物理化学特性,考察多种磷矿石试样的溶解方法,探讨柠檬酸-硝酸铝混合溶剂溶解磷矿石的反应机理,借助示差光度法提出了快速准确测定磷矿石中高含量全磷的新方法.试验表明,此方法测定结果与磷钼酸喹啉重量法分析结果相符,其RSD(相对标准偏差)<5%(n=6). 相似文献