共查询到19条相似文献,搜索用时 15 毫秒
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Ti─17合金高温变形机理研究EI 总被引:9,自引:1,他引:8
用热模拟压缩试验研究了Ti-17合金高温变形特点,通过金相组织和TEM观察发现,β区变形是以扩散回复型变形机制占主导地位;高应变速率下只发生动态回复;低应变速率下发生连续再结晶。(α+β)区变形是界面滑移,高应变速率下易发生动态再结晶。试验还确定了变形激活能Q和应变速率敏感因子m值,β和(α+β)区中分别为161kJ/mol、437kJ/mol和0.32、0.25。 相似文献
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以Mg-9Gd-3Y-0.3Zr合金为研究对象,采用热模拟等温压缩的试验方法,利用Arrhenius关系式,分析了合金应力与应变的关系,同时利用金相显微镜和扫描电镜,观察合金在热变形过程中组织的演变。结果表明,合金高温等温压缩变形的真应力-真应变曲线属于动态再结晶型,并且当应变速率ε一定时,温度升高,峰值流变应力下降,当温度一定时,应变速率ε增大,峰值流变应力和它所对应的应变值均提高;变形过程中随着温度的升高,合金发生不同程度的再结晶。当变形温度为623K时,组织变化以动态回复为主,变形温度提高到673K,开始出现再结晶现象,温度达到773K时得到完全再结晶组织。 相似文献
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为研究工业纯钛的动态再结晶行为,利用Gleebe实验机对工业纯钛在变形温度为700,800,900和950℃及应变速率为0.01,0.1,1和5s-1的条件下进行热模拟压缩实验。应用加工硬化率对实验得到的应力-应变数据进行处理,结合变形后材料微观组织的分析,求得工业纯钛的动态再结晶临界条件。结果表明,工业纯钛在热变形过程中发生了回复与再结晶;发生动态再结晶时,再结晶临界应变随温度的升高及变形速率的降低而减小。将lnθ-ε曲线的拐点处对应的应变作为材料的再结晶临界应变是合理的,工业纯钛动态再结晶临界应变εc与峰值应变εp之间满足εc=0.485εp。 相似文献
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Ti-6Al-2Zr-1Mo-1V合金热变形激活动态再结晶的临界条件识别及表征 总被引:1,自引:0,他引:1
热压缩实验获得Ti-6Al-2Zr-1Mo-1V合金在温度1073~1323K,应变速率0.01~10s-1条件下的真应力-应变曲线,以此作为识别及表征动态再结晶临界条件的底层数据。对比分析流变应力曲线发现高温、低应变速率下动态回复型软化态势显著;低温、高应变速率下动态再结晶型软化态势显著。引入材料加工硬化率θ,结合θ-σ曲线拐点判据识别了流变应力曲线隐含表征激活动态再结晶的特征参量:临界应变、临界应力。采用含动态再结晶激活能Q的Arrhenius方程求得α、β、n1、n2等材料常数并获得该合金动态再结晶激活能对应变速率及温度的响应图。进一步引入表征动态再结晶临界条件的临界应变模型,获得了临界应变与各热力参数之间的数学关系,验证表明该临界模型预测精度最大为12.9%。 相似文献
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本报道Nb,Ti微合金钢的热变形动态模拟变形抗力模型。在试验中用热加工模拟试验机进行高温压缩试验,其变形温度为1123-1423K,变形速率为0.1-60s^-1。结果表明,在峰值以前该钢种的流变应力数学模型为:σ=5.99.ε^0.167·ε^(6.47×10^-5·T)·exp(4064/T)。形变激活能(Q)为444kj/mol,0β系数为0.080。峰值应力(σp),临界应变(εc)和… 相似文献
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通过Gleeble-3800热压缩模拟试验机对TB17钛合金β相区进行热压缩实验,研究该合金β相区的动态再结晶行为及转变机理。结果表明:TB17钛合金在β相区变形时会发生动态回复(DRV)与动态再结晶(DRX)。不同应变速率下存在两种动态再结晶形核位置,低应变速率下主要在晶粒内部形核,高应变速率下主要在晶界附近形核。通过EBSD和TEM分析可知,在低应变速率下发生连续动态再结晶(CDRX),其发生的主要形式为亚晶合并转动。高应变速率下发生不连续动态再结晶(DDRX),发生的主要形式为晶界剪切伴随着亚晶转动。尽管两种动态再结晶的转变方式不同,其本质都是通过位错的增殖、滑移和胞状结构演化形成新的动态再结晶晶粒。 相似文献
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通过高温等温压缩试验,对Cu-Ni-Si-Ag合金在应变速率为0.01~5s-1、变形温度为600~800℃的动态再结晶行为以及组织转变进行了研究。结果表明,在应变温度为750、800℃时,合金热压缩变形流变应力出现了明显的峰值应力,表现为连续动态再结晶特征。同时从流变应力、应变速率和温度的相关性,得出了该合金高温热压缩变形时的热变形激活能Q和流变应力方程。并综合考虑应变速率与温度的影响,采用动态材料模型建立了该合金的热加工图,并利用热加工图分析了该合金不同区域的高温变性特征以及组织变化。 相似文献
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将Mg-8Gd-0. 5Zr合金在350~500℃、应变速率为0. 002~1 s~(-1)范围内进行热压缩实验,研究合金的流变应力行为,观察热压缩后的组织,分析动态再结晶晶粒尺寸和温度的关系,并利用加工硬化率的方法计算合金的再结晶临界应变(εc)。结果表明:Mg-8Gd-0. 5Zr合金热压缩流变曲线符合动态再结晶的特征,随着温度升高或者应变速率的减小,峰值应力下降,且峰值应力对应的峰值应变(εp)也降低。在350~450℃范围内,再结晶晶粒细小,且其随温度升高增长较慢;而温度在450~500℃范围内,再结晶晶粒尺寸迅速长大至约25μm。根据加工硬化率的计算及组织分析,发现动态再结晶先于峰值应变发生,峰值应变和临界应变的关系为ε_c=0. 442εp,同时构建了再结晶的临界模型。 相似文献
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在形变温度为1133K、形变速率为2×10~(-3)s~(-1)的试验条件下,采用两段加载拉伸试验方法研究了0.4%C-1.5%Mn钢高温变形后的静态软化行为.调查了由两次加载拉伸变形时的屈服应力求得的静态软化率以及相对峰值应力比和峰值应变比随等温保持时间的变化.详细讨论了动态回复组织和动态再结晶组织对高温变形后的静态软化过程的影响. 相似文献
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Zeynab Aalipour Abbas Zarei-Hanzaki Ali Moshiri Daudi Waryoba Anna Kisko L. Pentti Karjalainen Hamid Reza Abedi 《Advanced Engineering Materials》2023,25(17):2300297
Herein, dynamic and postdynamic recrystallization behaviors of GWZ magnesium are investigated. Toward this end, the single-hit and double-hit hot compression tests are conducted under strain rate of 0.001 s−1 at 400 °C. The prestrains of 0.1 and 0.5 are considered to investigate the effect of interpass time (5–300 s) on the compressive strength level. At the low strain level of 0.1, the contribution of Hall–Petch effect is considerable due to the occurrence of static recrystallization. In addition, the rare earth texture component is eliminated during interpass annealing. This causes increasing the strength of the material during second pass of hot compression. In contrast, at higher imposed strain, the strength level decreases with increasing the interpass time of annealing. The high amount of strain is completely consumed and the remaining stored energy is not high enough to trigger the occurrence of static recrystallization. The occurrence of metadynamic recrystallization and subsequent growth are characterized. In addition, the texture does not change in respect of the intensity or numbers/types of components. Accordingly, the observed decreasing trend of the strength is justified relying on the occurrence grain growth. 相似文献
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A. R. Morgridge 《Bulletin of Materials Science》2002,25(4):291-299
Metadynamic recrystallization has been investigated in three plain carbon steels (ENIA, EN2 and EN24) through the use of hot
interrupted compression tests on a wedge plastometer. Holding time was 0.5 s between passes. Strain rates of 0.05 and 0.12/s
and small strain increments of 3, 5 and 7% were employed. Test temperatures were varied between 800 and 1100°C.
Various incremental and continuous stress strain curves were highlighted at different temperatures and strain rates for 3
steels, ENIA, EN2 and EN24, resulting in varying flow stresses and strains. Highest peak stress was 180 MPa for EN24 at peak
strain of 0.25 and 900°C, with a strain rate 0.12/s. Peak strain values for all steels at 1100°C was 0.133 at a strain rate
of 0.05/s and 0.15 at a strain rate of 0.12/s.
Strain accumulation resulted in dynamic and metadynamic recrystallization with refinement to about 15 μm for dynamic and 22
μm for metadynamic recrystallization. Fractional softening,X, decreased from 0.27 to 0.12 as recrystallization times in metadynamic recrystallization increased from 0.9 s to 1.5 s at
1100°C. Time for 50% metadynamic recrystallization was also reduced as temperature increased.
For ENIA, a drop from 10000 s to 20 s, as temperature increased from 800 to 1100°C was observed. For EN24 and EN2 steels,
a drop from 4000 s to 6 s for similar temperature rise was observed.
Metadynamic recrystallization (at strains higher than critical strain) is observed to be a strong function of strain rate
and a very weak function of temperature and strain. It significantly refined the austenite grain size prior to transformation. 相似文献
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Yasuyuki Hayakawa 《Science and Technology of Advanced Materials》2013,14(1):480-497
AbstractSince its invention by Goss in 1934, grain-oriented (GO) electrical steel has been widely used as a core material in transformers. GO exhibits a grain size of over several millimeters attained by secondary recrystallization during high-temperature final batch annealing. In addition to the unusually large grain size, the crystal direction in the rolling direction is aligned with <001>, which is the easy magnetization axis of α-iron. Secondary recrystallization is the phenomenon in which a certain very small number of {110}<001> (Goss) grains grow selectively (about one in 106 primary grains) at the expense of many other primary recrystallized grains. The question of why the Goss orientation is exclusively selected during secondary recrystallization has long been a main research subject in this field. The general criterion for secondary recrystallization is a small and uniform primary grain size, which is achieved through the inhibition of normal grain growth by fine precipitates called inhibitors. This paper describes several conceivable mechanisms of secondary recrystallization of Goss grains mainly based on the selective growth model. 相似文献
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根据形核热力学理论,分析了亚动态再结晶形核的热力学过程,导出亚动态再结晶的临界形核尺寸和形核功均小于动态再结晶的临界形核尺寸和形核功的结论。在变形温度1100℃和变形速率5×10~(-2)s~(-1)条件下对 Cr25Ti 铁素体钢进行双道次热模拟试验,试验验证了上述结论。由于动态再结晶组织中尺寸为 n~*′≤n相似文献
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在2618铝合金的基础上,添加Sc,Zr,降低Cu量,配制实验合金,采用金相,X-射线衍射,透射电镜,硬度测量等手段,研究了实验合金冷轧板材经不同温度退火组织性能的变化,探讨了Sc对实验合金再结晶过程与退火行为的影响规律,结果表明,Al3(Ac,Zr)质点钉扎位错,稳定亚结构,迟滞以亚晶聚合与长大为主的再结晶形核,同时也阻碍晶粒长大,因此,2618铝合金中添加Sc,Zr合金化可以提高再结晶温度;并细化再结晶组织,但Sc,Zr不宜过量,否则不利于稳定未再结晶组织,降低Cu量,虽然合金硬度下降,但是可能防止W相生成,要增添Sc,Zr含量,进一步推迟再结晶过程,提高再结晶温度。 相似文献