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Realization and control of multiple temperature zones in liquid‐containing gas–solid fluidized bed reactor
Authors:Yefeng Zhou  Qiang Shi  Zhengliang Huang  Zuwei Liao  Jingdai Wang  Yongrong Yang
Affiliation:1. State Key Laboratory of Chemical Engineering and College of Chemical and Biological Engineering, Department of Chemical Engineering, Zhejiang University, Zhejiang Province, P. R. China;2. Department of Chemical Engineering, Xiangtan University, Hunan Province, P. R. China
Abstract:Fluidized bed reactors (FBRs) have been developed to establish multiple temperature zones for various industrial processes. To overcome the common weakness, this work proposed to spray liquid into bottom and upper zones, respectively, to realize multiple temperature zones FBR (MTZFBR). Temperature, pressure, and acoustic emission techniques were applied to fully characterize liquid interaction and hydrodynamics. Compared with the bottom liquid‐spraying approach, the upper liquid‐spraying approach showed higher temperature difference (ΔT) and better fluidization stability, thus was selected for further control studies. Effects of liquid flow rate, static bed height, and inlet gas temperature on MTZFBR were studied systematically. The results showed that increasing liquid evaporation behavior or decreasing liquid bridge behavior enhance ΔT and fluidization stability and vice versa. G–L–S fluidization pattern depended mostly on the liquid behaviors and fluidization stability, and thus the stabilized MTZFBR could be regarded as a coexisted mode of two distinctive G–L–S fluidization patterns. © 2016 American Institute of Chemical Engineers AIChE J, 62: 1454–1466, 2016
Keywords:multiple temperature zones  liquid‐containing gas–  solid fluidized bed reactor  realization and control  liquid evaporation and liquid bridge  multiple measurement techniques
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