| HPLC法测定蒙成药布仁他拉哈胡椒碱的含量 |
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| 引用本文： | 吴学军,孟和.HPLC法测定蒙成药布仁他拉哈胡椒碱的含量[J].中国药事,2011,25(3):287-288. |
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| 作者姓名： | 吴学军 孟和 |
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| 作者单位： | 1. 内蒙古通辽市传染病医院,通辽,028000
2. 内蒙古通辽市药品检验所 |
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| 摘 要： | 目的 建立蒙成药布仁他拉哈含量测定方法.方法 采用HPLC法测定胡椒碱的含量,色谱柱为Diamonsil C18柱,流动相为甲醇-水(75:25),检测波长为343nm.结果 胡椒碱在0.03206~0.3206μg范围内呈良好的线性关系(r=0.9999),平均加样回收率为97.72%,RSD为1.08%.结论 该方...
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| 关 键 词： | HPLC 布仁他拉哈 胡椒碱 含量 |
Determination of Peperine in Burentalaha by HPLC |
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| Wu Xuejun,Meng He.Determination of Peperine in Burentalaha by HPLC[J].Chinese Pharmaceutical Affairs,2011,25(3):287-288. |
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| Authors: | Wu Xuejun Meng He |
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| Affiliation: | Wu Xuejun and Meng He1(Hospital for Infectious Diseases of Tongliao City,Inner Mongolia Autonomous Region,Tongliao 028000,1Institute for Drug control of Tongliao City,Inner Mongolia Autonomous Region) |
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| Abstract: | Objective A HPLC method was established for determination of peperine in Burentalaha,prepared Mongolia traditional medicine.Methods A Diamonsil C18 column was used.The mobile phase was methanol-water（75∶25）.The detection wavelength was 343nm.Results The linear range was within 0.03206～0.3206μg,r=0.9999.The average recovery rate was 97.72% and RSD was 1.08%.Conclusion The method is simple,rapid and accurate.It can be used for the quality control of Burentalaha. |
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| Keywords: | HPLC Burentalaha piperine determination |
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