20MnTiB钢螺栓断裂失效分析

应用扫描电子显微镜、光学显微镜、显微硬度仪和电子探针X射线显微分析仪，对发射架20MnTiB高强度螺栓断裂件的金相组织、显微硬度、断口微观形貌和合金元素分布状态进行了分析。结果表明，断裂螺栓金相组织正常，力学性能符合技术要求；螺栓断裂失效是由于在螺栓根部存在因加工不当产生的初始裂纹，在初始裂纹尖端的应力集中和露天使用环境中水介质的共同作用下，螺栓发生应力腐蚀开裂。应力腐蚀开裂的方式是阳极溶解型。     

金属波纹管补偿器的应力腐蚀开裂分析

采用宏观及微观断口分析、金相检验与化学成分检测等方法,对某铬一镍奥氏体不锈钢波纹管补偿器的腐蚀开裂失效原因进行了分析。结果表明：由于该铬一镍奥氏体不锈钢波纹管在氯离子含量超标的环境中服役,并承受来自于波纹管自身加工变形过程中形成的残余应力、工作应力以及装配应力,最终导致波纹管补偿器发生了由表及里的应力腐蚀开裂。     

110钢级φ88.9mm×6.45mm超级13Cr钢油管刺穿失效分析

采用宏观分析、化学成分分析、力学性能测试、金相检验及扫描电镜断口分析等手段,对某油田一根规格为φ88.9mm×6.45mm的110钢级超级13Cr马氏体不锈钢油管的刺穿失效原因进行了分析。结果表明:油管失效的实质是油管发生了氯离子应力腐蚀开裂,裂纹起源于外壁腐蚀坑底部,从外壁向内壁扩展,直到穿透壁厚,形成刺穿通道,高压流体从内向外刺出并在随后的过程中形成了刺穿孔洞。     

1Cr18Ni9Ti不锈钢输油管道开裂原因分析

通过化学成分分析、宏观检验、金相检验和断口分析等方法对1Cr18Ni9Ti不锈钢液压油输送管道开裂原因进行了分析。结果表明:不锈钢管开裂为应力腐蚀开裂,裂纹起源于管道外壁并逐渐向内壁扩展;产生开裂的主要原因是工业水中氯、硫和氧等腐蚀性物质不断在钢管外壁沉积,在管道压力和腐蚀介质共同作用下,不锈钢管发生应力腐蚀开裂。     

Failure analysis of stress corrosion cracking in aircraft bolts

This research was conducted on the failure analysis of the failed clamp bolt from a helicopter engine in the RoKAF. Through the fractography, metallography, and stress analysis of the failed part, it was found that the clamp bolt was fractured by stress corrosion cracking due to the interaction of tensile residual stress and corrosive environment. The stress corrosion crack is a phenomenon that occurs in susceptible alloys and is caused by the conjoint action of a surface tensile stress and the presence of a specific corrosive environment. Therefore, it is recommended that the material of the clamp bolt should be changed to prevent similar failures.     

矩形脉动真空灭菌器内腔开裂原因

某医院矩形脉动真空灭菌器内腔发生开裂事故,通过宏观分析、金相检验和光谱分析等方法,结合工作介质,对内腔开裂的原因进行了分析。结果表明:灭菌器内腔与加强筋不连续焊接处存在焊接残余应力,且靠近内腔弯折处存在局部应力集中现象;灭菌器内腔的工作介质中含有氯离子,而氯离子水溶液是300系列不锈钢发生应力腐蚀开裂的敏感介质。灭菌器内腔在焊接残余应力、含氯离子介质等因素的综合作用下发生起始于靠近内腔弯折的焊接起始处的应力腐蚀开裂。     

Cracking in bolted SMC components

Recent developments in the substitution of plastics for metal components have led to a requirement for further information on the applicability of existing mechanical fastenings to these newer materials.The generic group of glass reinforced thermoset plastics known as ‘polyester moulding compounds’ has been found to be suitable for many replacement components, particularly in the automotive industry, but these materials are subject to cracking under certain loading conditions. The present work uses a simulated bolt loading technique to relate material thickness, bolt diameter, and support configuration to a limiting sustainable load. Acoustic emission methods are also used to relate the onset of cracking to the support conditions and the ultimate load.The conclusions suggest that, for the material studied, positioning of the fixing hole at least two hole diameters from the material edge and use of a material thickness/bolt diameter ratio $\text{≥3}$, should result in the equivalent mild steel bolt failing before cracking is initiated or ultimate composite failure occurs.     

Material influence on the stress corrosion cracking of rock bolts

Rock bolt stress corrosion cracking (SCC) has been investigated using the linearly increasing stress test (LIST). One series of experiments determined the threshold stress of various bolt metallurgies (900 MPa for 1355AXRC, and 800 MPa for MAC and MA840B steels). The high values of threshold stress suggest that SCC begins in rock bolts when they are sheared by moving rock strata. SCC only occurred for environmental conditions which produce hydrogen on the sample surface, leading to hydrogen embrittlement and SCC. Different threshold potentials were determined for a range of metallurgies.Cold work was shown to increase the resistance of the steel to SCC. Rock bolt rib geometry does not have a direct impact on the SCC resistance properties of the bolt, although the process by which the ribs are produced can introduce tensile stresses into the bolt which lower its resistance to SCC.     

螺栓夹持填充孔复合材料层压板层间应力分析

为了研究含螺栓复合材料层压板连接接头的层间应力分布规律,提出了采用填充孔形式和虚拟界面层方法求解层间应力,并建立了三维有限元模型对受面内压缩载荷的螺栓夹持填充孔层压板进行分析。结果表明:层压板层间应力集中不仅发生在孔边,还会在螺栓头边缘附近出现,且夹持力越大螺栓头边缘附近的层间应力集中越严重;合理的螺栓夹持力能改善孔边应力状态,提高孔边抵抗分层的能力,但无法改善螺栓头边缘附近的层间剪切应力集中状态。因此,在进行含螺栓夹持的层压板机械连接结构孔边层间强度设计时,也要考虑螺栓头边缘的层间剪切应力集中问题,以提高复合材料结构的安全性。     

Failure analysis of Integrated Nozzle Actuating System (INAS) cooling hydraulic pipeline

During post test disassembly of a developmental aero engine, a hydraulic pipeline was found fractured from near weld joint. The pipeline was manufactured from a α–β Titanium alloy and was welded using Tungsten Inert Gas Welding (TIG) technique. The pipeline was in service for approximately 100 h. Fractographic features of the surface revealed transgranular cracking mode with presence of corrosive elements near the outer wall. Crack branching was also observed on the pipeline near to the fractured surface. Evidences of corrosion pits along with microcracks were also present near to the fractured surface. From the evidences, it was corroborated that the pipe failure was due to synergistic effect of corrosion fatigue and stress corrosion cracking.     

超级13Cr不锈钢在磷酸盐完井液中的应力腐蚀开裂敏感性研究

超级13Cr不锈钢常应用于高温井段,为明确其在高温磷酸盐完井液中的腐蚀及断裂风险,通过慢速率应变拉伸试验(SSRT)和高温高压电化学测试等,结合扫描电镜研究了超级13Cr不锈钢在高温磷酸盐完井液环境中的应力腐蚀开裂敏感性。结果表明:超级13Cr不锈钢在高温磷酸盐完井液环境下具有一定的应力腐蚀开裂敏感性,其应力腐蚀开裂机制为阳极溶解型;随温度升高,超级13Cr不锈钢表面的钝化膜稳定性下降,点蚀敏感性增加,应力腐蚀开裂敏感性增大。     

SCC Behaviour of X-70 Pipeline Steel in Near-Neutral pH Solutions

The stress corrosion cracking (SCC) behaviour of X-70 pipeline steel in near-neutral pH solutions was studied via slow strain rate testing (SSRT). The results showed that the cracking mode of X-70 pipeline steel in near-neutral pH solutions was transgranular at different temperatures and applied potentials with the feature of quasi-cleavage. The pH value of the solution decreased with increasing the addition of CO2, which increased the susceptibility to SCC. SCC susceptibility increased as the applied potential moved towards the cathodic direction, suggesting that hydrogen induced cracking (HIC) dominated the cracking process at cathodic potentials. The slight decrease of pH values with decreasing temperature of the solution increased the susceptibility to SCC, which attributed to the change of solubility of CO2 in the solution at different temperatures. The propagating directions of SCC cracks were different at different potentials. At rather negative cathodic potentials, the cracks were almost perpendi     

应力作用下X80钢焊接接头在近中性pH值溶液中的电化学行为研究

管线钢近中性p H值环境应力腐蚀开裂(SCC)是管线失效的一种重要形式,但其发生机理仍不清楚,现场实际发现其易发生在焊缝附近。采用动电位极化和电化学阻抗技术研究了外加拉应力对X80钢焊接接头在近中性p H值溶液中电化学行为的影响。结果表明:应力使X80钢母材和焊缝的腐蚀电位负移,腐蚀电流密度增大,应力促进了母材和焊缝的阳极溶解和阴极反应;在弹性变形区间,外加应力没有破坏腐蚀产物膜的完整性,腐蚀产物膜电阻几乎不变,应力使腐蚀产物膜孔隙结构变大,促进侵蚀性离子向电极表面扩散,母材和焊缝的电荷转移电阻明显减小;由于组织结构的原因,焊缝的应力影响系数比母材的大,X80钢焊缝比母材有更强的应力敏感性。     

Stress Corrosion Cracking and Blue Brittleness of Rotor Steels in High Temperature Aqueous Solutions

The tensile behaviors of two bolt steels 20Cr12NiMoWV and 25Cr2MoV, and rotor steel 30Cr2Ni4MoV used in a nuclear power plant were studied at different temperatures up to 280 degreesC in air and aqueous solution. The results showed that blue brittleness occurred near 230 degreesC and 180 degreesC for steels 30Cr2Ni4MoV and 25Cr2MoV, respectively. No blue brittleness was found for the steel containing higher Cr content. Susceptibility to stress corrosion cracking.(SCC) for the steels in aqueous solution at the test temperatures was very low except at the blue brittleness temperature. At the blue brittleness temperatures, however, the susceptibility to SCC was very high.     

A Fracture Probability Competition Mechanism of Stress Corrosion Cracking

The stress corrosion cracking (SCC) of austenitic stainless steel was studied via polarization, slow strain rate and scanning electron microscope (SEM) techniques. Many SCC mechanisms have been proposed in which hydrogen embrittlement and passive film rupture-repassivation theories are generally accepted, but they can hardly explain the SCC mechanism of austenitic stainless steel in acidic chloride solution adequately, because the steel is in active dissolution state and cathodic polarization can prevent it from occurring. Our experiment shows that the anodic current increases the creep rate and decreases the plastic strength of the material on single smooth specimen as well as at the SCC crack tip. The fractured surface was characterized as brittle cleavage, while the surface crack of smooth specimen was almost vertical to the tensile strength, which can confirm that the cracks were caused by tensile stresses. A fracture probability competition mechanism of SCC was proposed on the basis of the experimental results combined with the viewpoint of ductile-brittle fracture competition. When the anodic dissolution current is increased to a certain degree, the probability of fracture by tensile stress will exceed that by shear stress, and the brittle fracture will occur. The proposed SCC mechanism can riot only explain the-propagation of SCC cracks but can explain the crack initiation as well. The strain on the surface distributes unevenly when a smooth specimen is deformed, so does the anodic current distribution. The crack will initiate at a point where the anodic current density is large enough to cause the material at a specific point to fracture in brittle manner.     

管线钢在近中性pH值溶液中的应力腐蚀

为研究不同强度管线钢在近中性土壤环境中的耐腐蚀性能,模拟近中性土壤环境,采用C型环试样进行浸泡试验、电化学试验(极化曲线)来研究X80和X100这2种高强度管线钢在近中性环境中的应力腐蚀行为,采用扫描电镜(SEM)、X射线衍射仪(XRD)对试验后的试样腐蚀形貌、产物、结构进行了分析。结果表明:在模拟近中性土壤环境下,耐点腐蚀性能X100>X80,加载应力试样<不加载应力试样; 2种材料均表现出应力腐蚀开裂(SCC)敏感性,SCC敏感性X100>X80,说明随着管线钢强度的提高,SCC敏感性增大;应力腐蚀机制为阳极溶解(AD)+氢脆(HE)。     

X65管线钢焊接接头在模拟浅表海水环境中的应力腐蚀试验研究

在海水环境中,由于海水从海底管道外管焊缝浸入,导致外管焊接接头断裂。为了研究可能导致X65外管焊接接头断裂的因素,应用慢应变速率拉伸试验(SSRT),通过应力-应变曲线、扫描电镜(SEM)等手段分析了3个X65管线钢焊接接头在空气及模拟浅表海水环境中的应力腐蚀性能。结果表明:在空气中X65钢焊接接头试样的延长量最大,达5.6 mm,在模拟海水中试样的延长量均减小,其中2号试样延长量最小,仅3.6 mm,表明试样在浅表海水中塑性变形能力降低;模拟海水中3个试样的应力腐蚀敏感性指数均处于有应力腐蚀倾向的范围;在空气中试样的断裂为韧性断裂;在浅表海水环境中试样的断裂为韧性断裂与脆性断裂的混合断裂,有应力腐蚀开裂的趋势;海水中含有的大量Cl~-导致焊接接头的应力腐蚀敏感性升高,失效风险增加。     

Influence of ring size on the restrained shrinkage behavior of ultra high performance fiber reinforced concrete

In order to evaluate the restrained shrinkage behavior of ultra high performance fiber reinforced concrete (UHPFRC), ring-tests with three different wall thicknesses and two different diameters of inner steel ring were performed. Partially exposed free shrinkage and tensile tests were carried out simultaneously to assess the theoretical elastic stress, stress relaxation, degree of restraint and potential for cracking in the concrete. Test results indicated that the UHPFRC ring specimen with a thicker steel ring demonstrated a faster theoretical cracking time, higher stress relaxation and degree of restraint than that of a thinner steel ring, whereas those factors were rarely affected by the diameter of the inner steel ring. About 39–65 % of the theoretical elastic stress was relaxed by the sustained interface pressure. Since the actual residual tensile stress of all specimens was less than the tensile strength, the computed cracking potential varied from 0.43 to 0.7, and thus no shrinkage crack was observed. Finally, the degree of restraint provided a linear relationship with the ratio of steel and concrete wall thickness.     

外压型不锈钢波纹管膨胀节开裂分析

奥氏体不锈钢外压轴向型波纹管膨胀节在使用较短时间后发生了开裂。采用化学成分分析、金相检验和断口分析等方法对开裂的原因进行了分析。结果表明:波纹管膨胀节的工作介质过热蒸汽中含有腐蚀性氯离子,在服役环境下受到拉伸应力的作用,导致其发生了应力腐蚀开裂。